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0001589182
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A [1,3]-shift was postulated but not directly observed in a rhodium alkynyl carbene complex that had presumably formed in a catalytic cycle: Padwa, A.; Austin, D. J.; Gareau, Y.; Kassir, J. M.; Xu, S. L. J. Am. Chem. Soc. 1993, 115, 2637.
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0034006818
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(g) Caro, B.; Le Poul, P.; Robin-LeGuen, F.; Séńchal-Tocquer, M.-C.; Saillard, J.-Y.; Kahlal, S.; Ouahab, L.; Golhen, S. Eur. J. Org. Chem. 2000, 577.
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Miguel, D.1
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16
-
-
85036895057
-
-
note
-
Since dimerization is a second-order process and isomerization is a first-order process, low concentrations maximize the [1,3]-metal shift to dimerization ratio.
-
-
-
-
17
-
-
85036898312
-
-
See the Supporting Information
-
See the Supporting Information.
-
-
-
-
19
-
-
85036891905
-
-
note
-
eq = 4.0 for [2d]/[1d]) is probably related to the fact that both arene rings are conjugated with the electron-deficient carbene carbon.
-
-
-
-
20
-
-
85036904878
-
-
note
-
The 20:80 equilibrium ratio of 1d to 2d was solvent-independent.
-
-
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21
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0038281244
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(a) Rerek, M. E.; Ji, L.-N.; Basolo, F. J. Chem. Soc., Chem. Commun. 1983, 1208.
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0001647830
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30
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18844420672
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1H NMR spectrum of this compound is consistent with a low barrier: Fischer, E. O.; Besl, G. Z. Z. Naturforsch., B: Anorg. Chem., Org. Chem. 1979, 34, 1186.
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35
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37049084102
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note
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Dehydrometallacyclobutadienes were identified as key intermediates in the decomposition of active alkyne metathesis catalysts: (a) References 14c, d. (b) Bray, A.; Mortreux, A.; Petit, F.; Petit, M.; Szymanska-Buzar, T. J. Chem. Soc., Chem. Commun. 1993, 197.
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Bray, A.1
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Petit, M.4
Szymanska-Buzar, T.5
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