Photochemical synthesis of metal carbonyl complexes of tetraalkyldiphosphine disulfides, [M2(CO)10(μ-R2P(S)P(S)R2)] (M = Mo, W; R = Me, Et, n-Pr, n-Bu)

Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry

Volumn 31, Issue 10, 2001, Pages 1843-1851

  Şentürk, Ozan Sanlı ^a   Ugˇur, Fadime ^a  

^a EGE UNIVERSITY   (Turkey)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0035565366     PISSN: 00945714     EISSN: None     Source Type: Journal    
DOI: 10.1081/SIM-100108266     Document Type: Article

References (18)

1. Baker, K.; Fowles, G.W. A Sulphur Complexes of Quadrivalent Titanium. J. Less Common Met. 1965, 8, 45.
2. Cowley, A.H. The Chemistry of the Phosphorus-Phosphorus Bond. Chem. Rev. 1965, 65 (6), 617.
3. Meek, D.W.; Nicpon, P. Metal Complexes of Tertiary Phosphine Sulfides. J. Chem. Soc. 1965, 37, 4951.
4. Cotton, F.A.; Franz, B.A.; Hunter, D.L.; Mester, Z.C. Copper(I) and Copper(II) Complexes of Tetramethyldiphosphinedisulfide. Structural Characterization of the Dinuclear, Molecular Complex of Copper(I) Chloride. Inorg. Chim. Acta 1974, 11, 111.
5. 2. Inorg. Chim. Acta 1974 11, 119.
6. 2 (Pt-Pt). Inorg. Chem. 1975, 14, 1121.
7. n). Polyhedron 1997, 16, 1101.
8. Moeller, T.; Birch, H.J.; Nielson, N.C. Phosphorus(V) Sulfochloride. Inorg. Synth. 1953, 4, 71. Butler, S.A.; Chatt, J. Ethylenebis(dimethylphosphine) [1,2-bis(dimethylphosphino)ethane], Tetramethyl diphosphine Disulfides, and Tetramethyldiphosphine. Inorg. Synth. 1974, 15, 186. Vogel, A.I. Purification of the Common Organic Solvents. In Text-book of Practical Organic Chemistry; 3rd Edn.; Longman London, 1977; 139-145, 163-179, 193 and 280-288. Nierbergall, H.; Langenfeld, B. Synthese von Tetraorgano-diposphinen, Diorganophosphinen und Tetraorgano diphosphindisulfiden. Chem. Ber. 1962, 95, 64.
9. Moeller, T.; Birch, H.J.; Nielson, N.C. Phosphorus(V) Sulfochloride. Inorg. Synth. 1953, 4, 71. Butler, S.A.; Chatt, J. Ethylenebis(dimethylphosphine) [1,2-bis(dimethylphosphino)ethane], Tetramethyl diphosphine Disulfides, and Tetramethyldiphosphine. Inorg. Synth. 1974, 15, 186. Vogel, A.I. Purification of the Common Organic Solvents. In Text-book of Practical Organic Chemistry; 3rd Edn.; Longman London, 1977; 139-145, 163-179, 193 and 280-288. Nierbergall, H.; Langenfeld, B. Synthese von Tetraorgano-diposphinen, Diorganophosphinen und Tetraorgano diphosphindisulfiden. Chem. Ber. 1962, 95, 64.
10. Moeller, T.; Birch, H.J.; Nielson, N.C. Phosphorus(V) Sulfochloride. Inorg. Synth. 1953, 4, 71. Butler, S.A.; Chatt, J. Ethylenebis(dimethylphosphine) [1,2-bis(dimethylphosphino)ethane], Tetramethyl diphosphine Disulfides, and Tetramethyldiphosphine. Inorg. Synth. 1974, 15, 186. Vogel, A.I. Purification of the Common Organic Solvents. In Text-book of Practical Organic Chemistry; 3rd Edn.; Longman London, 1977; 139-145, 163-179, 193 and 280-288. Nierbergall, H.; Langenfeld, B. Synthese von Tetraorgano-diposphinen, Diorganophosphinen und Tetraorgano diphosphindisulfiden. Chem. Ber. 1962, 95, 64.
11. Moeller, T.; Birch, H.J.; Nielson, N.C. Phosphorus(V) Sulfochloride. Inorg. Synth. 1953, 4, 71. Butler, S.A.; Chatt, J. Ethylenebis(dimethylphosphine) [1,2-bis(dimethylphosphino)ethane], Tetramethyl diphosphine Disulfides, and Tetramethyldiphosphine. Inorg. Synth. 1974, 15, 186. Vogel, A.I. Purification of the Common Organic Solvents. In Text-book of Practical Organic Chemistry; 3rd Edn.; Longman London, 1977; 139-145, 163-179, 193 and 280-288. Nierbergall, H.; Langenfeld, B. Synthese von Tetraorgano-diposphinen, Diorganophosphinen und Tetraorgano diphosphindisulfiden. Chem. Ber. 1962, 95, 64.
12. Christen, P.J.; Van der Linde, L.M.; Hooge, F.N. The Reaction of Alkylmagnesium Halides with Thiophosphoryl Chloride. Rec. Trav. Chim. 1959, 78, 161.
13. Cotton, F.A.; Wilkinson, G. Photochemical Reactions of Metal Carbonyls. Advanced Inorganic Chemistry, 5th Edn.; Wiley Interscience: New York, 1988; 1047.
14. 5-phosphane (Tetramethyldiphosphine Disulfides) and the Vibrational Spectra and Structures of some its Complexes. J. Chem. Soc., Dalton Trans. 1979, 895. Cowley, A.H.; White, W.D. The Vibrational Spectra and Structures of Phosphorus Compounds. Diphosphine Disulfides. Spectrochim. Acta 1966, 22, 1431.
15. 5-phosphane (Tetramethyldiphosphine Disulfides) and the Vibrational Spectra and Structures of some its Complexes. J. Chem. Soc., Dalton Trans. 1979, 895. Cowley, A.H.; White, W.D. The Vibrational Spectra and Structures of Phosphorus Compounds. Diphosphine Disulfides. Spectrochim. Acta 1966, 22, 1431.
16. 5-phosphane (Tetramethyldiphosphine Disulfides) and the Vibrational Spectra and Structures of some its Complexes. J. Chem. Soc., Dalton Trans. 1979, 895. Cowley, A.H.; White, W.D. The Vibrational Spectra and Structures of Phosphorus Compounds. Diphosphine Disulfides. Spectrochim. Acta 1966, 22, 1431.
17. 5-phosphane (Tetramethyldiphosphine Disulfides) and the Vibrational Spectra and Structures of some its Complexes. J. Chem. Soc., Dalton Trans. 1979, 895. Cowley, A.H.; White, W.D. The Vibrational Spectra and Structures of Phosphorus Compounds. Diphosphine Disulfides. Spectrochim. Acta 1966, 22, 1431.
18. 4. J. Organomet. Chem. 1989, 373, 269.