Transition metal halide salts and complexes of 2-aminopyrimidine: Cobalt(II) and nickel(II) compounds, crystal structures of bis(2-aminopyrimidinium)MX4 [M=Co, Ni; X=Cl, Br] and 2-aminopyrimidinium(+2) [NiBr2(H2O)4]Br2

Journal of Coordination Chemistry

Volumn 55, Issue 11, 2002, Pages 1337-1351

  Masaki, M E ^a   Prince, B J ^b   Turnbull, M M ^c  

^a CLARK UNIVERSITY   (United States)

^b UNIVERSITY OF CANTERBURY   (New Zealand)

^c NONE

Author keywords

2 Aminopyrimidine; Cobalt; Metal halides; Nickel crystal structure

Indexed keywords

2 AMINOPYRIDINE; BROMINE; CHLORINE; COBALT COMPLEX; HALIDE; METAL COMPLEX; NICKEL COMPLEX;

ARTICLE; COMPLEX FORMATION; CRYSTAL STRUCTURE; CRYSTALLIZATION; INFRARED SPECTROPHOTOMETRY; SYNTHESIS; X RAY DIFFRACTION;

EID: 0036842812     PISSN: 00958972     EISSN: None     Source Type: Journal    
DOI: 10.1080/0095897021000036587     Document Type: Article

References (33)

1. (a) U. Geiser, R.D. Willett, M. Lindbeck and K. Emerson (1986). J. Am. Chem. Soc., 108, 1173;
2. (b) T.M. Kite and J.E. Drumheller (1981). J. Magn. Res., 54, 253.
3. (a) R.D. Willett, C. Galeriu, C.P. Landee and B. Twamley. Phys. Rev. B., (submitted);
4. (b) B.R. Patyal, B.L. Scott and R.D. Willett (1990). Phys. Rev. B., 41, 1657.
5. (a) C.P. Landee and R.E. Greeney (1992). J. Mag. Mag. Mat., 104-107, 788;
6. (b) N. Sivron, T.E. Grigerei, J.E. Drumheller, K. Emerson, R.D. Willett (1994). J. Appl. Phys., 75, 5952.
7. T.J. Coffey, C.P. Landee, W.T. Robinson, M.M. Turnbull, M. Winn and F.M. Woodward (2000). Inorg. Chim. Acta, 303, 54-60.
8. (a) C.P. Landee, M.M. Turnbull, C. Galeriu, J. Giantsidis and F.M. Woodward (2001). Phys. Rev. B, Rapid Commun., 63, 100402R;
9. (b) M.M. Turnbull, C. Galeriu, J. Giantsidis and C.P. Landee (2002). Mol. Cryst. Liq. Cryst., 376, 469.
10. (a) T. Matsumoto, Y. Miyazaki, A.S. Albrecht, C.P. Landee, M.M. Turnbull and M. Sorai (2000). J. Phys. Chem. B., 104, 9993-10000;
11. (b) F.M. Woodward, C.P. Landee, J. Giantsidis, M.M. Turnbull and C. Richardson (2001). Inorg. Chim. Acta, 324, 324;
12. (c) F.M. Woodward, A.S. Albrecht, C.M. Wynn, C.P. Landee and M.M. Turnbull (2002). Phys. Rev. B, 65, 144412;
13. (d) P.R. Hammar, D.C. Dender, D.H. Reich, A.S. Albrecht and C.P. Landee (1997). J. Appl., Phys., 81, 4615-4617.
14. (a) J. Giantsidis, M.M. Turnbull, C.P. Landee and F.M. Woodward (2002). J. Coord. Chem., 55, 393;
15. (b) J. Giantsidis, C.P. Landee, M.M. Turnbull and F.M. Woodward (2002). J. Coord. Chem., 55, 795.
16. SHELXTL/PC, Siemens Corp., (1990).
17. Siemans (1996). SMART and SAINT, Area Detector Control and Integration Software. Siemans Analytical X-ray Instruments, Inc, Madison, WI, USA.
18. G.M. Sheldrick (1996). SADABS, Program for Empirical Absorption Correction of Area Detector Data. University of G6ttingen, Germany.
19. G.M. Sheldrick (1997). SHELX97-2, Programs for the Solution and Refinement of Crystal Structures. University of G6ttingen, Germany.
20. J.A. Ibers and W.C. Hamilton, (Eds.) (1992). International Tables for Crystallography, Vol. C, Kynoch Press, Birmingham.
21. The structures have been deposited with the CCDC. Ref. numbers: 1, 172760; 2, 172761; 3, 172762; 4, 172762; 5, 172763; 172764
22. w(obs) = 19.56 (22.10 all data), GooF = 1.085. The data has been deposited with the CCDC; Ref. No. 172986.
23. C. Zanchini and R.D. Willett (1990). Inorg. Chem., 29, 3027.
24. (a) G. Pon, R.D. Willett, B.A. Prince, W.T. Robinson and M.M. Turnbull (1997). Inorg. Chim. Acta, 255, 325;
25. (b) R. Corzo-Suarez, S. Garcia-Granda, I. Diaz, V. Fernandez-Herrero and J.L. Martinez (1997). Acta Crystallogr. C, 53, 1786.
26. P. Jensen, S.R. Batten, B. Moubaraki and K.S. Murray (2000). J. Chem. Soc., Chem. Commun., 793.
27. P.O. Lumme, H. Knuuttila and E. Lindell (1996). Acta Cryststallgr., Sect. C (Cr.Str.Comm.), 52, 51.
28. (a) S. Furberg, J. Grogaard and B. Smedsrud (1979). Acta Chem. Scand. Ser. B, 33, 715;
29. (b) J. Scheinbeim and E. Schempp (1976). Acta Crystallogr., Sect. B, 32, 607.
30. T. Manfredini, G.C. Pellacani, A. Bonamartini-Corradi, L.P. Battaglia, G.G.TT. Guarini, J.G. Giusti, G. Pon, R.D. Willett and D.X. West (1990). Inorg. Chem., 29, 2221.
31. See for example; G. Smith, C.H.L. Kennard and K.A. Byriel (1991). Polyhedron, 10, 873. Several pyrimidine bridged copper carboxylate complexes such as this have been reported.
32. F.A. Cotton and G. Wilkinson (1988). Advanced Inorganic Chemistry. John Wiley and Sons, New York.
33. H.B. Silber and M.A. Murguia (1985). Inorg. Chem., 24, 3794.