Synthesis and spectral studies of tri- and diorganotin(IV) complexes with 5-benzoyl-α-methyl-2-thiopheneacetic acid: Crystal structure of [(CH3)3Sn(C14H11O3S)]

Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry

Volumn 32, Issue 4, 2002, Pages 665-687

  Ahmad, Fiaz ^a   Parvez, Masood ^a   Ali, Saqib ^a   Mazhar, M ^a   Munir, Arshad ^a  

^a QUAID I AZAM UNIVERSITY   (Pakistan)

Author keywords

[No Author keywords available]

Indexed keywords

ACETIC ACID DERIVATIVE; ORGANOTIN COMPOUND; SILVER; SODIUM CHLORIDE; TIN;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL REACTION; ELECTRIC CONDUCTIVITY; ELECTRON SPIN RESONANCE; INFRARED SPECTROSCOPY; MASS SPECTROMETRY; PROTON NUCLEAR MAGNETIC RESONANCE; ULTRAVIOLET SPECTROPHOTOMETRY; ULTRAVIOLET SPECTROSCOPY; X RAY CRYSTALLOGRAPHY;

EID: 0035998476     PISSN: 00945714     EISSN: None     Source Type: Journal    
DOI: 10.1081/SIM-120004439     Document Type: Article

References (33)

1. Blunden, S.J.; Chapman, A. In Organometallic Compounds in the Enviroment; Craig, P., Ed.; J. Wiley: New York, 1986; 111-159.
2. Thayer, J.S. Organometallic Compounds and Living Organisms; Academic Press: New York, 1984.
3. Blunden, S.J.; Cusack, P.A.; Hill, R. The Industrial Uses of Tin Chemicals; The Royal Society of Chemistry: London, 1985.
4. Crowe, A.J.; Smith, P.J.; Atassi, G. Investigations into the Antitumor Activity of Organotin Compounds. I. Diorganotin Dihalide and Dipseudohalide Complexes. Chem. Biol. Interactions, 1980, 32, 171-178.
5. Gielen, M.; Lilieveld, P.; Devos, D.; William, R. In Metal-Based Antitumour Drugs; Gielen, M., Ed.; Friend Publishing House; Tel Aviv, 1992; Vol. 2, 29-50.
6. Molloy, K.C.; Quill, K.; Nowell, I.W. Organotin Biocides. Part 8. The Crystal Structure of Triphenyltin Formate and Comparative Variable-temperature Tin-119 Mössbauer Spectroscopic Study of Organotin Formate and Acetates. J. Chem. Soc. Dalton Trans. 1987, 101-106.
7. Holmes, R.R. Organotin Cluster Chemistry. Acc. Chem. Res. 1989, 22, 190-197.
8. Molloy, K.C.; Purcell, T.G.; Hahn, E.; Schumann, H.; Zuckerman, J.J. Orgonotin Biocides. 4. Crystal and Molecular Structure of Tricyclohexylstannyl-3indolylacetate, Incorporating the First Monodentate Carboxylate Group Bonded to Triorganotin(IV). Organometallics 1986, 5, 85-89.
9. Bull, W.E.; Madan, S.K.; Willis, J.E. Amides as Ligands. I. Metallic Complexes of N,N-Dimethylacetamide. Inorg. Chem. 1963, 2, 303-306.
10. Nath, M.; Sharma, C.L.; Sharma, N. Dibutyltin(IV) Complexes of Schiff Bases Derived from Amino Acids. Synth. React. Inorg. Met.-Org. Chem. 1991, 21, 807-824.
11. Saxena, A.; Tandan, J.P.; Molloy, K.C.; Zuckerman, J.J. Tin(IV) Complexes of Tridentate Schiff Bases having ONS Donor System. Inorg. Chim. Acta 1982, 63, 71-74.
12. 119mSn Mössbauer Infrared and Mass Spectrometric Studies of Organotin Carboxylates of 2-[(2,3-Dimethyphenyl)amino]benzoic Acid. Their Effect on Microoganism. Synth. React. Inorg. Met.-Org. Chem. 1997, 26, 863-885.
13. Sandhu, G.K.; Boparoy, N.S. Preparation and Sn-119 Mössbauer Spectra of Diorganotin(IV) Complexes of Picolinic Acid and Picolinic Acid N-Oxide. J. Organomet. Chem. 1991, 411, 89-98.
14. 2. J. Organomet. Chem. 1989, 371, C1-C3.
15. Sandhu, G.K.; Gupta, R.; Sandhu, S.S.; Parish, R.V.; Brown, K. Diorganotin(IV) Derivatives of N-Phthaloyl Amino Acids. J. Organomet. Chem. 1985, 279, 373-384.
16. Sandhu, G.K.; Gupta, R.; Sandhu, S.S.; Parish, R.V. Diorganotin(IV) Complexes of N-Acetylamino Acids. Polyhedron 1985, 4, 81-87.
17. Sandhu, G.K.; Gupta, R.; Sandhu, S.S.; Moore, L.S.; Parish, R.V. Diorganotin(IV) Complexes of N-Protected Dipeptides. J. Organomet. Chem. 1986, 311, 281-288.
18. Sandhu, G.K.; Kaur, G. Preparation and Infrared and Tin-119 NMR Spectral Studies of Diorganotin(IV) Derivatives of N-Benzoylglycine and N-Benzoylglycylglycine. Main Group Met. Chem. 1990, 13, 149-165.
19. Harrison, P. G. Chemistry of Tin; Chapman and Hall: U.K., 1989; 71-75.
20. 1H)| and the Me-Sn-Me Angle in Methyltin(IV) Compounds. Inorg. Chem. 1986, 25, 892-895.
21. 13C)| on the C-Sn-C Angle in n-Butyltin(IV) Compounds. Inorg. Chim. Acta 1986, 118, L15-L16.
22. 119Sn NMR Spectra of some Four- and Five-Coordinated Tri-n-butyltin(IV) Compounds. J. Organomet. Chem. 1984, 275, 43-51.
23. 119Sn NMR Spectra of Di-n-butyltin(IV) Compounds. J. Organomet. Chem. 1986, 315, 299-308.
24. 119Sn de Nouveaux Composes Benzyliques Organostanniques. J. Organomet. Chem. 1982, 238, 171-175.
25. Danish, M.; Ali, S.; Mazhar, M.; Badshah, A.; Masood, T.; Tiekink, E.R.T. Crystal and Molecular Structures of Two Polymeric Triorganotin 3-(2-Thienyl)-2-propenoate Derivatives. Main Group Met. Chem. 1995, 18, 27-34.
26. Tiekink, E.R.T.; Sandhu, G.K.; Verma, S.P. Trimethylstannyl-2-furancarboxylate. Acta Cryst. 1989, C45, 1810-1811.
27. Thair, M.; Ülkü, D.; Danish, M.; Ali, S.; Badshah, A.; Mazhar, M. 2-[(2,3-Dimethylphenyl)amino]benzoatetrimethyltin(IV). Acta. Cryst. 1997, C53, 183-185.
28. Kalsoom, A.; Mazhar, M.; Ali, S.; Mahon, M.F.; Molloy, K.C.; Chaudhry, M.I. Synthesis, Characterization and Biological Activity of Organotin Derivatives of Thionaphthaline, Including the Crystal Structure of Triphenyl-2-thionaphthyltin(IV) and Dimethyl-bis(2-thionaphthyl)tin(IV). Appl. Organomet. Chem. 1997, 11, 47-55.
29. Danish, M.; Ali, S.; Mazhar, M.; Badshah, A.; Tiekink, E.R.T. Crystal and Molecular Structures of Bis[(3-(2-furanyl)-2-propenoate)di-n-butyltin]oxide and Triphenyltin 3-(2-furanyl)-2-propenoate. Main Group Met. Chem. 1995, 18, 697-705.
30. Sisido, K.; Takeda, Y.; Kingawa, Z. Direct Synthesis of Organotin Compounds. I. Di- and Tribenzyltin Chloride. J. Am. Chem. Soc. 1961, 83, 538-541.
31. Perrin D.D.; Armarego, W.L.F. Purification of Labortary Chemicals, 3rd Edn., Pergenmon, Oxford, 1988.
32. teXsan, Structural Analysis Package, Molecular Structural Coorporation, Texas, 1992.
33. Walker, N.; Stuart, D. An Empirical Method for Correcting Diffractometer Data for Absorption Effect. Acta Cryst. 1983, A39, 158-166.