Synthesis and structure of new binuclear organopalladium macrocyclic complexes

Organometallics

Volumn 20, Issue 18, 2001, Pages 3833-3835

  Tsubomura, Taro ^a   Tanihata, Takayuki ^a   Yamakawa, Tetsuya ^a   Ohmi, Rakuko ^a   Tamane, Tsuyoshi ^a   Higuchi, Akon ^a   Katoh, Akira ^a   Sakai, Ken ^a,b  

^a SEIKEI UNIVERSITY   (Japan)

^b TOKYO UNIVERSITY OF SCIENCE   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

BINUCLEAR ORGANOPALLADIUM MACROCYCLIC COMPLEXES; BISDIAMINOMETYLPHENYL UNITS; MACROCYCLIC LIGAND;

CONFORMATIONS; ISOMERS; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS (CHEMICAL); X RAY ANALYSIS;

ORGANOMETALLICS;

EID: 0035802161     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om0103862     Document Type: Article

References (26)

1. Rietveld, M. H. P.; Grove, D. M.; van Koten, G. New J. Chem 1997, 21, 751.
2. (a) van Koten, G.; Jastrzenbski, J. T. B. H.; Noltes, J. G.; Spek, A. L.; Schoone, J. C. J. Organomet. Chem. 1978, 148, 233.
3. (b) Empsall, H. D.; Hyde, E. M.; Markham, R.; McDonald, W. S.; Norton, M. C.; Shaw, B. L.; Weeks, B. J. Chem. Soc., Chem. Commun. 1977, 589.
4. (c) Grove, D. M.; van Koten, G.; Aoet, R.; Murrall, N. W.; Welch, A. J. J. Am. Chem. Soc. 1983, 105, 1379.
5. (d) Grove, D. M.; van Koten, G.; Louwen, J. N.; Noltes, J. G.; Spek, A. L.; Ubbels, H. J. C. J. Am. Chem. Soc. 1982, 104, 6609.
6. Moulton, C. J.; Shaw, B. L. J. Chem. Soc., Dalton Trans. 1976, 1020.
7. Knapen, J. W. J.; van der Made, A. W.; de Wilde, J. C.; van Leeuwen, P. W. N. M.; Wijkens, P.; Grove, D. M.; van Koten, G. Nature 1994, 372, 659.
8. (a) Vifalok, A.; Uzan, O.; Shimon, L. J. W.; Ben-David, Y.; Martin, J. M. L.; Milstein, D. J. Am. Chem. Soc. 1998, 120, 12539.
9. (b) Gupta, M.; Hage, C.; Kaska, W. C.; Cramer, R. E.; Jensen, C. M. J. Am. Chem. Soc. 1997, 119, 840.
10. Stark, M. A.; Jones, G.; Richards, C. J. Organometallics 2000, 19, 1282.
11. (a) Bergbreiter, D. E.; Osburn, P. L.; Liu, U.-S. J. Am. Chem. Soc. 1999, 121, 9538.
12. (b) Ohff, M.; Ohff, A.; van der Boom, M. E.; Milstein, D. J. Am. Chem. Soc. 1997, 119, 11687.
13. (a) Steenwinkel, P.; Kooijman, H.; Smeets, W. J. J.; Spek, A. L.; Grove, D. M.; van Koten, G. Organometallics 1998, 17, 5411.
14. (b) Lagunas, M.-C.; Gossage, R. A.; Spek, A. L.; van Koten, G. Organometallics 1998, 17, 731.
15. James, S. L.; Verspui, G.; Spek, A. L.; van Koten, G. Chem. Commun. 1996, 1309.
16. (a) Hiraki, K.; Tsutsumida, J.; Fuchita, Y. Chem. Lett. 1986, 337.
17. (b) Hiraki, K.; Fuchita, Y.; Ohta Y.; Tsutsumida, J.; Hardcastle, K. I. J. Chem. Soc., Dalton Trans. 1992, 833.
18. Kickham, J. E.; Loeb, S. J. J. Chem. Soc., Chem. Commun. 1993, 1848.
19. (a) Tsubomura, T.; Ezawa, M.; Sato, T.; Sakai, K. Inorg. Chim. Acta 2000, 31, C265.
20. (b) Sato, T.; Sakai, K.; Tsubomura, T. Supramol. Chem. 1996, 7, 157.
21. (c) Tsubomura, T.; Yasaku, K.; Sato, T.; Morita, M. Inorg. Chem. 1992, 31, 447.
22. 1H NMR. See the Supporting Information for details.
23. +, 654, 609, 551, 397, 313. NMR spectra of the reaction mixture showed unidentified products in addition to the isolated complex.
24. 2).
25. 3). See the Supporting Information for details.
26. 2).