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The crystals obtained from the given solvent have uniform shape, morphology and color. In order to check whether the single crystals represent the bulk X-ray powder diffraction experiments were done. However, the diffraction patterns of the solvated crystals 3-6 did not match with that generated from the single crystal data due to change of the crystal system by desolvation. However, the patterns of desolvated 3-6 were used to follow the interconversion (ESI supporting information).
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