Derivatives of N,N'-bis[2-hydroxy-1,1-bis(hydroxymethyl)ethyl]ethanediamide

Journal of the Brazilian Chemical Society

Volumn 13, Issue 2, 2002, Pages 207-217

  Low, John N ^a   Milne, Bruce F ^a   Ross, Jennifer Nicola ^a   Wardell, James L ^b  

^a UNIVERSITY OF ABERDEEN   (United Kingdom)

^b FEDERAL UNIVERSITY OF RIO DE JANEIRO   (Brazil)

Author keywords

Alkylidene formation; Molecular mechanics; Oxymercuriation; Stannylation; X ray crystallography

Indexed keywords

DIAMIDE; MERCURY DERIVATIVE; N,N' BIS(5 HYDROXYMETHYL 2 PHENYL 1,3 DIOXAN 5 YL)ETHANEDIAMIDE; N,N' BIS(5 HYDROXYMETHYL 2,2 DIMETHYL 1,3 DIOXAN 5 YL)ETHANEDIAMIDE; N,N' BIS(5 OXYMETHYL 2 PHENYL 1,3 DIOXAN 5 YL)ETHANEDIAMIDE; N,N' BIS[(5 HYDROXYMETHYL 2 (4 METHOXYPHENYL) 1,3 DIOXAN 5 YL)]ETHANEDIAMIDE; N,N' BIS[(5 HYDROXYMETHYL 2 (4 METHYPHENYL) 1,3 DIOXAN 5 YL)]ETHANEDIAMIDE; N,N' BIS[2 HYDROXY 1,1 BIS(HYDROXYMETHYL)ETHYL]ETHANEDIAMIDE; N,N' BIS[5 (3 CHLOROMERCURI 2 METHOXYPROPYLOXYMETHYL) 2 PHENYL 1,3 DIOXAN 5 YL]ETHANEDIAMIDE; N,N' BIS[TRIS(HYDROXYMETHYL)METHYL]ETHANEDIAMIDE; UNCLASSIFIED DRUG;

ARTICLE; CALCULATION; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL REACTION; CRYSTALLOGRAPHY; ION EXCHANGE; MOLECULAR DYNAMICS; NUCLEAR MAGNETIC RESONANCE; PROTON NUCLEAR MAGNETIC RESONANCE; STEREOISOMERISM; X RAY CRYSTALLOGRAPHY;

EID: 0036381197     PISSN: 01035053     EISSN: None     Source Type: Journal    
DOI: 10.1590/S0103-50532002000200012     Document Type: Article

References (35)

1. Pierce, J.S.; Lunsford, C.D.; Raiford, R.W.; Rush, J.L.; Riley, D.W.; J. Am. Chem. Soc. 1951, 73, 2595.
2. Frankel, M.B. US Patent 3.228.929, 1966 [CA: 64, P9594].
3. EniChem Anic S.P.A.: Jpn. Kokai Tokkyo. J. Patent 62.249.958 (87.249.958), 1988 [CA: 109, P92287].
4. Malhotra, S.L.; Naik, K.N.; MacKinnon, D.N.; Mayo, J.D.; Gagnon, Y.; Goodgrand, H.B.; US Patent 57709737, 1998 [CA: 128, P129292].
5. Wheeler, E.L.; Jancis, E.H.; Gencarelli, R.A.; Barrows, F.H.; US Patent 4.304.714, 1982 [CA: 96, P86482].
6. Dubois, G.E.; Zhi, B.; Roy, G.M.; Stevens, S.Y.; Yalpani, M.; J. Chem. Soc., Chem. Commun. 1992, 1604.
7. Rammo, J; Schneider, H.-J.; Liebigs Ann. 1996, 1957.
8. Ross, J.-N.; Wardell, J.L.; Low, J.N.; Ferguson, G.; Acta Crystallogr. 1996, C52, 228.
9. Mohamadi, F.; Richards, N.G.J.; Guida, W.C.; Liskamp, R.; Lipton, M.; Caulfield, C.; Chang, G.; Hendrickson, T.; Still, W.C.; J. Comput. Chem. 1990, 11, 440.
10. Still, W.C.; Tempczyk, A.; Hawley, R.C.; Hendrickson, T.; J. Am. Chem. Soc. 1990, 12, 6127.
11. Eliel, E.L.; Wilen, S.H.; Organic Stereochemistry; Wiley: New York, 1994.
12. Wardell, J.L. In Inorganic Reactions and Mechanisms; Zuckerman, J.J. ed.; VCH Publications: New York, 1988, Vol. 11, 277.
13. Cremer, D.; Pople, J.A.; J. Amer Chem. Soc. 1975, 97, 1354.
14. Casas, J.S.; García-Tasende, M.S.; Sordo, J.; Coord. Chem. Revs. 1999, 193-195, 283.
15. Holloway, C.E.; Melnik, M.; J. Organomet. Chem. 1995, 495,1.
16. nd ed.; Pergamon Press: Oxford, 1995, Volume 3, p 135;
17. st ed.; Pergamon Press: Oxford, 1982, Volume 1, p 863.
18. Grdenic, D.; Quart. Rev. 1955, 19, 303.
19. Canty, A.J.; Deacon, G.B.; Inorg. Chim. Acta 1980, 45, L225.
20. Batsanov, S.S.; Russ. J. Inorg. Chem. 1991, 36, 1694.
21. th ed., Harper Collins: New York, 1993.
22. Zamora, F.; Sabat, M.; Janik, M.; Siethoff, C.; Lippert, B.; Chem. Commun. 1997, 485.
23. Wardell, J.L.; Wigzell, J.McM.; J. Organomet. Chem. 1982, 244, 225.
24. Cox, P.J.; Doidge-Harrison, S.M.S.V.; Howie, R.A.; Wardell, J.L.; J. Crystallogr. Spectrosc. Res. 1991, 21, 735.
25. Ross, J.-N.; Wardell, J.L.; Low, J.N.; Ferguson, G.; Acta Crystallogr. 1996, C52, 1961.
26. Allen, F. H., Kennard, O.; Chem. Des. Autom. News 1993, 8, 31.
27. see for example, Lo, K.M.; Ng, S.W.; Das, V.G.K.; J. Cryst. Chem. Res. 1997, 12, 933;
28. Fu, F.Z.; Li, H.Y.; Zhu, D.S.; Fang, Q.X., Pan, H.A.; Tiekink, E.R.T.; Kayser, F.; Biesemans, M.; Verbruggen, I.; Willem, R.; Gielen, M.; Organometallics 1995, 490, 163;
29. Jurkschat, K.; Schilling, J.; Mugge, C.; Tzschach, A.; Meunier-Piret, J.; van Meerssche, M.; Gielen, M.; Willem, R.; Organometallics 1988, 7, 38.
30. Enraf-Nonius; CAD4-PC Software; Version 1.1; Delft, Holland, 1992.
31. Gabe, E.J.; Le Page, Y.; Charland, J.-P.; White, P.S.; J. Appl. Cryst. 1989, 22, 384.
32. Sheldrick, G.M; SHELXS-97: Program for the solution of crystal structures; University of Göttingen, Germany, 1997.
33. Sheldrick, G.M.; SHELXL-97; Program for the refinement of crystal structures; University of Göttingen, Germany, 1997.
34. Ferguson, G.; PRPKAPPA - a WordPerfect-5.1 macro to formulate and polish CIF format files from the SHELXL-97 refinement of Kappa-CCD data; University of Guelph, Canada, 1999.
35. Spek, A.L.; PLATON: Molecular Geometry and Graphics Program, January March 2000 version; University of Utrecht, Holland, 2000.