Facile preparation of chloro-cage-substituted 11-vertex 1-(η6-Arene)-isonido-1,2,4-Ruthenacarboranes from [RuCl2(PPh3)3] and nido-5,6-C2B8H12 in arene solvents

Collection of Czechoslovak Chemical Communications

Volumn 67, Issue 7, 2002, Pages 936-948

  Konoplev, Vitalii E ^a   Pisareva, Irina V ^a   Lemenovskii, Dmitrii A ^a   Petrovskii, Pavel V ^a   Tok, Oleg L ^a   Dolgushin, Fedor M ^a   Chizhevsky, Igor T ^a  

^a A N NESMEYANOV INSTITUTE OF ORGANOELEMENT COMPOUNDS   (Russian Federation)

Author keywords

Arene complexes; Boranes; Isonido Ruthenacarboranes; Metallaboranes; Metallacarboranes; Middle carboranes; NMR spectroscopy, 1H, 11B, 13C, 11B 11B COSY; Ruthenium; X Ray diffraction

Indexed keywords

1,3,5 TRIMETHYLBENZENE; BENZENE; BENZENE DERIVATIVE; CARBORANE DERIVATIVE; DIAMINE DERIVATIVE; DICHLOROETHANE; PARA XYLENE; POLYCYCLIC AROMATIC HYDROCARBON DERIVATIVE; RUTHENIUM COMPLEX; SOLVENT; TOLUENE;

ANALYTIC METHOD; ARTICLE; CHEMICAL BOND; COMPLEX FORMATION; CRYSTAL STRUCTURE; INFRARED SPECTROSCOPY; ISOMERISM; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS; TEMPERATURE; X RAY CRYSTALLOGRAPHY; X RAY DIFFRACTION;

EID: 0036660078     PISSN: 00100765     EISSN: None     Source Type: Journal    
DOI: 10.1135/cccc20020936     Document Type: Article

References (23)

1. Jeffery J. C., Lebedev V. N., Stone F. G. A.: Inorg. Chem 1996, 35, 2967
2. Bown M., Fontaine X. L. R., Greenwood N. N., Kennedy J. D., Thornton-Pett M.: Organometallics 1987, 6, 2254.
3. Bown M., Fontaine X. L. R., Greenwood N. N., Kennedy J. D., Thornton-Pett M.: J. Chem. Soc., Dalton Trans. 1990, 3039.
4. Bown M., Grüner B., Štíbr B., Fontaine X. L. R., Thornton-Pett M., Kennedy J. D.: J. Organomet. Chem. 2000, 614-615, 269.
5. Jones C. J., Francis J. N., Hawthorne M. F.: J. Am. Chem. Soc. 1972, 94, 8391.
6. Hanusa T. P., Huffman J. C., Curtis T. L., Todd L. J.: Inorg. Chem. 1985, 24, 787.
7. Pisareva I. V., Dolgushin F. M., Tok O. L., Konoplev V. E., Suponitsky K. Yu., Yanovsky A. I., Chizhevsky I. T.: Organometallics 2001, 20, 4216.
8. Bennet M. A., Smith A. K.: J. Chem. Soc., Dalton Trans. 1974, 233.
9. See for instance a) Hanusa T. P., Huffman J. C., Todd L. J.: Polyhedron 1982, 1, 77;
10. b) Swisher R. G., Sinn E., Grimes R. N.: Organometallics 1983, 2, 506.
11. Timofeev S. V., Lobanova I. A., Petrovskii P. V., Starikova Z. A., Bregadze V. I.: Russ. Chem. Bull., Int. Ed. 2001, 50, 1683
12. Bown M., Plešek J., Baše K., Štíbr B., Fontaine X. L. R., Greenwood N. N., Kennedy J. D.: Magn. Reson. Chem. 1989, 27, 947.
13. Jung C. W., Hawthorne M. F.: J. Am. Chem. Soc. 1980, 102, 3024.
14. a) Nestor K., Fontaine X. L. R., Greenwood N. N., Kennedy J. D., Plešek J., Štíbr B., Thornton-Pett M.: Inorg. Chem. 1989, 28, 2219;
15. b) Bould J., Rath N. P., Barton L.: Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1997, 53, 416.
16. a) Lee S. S., Knobler C. B., Hawthorne M. F.: J. Organomet. Chem. 1990, 394, 29;
17. b) Garcia M. P., Green M., Stone F. G. A., Somerville R. G., Welch A. J., Briant C. E., Cox D. N., Mingos M. P.: J. Chem. Soc., Dalton Trans. 1985, 2343;
18. c) Kang H. C., Knobler C. B., Hawthorne M. F.: Inorg. Chem. 1987, 26, 3409;
19. d) Lee S. S., Knobler C. B., Hawthorne M. F.: J. Organomet. Chem. 1990, 394, 29.
20. a) Plešek J., Heřmánek S.: Chem. Ind. (London) 1971, 1267;
21. b) Colquhoun H. M., Greenhough T. J., Wallbridge M. G. H., Heřmánek S., Plešek J.: J. Chem. Soc., Dalton Trans. 1978, 944.
22. Stephenson T. A., Wilkinson G.: J. Inorg. Nucl. Chem. 1966, 28, 945.
23. Sheldrick G. M.: SHELXTL97, V5.10. Bruker AXS Inc., Madison (WI) 1997.