How to make things work again - Troubleshooting using the GC-IDMS determination of triacyglycerols as an example

Clinical Laboratory

Volumn 48, Issue 11-12, 2002, Pages 635-646

  Kress, Michael ^a   Meißner, Dieane ^a   Kaiser, Patricia ^a   Wood, William Graham ^a  

^a INSTAND   (Germany)

Author keywords

Accuracy; Derivatisation; Extraction; Gas chromatography; GC IDMS; Glassware; Glycerol; Internal standard; Isotope dilution; Mass spectrometry; Precision; Recovery; Tripalmitin; Troubleshooting

Indexed keywords

ACYLGLYCEROL; CARBON 13; GLYCEROL; HUMAN SERUM ALBUMIN; SOLVENT; TRIACYLGLYCEROL; TRIPALMITIN;

ACCURACY; ALKALINITY; ANALYTIC METHOD; AQUEOUS SOLUTION; ARTICLE; BLOOD ANALYSIS; BLOOD SAMPLING; CONTROLLED STUDY; EVAPORATION; EXTRACTION; GAS CHROMATOGRAPHY; GLYCEROL BLOOD LEVEL; HUMAN; HYDROLYSIS; INTERMETHOD COMPARISON; ISOTOPE DILUTION ASSAY; ISOTOPE LABELING; LIPID ANALYSIS; MASS SPECTROMETRY; STANDARD;

CARBON RADIOISOTOPES; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; HUMANS; REFERENCE STANDARDS; RESEARCH DESIGN; SERUM ALBUMIN; TRIGLYCERIDES;

EID: 0036445098     PISSN: 14336510     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (1)

1. Siekmann L, Schn̈felder A, Siekmann Anita. Isotope dilution-mass spectrometry of total glycerol in human serum - a reference method in clinical chemistry. Z Anal Chem 1986: 324; 280-1