The Knoevenagel condensation reaction of aromatic aldehydes with malononitrile by grinding in the absence of solvents and catalysts

Synthetic Communications

Volumn 32, Issue 22, 2002, Pages 3475-3479

  Ren, Zhongjiao ^a   Cao, Weigud ^a,b   Tong, Weiqi ^a  

^a SHANGHAI UNIVERSITY   (China)

^b SHANGHAI INSTITUTE OF ORGANIC CHEMISTRY   (China)

Author keywords

[No Author keywords available]

Indexed keywords

ALDEHYDE; MALONONITRILE; ORGANIC SOLVENT;

ARTICLE; CATALYST; GRINDING; MICROWAVE IRRADIATION; POLYMERIZATION; ROOM TEMPERATURE;

EID: 0036034963     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1081/SCC-120014780     Document Type: Article

References (29)

1. Tanaka, K.; Toda, F. Chem. Rev. 2000, 100, 1025.
2. Toda, F.; Takumi, H.; Yamaguchi, H. Chem. Exp. 1989, 4, 507.
3. Tanaka, K.; Kishigami, S.; Toda, F. J. Org. Chem. 1991, 56, 4333.
4. Toda, F.; Tanaka, K.; Hamai, K. J. Chem. Soc., Perkin Trans. 1 1990, 3207.
5. Toda, F.; Suzuki, T.; Higa, S. J. Chem. Soc., Perkin Trans. 1 1998, 3521.
6. Toda, F.; Tanaka, K.; Iwata, S. J. Org. Chem. 1989, 54, 3007.
7. Toda, F.; Kiyoshige, K.; Yagi, M. Angew. Chem. Int. Ed. Engl. 1989, 28, 320.
8. (a) Schmeyers, T.; Toda, F.; Boy, J.; Kaupp, G. J. Chem. Soc., Perkin Trans. 2 1998, 989
9. (b) Hagiwara, H.; Obtsubo, S.; Kato, M. Mol. Cryst. Liq. Cryst. 1996, 279, 291
10. (c) Tanaka, M.; Kobayashi, K. J. Chem. Soc., Chem. Commun. 1998, 1965
11. (d) Im, J.; Kim, J.; Kim, S.; Hahu, B.; Toda, F. Tetrahedron Lett. 1997, 38, 451
12. (e) Xiao, J.-P.; Wang, Y.-L.; Zhou, Q.-X. Synth. Commun. 2001, 31, 661
13. (f) Li, J.-P.; Wang, Y.-L.; Wang, H.; Luo, Q.-F.; Wang, X.-Y. Synth. Commun. 2001, 31, 781.
14. (a) Knoevenagel, E. Chem. Ber. 1894, 27, 2345
15. (b) Jones, G. Organic Reactions; Wiley: New York, 1967; Vol. 15, 204
16. Trost, B.M. Comprehensive Organic Synthesis; Pergamon Press: Oxford, 1991; Vol. 2, 341.
17. Lehnert, W. Synthesis 1974, 667.
18. Rao, P.S.; Venkataratnam, R.V. Tetrahedrom Lett. 1991, 32, 5821.
19. Prajapati, D.; Sandhu, J.S. Chem. Lett. 1992, 1945.
20. Prajapati, D.; Sandhu, J.S. J. Chem. Soc., Perkin. Trans. 1 1993, 739.
21. (a) Abdallah-El Ayoubi, S.; Texier-Boullet, F.; Hamelin, J. Synthesis 1994, 258
22. (b) Villemin, D.; Labiad, B. Synth. Commun. 1990, 20, 3207;
23. (c) Villemin, D.; Diez-Barra, E.; Loupy, A.; Langa, F. Tetrahedron Lett. 1996, 37, 1113
24. (d) Kim, S.Y.; Kwon, P.S.; Kwon, W.T. Synth. Commun. 1997, 27, 533
25. (e) Kwon, P.S.; Kim, Y.M.; Kang, J. Synth. Commun. 1997, 27, 4091.
26. (a) Corson, B.B.; Stoughton, R.W. J. Am. Chem. Soc. 1928, 50, 2825
27. (b) Cabello, J.A.; Campel, J.M.; Garcia, A.; Luna, D.; Marinas, J.M. J. Org. Chem. 1984, 49, 5195
28. (c) Sturz, H.G.; Noller, C.R. J. Am. Chem. Soc. 1949, 71, 2949
29. (d) Schiemenz, G.P. Chem. Ber. 1962, 95, 485.