Crystal structure of 5,11,17,23-tetrakis-cyanomethyl 25,26,27,28-tetrahydroxycalix[4]arene, C36H28N4O4, a test case on microcrystals using synchrotron radiation

Zeitschrift fur Kristallographie - New Crystal Structures

Volumn 217, Issue 1, 2002, Pages 445-448

  Lecouvey, M ^a   Neuman, A ^a   Prange T ^a  

^a UNIVERSITÉ PARIS 13   (France)

Author keywords

[No Author keywords available]

Indexed keywords

5,11,17,23 TETRAKISCYANOMETHYL 25,26,27,28 TETRAHYDROXYCALIX[4]ARENE; CALIXARENE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE; CRYSTAL; CRYSTAL STRUCTURE; CRYSTALLIZATION; RADIOCHEMISTRY; SYNCHROTRON RADIATION;

EID: 0036385375     PISSN: 14337266     EISSN: None     Source Type: Journal    
DOI: 10.1524/ncrs.2002.217.1.445     Document Type: Article

References (7)

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3. Ottwinowski, Z.; Minor, W.: Processing of X-Ray diffraction data collected in oscillation mode. Methods in Enzymol. 276 (1997) 307-326.
4. Sheldrick, G. M.: SHELXL-97. A Program for Refining Crystal Structures. University of Göttingen, Germany 1997.
5. Sheldrick, G. M.: SHELXS-86. Program for Solution of Crystal Structures. University of Göttingen, Germany 1985.
6. Gutsche, D. C.; Bauer, L. J.: Calixarenes. 13. The Conformational Properties of Calix[4]arenes, Calix[6]arenes, Calix[8]arens, and Oxacalixaienes. J. Am. Chem. Soc. 107 (1985) 6052-6059.
7. Soi, A.; Bauer, W.; Mauser, H.; Moll, C.; Hampel, F.; Hirsch, A.: Investigations on the dynamic properties of 25,26,27,28-tetraalkoxycalix[4]arenes: para-substituent- and solvent-dependent properties of paco conformera and determination of thermodynamic parameters of the pinched cone/pinched cone conversion. J. Chem. Soc., Perkin Trans, II (1998) 1471-1478.