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Volumn 20, Issue 7, 2001, Pages 1282-1284

Synthesis and structure of a S4Si4 cage compound

Author keywords

[No Author keywords available]

Indexed keywords

BISTRIMETHYLSILYLMETHYL GROUP; SILICON SULFUR RING; TETRAAMINODISILANE;

EID: 0035795449     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om000899t     Document Type: Article
Times cited : (10)

References (31)
  • 18
    • 0011392867 scopus 로고    scopus 로고
    • note
    • 2S vaporized. The solid that formed was filtered, and the solvent was removed under vacuum. Benzene (10 mL) was added to the crude product. After a second filtration and slow crystallization at room temperature 1 (0.14 g, 0.16 mmol, 27%) was obtained as colorless crystals, suitable for an X-ray crystal structural analysis. For the other analytical investigation the crystals were ground and stored under vacuum for 5 h to remove the benzene.
  • 19
    • 0011483134 scopus 로고    scopus 로고
    • note
    • 12 (878.20): C, 38.3; H, 8.7. Found: C, 37.5; H, 8.8.
  • 20
    • 0011394939 scopus 로고    scopus 로고
    • note
    • 2 on all data by full-matrix least squares with SHELXL-97. All non-hydrogen atoms were refined anisotropically. All hydrogen atoms were included in the model at geometrically calculated positions and refined using a riding model. Other details of the data collection, structure solution, and refinement are listed in Table 1.
  • 23
    • 0011441798 scopus 로고    scopus 로고
    • Diplomarbeit, Universität Göttingen
    • Ackerhans, C. Diplomarbeit, Universität Göttingen, 1998.
    • (1998)
    • Ackerhans, C.1
  • 31
    • 0004150157 scopus 로고
    • Universität Göttingen
    • Sheldrick, G. M. SHELX-93; Universität Göttingen, 1993.
    • (1993) SHELX-93
    • Sheldrick, G.M.1


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.