The elusive C60S: Three attempted syntheses

Fullerenes Nanotubes and Carbon Nanostructures

Volumn 10, Issue 1, 2002, Pages 37-47

  Heymann, Dieter ^a   Bachilo, Sergei M ^b   Bruce Weisman, R ^b   Marriott, Terry ^b   Cataldo, Franco ^c  

^a RICE UNIVERSITY   (United States)

^b RICE UNIVERSITY   (United States)

^c Soc Lupi Chem Research Institute   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

DESORPTION; IONIZATION; LASER APPLICATIONS; MASS SPECTROMETRY; PHOTOLYSIS; SYNTHESIS (CHEMICAL); ULTRAVIOLET RADIATION;

ULTRAVIOLET PHOTOLYSIS;

FULLERENES;

EID: 0036450470     PISSN: 1536383X     EISSN: None     Source Type: Journal    
DOI: 10.1081/FST-120002928     Document Type: Article

References (29)

1. Krätschmer, W.L.; Lamb, D.; Fostiropoulos, K.; Huffinan, D.R. Nature 1990, 347, 354.
2. Creegan, K.M.; Robbins, J.L.; Robbins, W.K, Millar, J.M.; Sherwood, R.D.; Tindall, P.J.; Cox, D.M.; Smith, III, A.B.; MCCauley, J.P.; Jones, D.R.; Gallagher, R.T.J. J. Am. Chem. Soc. 1992, 114, 1103.
3. Heymann, D.; Stormer, Jr., J.C.; Pierson, M. Carbon 1991, 29, 1053.
4. 70O epoxides of which two were identified in Smith III, A.B.; Strongin, R.M.; Brard, L.; Furst, G.T.; Atkins, J.H.; Romanov, W.J.; Saunders, M.; Jimenez-Vazquez, H.A.; Owens, K.G.; Goldschmidt, R.J. J. Org. Chem. 1996, 6, 1904.
5. Roth, G.; Adelman, P. J. Phys. I (France) 1992, 2, 1541.
6. Burgi, H.B.; Venugopalan, P.; Schwarzenbach, D.; Diederich, F.; Thilgen, C. Helv. Chim. Acta 1993, 76, 2155.
7. Roth, G.; Adelman, P. Appl. Phys. 1993, A56, 169.
8. Roth, G.; Adelman, P.; Knitter, R. Mater. Lett. 1993, 16, 357.
9. Michel, R.H.; Kappes, M.M.; Roth, G.; Adelman, P. Angew. Chem. Int. Ed. Engl. 1994, 33, 1651.
10. Romberg, H.A.; Knupfer, M.; Armbruster, J.F.; Roth, G. Synth. Metals 1995, 70, 1397.
11. Talyzin, A.V.; Ramicov, V.V.; Syrnicov, P.P. Phys. Solid State 1996, 7, 1531.
12. Semkin, V.N.; Drichko, N.V.; Talyzin, A.V.; Graja, A.; Krol, S.; Konarev, D.N.; Lyubovskaya, R.N. Synth. Metals 1998, 93, 207.
13. Gardette, M.F.; Chilouet, A.; Toscani, S.; Allouchi, H.; Agafonov, V.; Rouland, J.C.; Swarc, H.; Céolin, R. Chem. Phys. Lett. 1999, 201, 149.
14. Talyzin, A.; Jansson, U. Thin Solid Films 1999, 350, 113.
15. Grell, A.S.; Masin, F.; Céolin, R.; Gardette, M.E; Swarc, H. Phys. Rev. B 2000, 62, 3722.
16. Talyzin, A.V.; Tergenius, L.E.; Jansson, U. J. Cryst. Growth 2000, 213, 63.
17. Talyzin, A.V.; Grell, A.S.; Masin, F.; Sherman, A.B.; Lemanov, V.V.; Lunkenheimer, P.; Brand, R.; Loidl, A. J. Phys. Chem. B 2001, 105, 1162.
18. Chibante, L.P.F. Rice University, 1994; 52-59, Ph.D. Thesis.
19. Glenis, S.; Cooke, S.; Chen, X.; Labes, M.M. Chem. Mater. 1996, 8, 123.
20. 60S ions.
21. Giesa, S.; Gross, J.H.; Gleiter, R.; Gromov, A.; Krätschmer, W.; Hull, W.E.; Lebedkin, S. Chem. Commun. 1999, 1999, 465.
22. Cataldo, F. Inorg. Chim. Acta. 1995, 232, 27.
23. Cataldo, F.; Heymann, D. Rad. Phys. Chem. 2001, 61, 115.
24. It is conceivable that the peak was due to two or more isomeric compounds.
25. Retention times on the 5PYE column are all about0.5 min longer than on the bp column.
26. The buckyprep column does not resolve the two compounds.
27. Cotton, F.A.; Wilkinson, G.; Murillo, C.A.; Bochmann, M. Advanced Inorganic Chemistry;J. Wiley Interscience Publishers: NY, 1999; 500-501.
28. 60 and sulfur having occurred during the dissolution in o-xylene.
29. Billmers, R.I.; Smith, A.L. J. Chem. Phys. 1991, 95, 4242.