Nucleation and metastability in crystallization of vanillin and ethyl vanillin

Chemical Engineering Science

Volumn 56, Issue 7, 2001, Pages 2295-2304

  Hussain, Khalid ^a   Thorsen, Gunnar ^a   Malthe Sørenssen, Dick ^b  

^a NORWEGIAN UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Norway)

^b ALTANA PHARMA AG   (Germany)

Author keywords

Ethyl vanillin; Metastable zone; Nucleation; SANS; Thermal history; Vanillin

Indexed keywords

AGGREGATES; CRYSTALLIZATION; DISSOLUTION; HEATING; NEUTRON SCATTERING; NUCLEATION; SATURATION (MATERIALS COMPOSITION);

METASTABLE PHASE;

CHEMICAL ENGINEERING;

CRYSTALLIZATION;

EID: 0035938004     PISSN: 00092509     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0009-2509(00)00438-3     Document Type: Article

References (31)

1. Davey, R. J. (1982). Solvent effects in crystallization processes. Current Topics in Material Science, 8, 429-479.
2. Findlay, A. (1951). The phase rule. USA: Dover Publication Inc.
3. Garside, J. (1984). Fundamental of industrial crystallization. In S. J. Jancic, & E. J. de Jong (Eds.), Industrial crystallization, vol. 84 (pp. 1-7). Netherlands: Hauge.
4. Gago-Duport, L., de la Rosa-Fox, N., & Garcia-Ruiz, J. M. (1995). Nucleation and clustering: a microscopic study of the aggregation behaviour in metastable solutions. Jounal of Non-Crystalline Solids, 192/193, 503-508.
5. Granberg, R. A., Bloch, D. G., & Rasmuson, A. C. (1999). Crystallization of paraacetamol in acetone-water mixtures. Journal of Crystal Growth, 192, 257-270.
6. Hussain, K. (1998). Nucleation and metastability in crystallization from liquid solutions. Ph.D. thesis, Norwegian University of Science and Technology, Trondheim.
7. Kubota, N., & Fujisawa, Y. (1984). The effects of filtration and thermal history on primary nucleation of potassium bromate from aqueous solution. In S. J. Jancic, & E. J. de Jong (Eds.), Industrial crystallization, vol. 84 (pp. 259-262). Netherlands: Hauge.
8. Lee, F., Stoops, C. E., & Lahti, L. E. (1976). An investigation of nucleation and crystal growth mechanism of urea from water-alcohol solutions. Journal of Crystal Growth, 32, 363-370.
9. McCrone, W. C. (1950). Analytical Chemistry, 22, 500.
10. McCrone, W. C. (1965). Polymorphism. In Fox, D., Labes, M. M., & Weissberger, A. (Eds.), Physics and chemistry of the organic solid state, vol. 11 (pp. 725-767). New York: Interscience.
11. Melia, T. P., & Moffitt, W. P. (1964). Crystallization from aqueous solution. Journal of Colloid Science, 19, 433-447.
12. Minezaki, Y., Niimura, N., Ataka, M., & Katsura, T. (1996). Small angle neutron scattering from lysozyme solutions in unsaturated and supersaturated states (SANS from lysozyme solutions). Biophysical Chemistry, 58, 355-363.
13. Mullin, J. W. (1993). Crystallization (3rd ed.). Oxford: Butterworth-Heinemann.
14. Mullin, J. W., & Leci, C. L. (1969). Some nucleation characteristics of aqueous citric acid solutions. Journal of Crystal Growth, 5, 75-76.
15. Myerson, A. S. (1993). In A. S. Myerson (Ed.), Handbook of industrial crystallization. Boston: Butterworth-Heinemann.
16. Myerson, A. S., & Ginde, R. (1993). Crystals, crystal growth and nucleation. In A. S. Myerson (Ed.), Handbook of industrial crystallization. Boston: Butterworth-Heinemann.
17. Myerson, A. S., & Izmailov, A. F. (1993). The structure of supersaturated solutions. In D. T. J. Hurle (Ed.), Handbook of crystal growth, vol. 1, Part A. Amsterdam: North-Holland.
18. Nakai, T. (1972). Effects of the thermal history of a solution to nucleation. Journal of The Chinese Institute of Chemical Engineers, 3, 83-93.
19. Nielsen, A. E. (1964a). Kinetics of precipitation. Oxford: Pergamon press.
20. Nielsen, A. E. (1964b). Kinetics of precipitation. Oxford: Pergamon Press.
21. Niimura, N., Minezaki, Y., Ataka, M., & Katsura, T. (1995). Aggregation in supersaturated lysozyme solution studied by time-resolved small angle neutron scattering. Journal of Crystal Growth, 154, 136-144.
22. Nyvlt, J. (1968). Kinetics and nucleation in solutions. Journal of Crystal Growth, 3(4), 377-383.
23. Nyvlt, J. (1984). Likely grounds of the thermal history of solution. In S. J. Jancic, & E. J. de Jong (Eds.), Industrial crystallization, vol. 84 (pp. 9-13). Netherlands: Hauge.
24. Nyvlt, J., Rychly, R., Gottfried, J., & Wurzelova, J. (1970). Metastable zone width of some aqueous solutions. Journal of Crystal Growth, 6, 151-162.
25. Nyvlt, J., Söhnel, O., Matuchova, M., & Broul, M. (1985). The kinetics of industrial crystallization. Amsterdam: Elsevier.
26. Popovych, O., & Tomkins, R. P. T. (1981). Nonaqueous solution chemistry. New York: Wiley.
27. Sureshkumar, P., Sivakumar, K., & Natarajan, S. (1994). Gel growth of vanillin and its X-ray characterisation. Crystal Research Technology, 29(4), K59-K61.
28. Threlfall, T. L. (1995). Analysis of organic polymorphs -a review. Analyst, 120, 2435-2460.
29. Velavan, R., Sureshkumar, P., Sivakumar, K., & Natarajan, S. (1995). Ada Crystallography, C51, 1131-1133.
30. Vidai, O., Roberts, M. C, & Boue, F. (1998). Gel growth of lysozyme crystals studied by small angle neutron scattering: Case of agarose gel, a nucleation promotor. Journal of Crystal Growth, 192, 257-270.
31. Zettlemoyer, A. C. (1969). Nucleation. New York: Marcel Dekker.