Conformational properties and intramolecular weak interactions in substituted dithia[3.3.1]metacyclophanes

Chemistry Letters

Volumn , Issue 6, 2001, Pages 586-587

  Moriguchi, Tetsuji ^a   Inoue, Megumi ^a   Sakata, Kazunori ^a   Tsuge, Akihiko ^a  

^a KYUSHU INSTITUTE OF TECHNOLOGY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 0035533967     PISSN: 03667022     EISSN: None     Source Type: Journal    
DOI: 10.1246/cl.2001.586     Document Type: Article

References (14)

1. "Cyclophanes," ed. by P. M. Keehn and S. M. Rosenfeld, Academic Press, New York (1983) Vol. I and II; V. Boekelheide, "Topics in Current Chemistry," ed. by F. L. Boschke, Springger-Verlag, Berlin (1987); F. Diederich, "Cyclophanes," The Royal Society of Chemistry, Cambridge (1989); "Monographs in Supramolecular Chemistry," ed. by J. F. Stoddart; The Royal Society of Chemistry, Cambridge (1989), Vol I; J. M. Lehn, "Supramolecular Chemistry," VCH, Weinheim (1995); "Suplamolecular Control of Structure and Reactivity," ed. by A. D. Hamilton, Weiley, Chichester (1996).
2. "Cyclophanes," ed. by P. M. Keehn and S. M. Rosenfeld, Academic Press, New York (1983) Vol. I and II; V. Boekelheide, "Topics in Current Chemistry," ed. by F. L. Boschke, Springger-Verlag, Berlin (1987); F. Diederich, "Cyclophanes," The Royal Society of Chemistry, Cambridge (1989); "Monographs in Supramolecular Chemistry," ed. by J. F. Stoddart; The Royal Society of Chemistry, Cambridge (1989), Vol I; J. M. Lehn, "Supramolecular Chemistry," VCH, Weinheim (1995); "Suplamolecular Control of Structure and Reactivity," ed. by A. D. Hamilton, Weiley, Chichester (1996).
3. "Cyclophanes," ed. by P. M. Keehn and S. M. Rosenfeld, Academic Press, New York (1983) Vol. I and II; V. Boekelheide, "Topics in Current Chemistry," ed. by F. L. Boschke, Springger-Verlag, Berlin (1987); F. Diederich, "Cyclophanes," The Royal Society of Chemistry, Cambridge (1989); "Monographs in Supramolecular Chemistry," ed. by J. F. Stoddart; The Royal Society of Chemistry, Cambridge (1989), Vol I; J. M. Lehn, "Supramolecular Chemistry," VCH, Weinheim (1995); "Suplamolecular Control of Structure and Reactivity," ed. by A. D. Hamilton, Weiley, Chichester (1996).
4. "Cyclophanes," ed. by P. M. Keehn and S. M. Rosenfeld, Academic Press, New York (1983) Vol. I and II; V. Boekelheide, "Topics in Current Chemistry," ed. by F. L. Boschke, Springger-Verlag, Berlin (1987); F. Diederich, "Cyclophanes," The Royal Society of Chemistry, Cambridge (1989); "Monographs in Supramolecular Chemistry," ed. by J. F. Stoddart; The Royal Society of Chemistry, Cambridge (1989), Vol I; J. M. Lehn, "Supramolecular Chemistry," VCH, Weinheim (1995); "Suplamolecular Control of Structure and Reactivity," ed. by A. D. Hamilton, Weiley, Chichester (1996).
5. "Cyclophanes," ed. by P. M. Keehn and S. M. Rosenfeld, Academic Press, New York (1983) Vol. I and II; V. Boekelheide, "Topics in Current Chemistry," ed. by F. L. Boschke, Springger-Verlag, Berlin (1987); F. Diederich, "Cyclophanes," The Royal Society of Chemistry, Cambridge (1989); "Monographs in Supramolecular Chemistry," ed. by J. F. Stoddart; The Royal Society of Chemistry, Cambridge (1989), Vol I; J. M. Lehn, "Supramolecular Chemistry," VCH, Weinheim (1995); "Suplamolecular Control of Structure and Reactivity," ed. by A. D. Hamilton, Weiley, Chichester (1996).
6. "Cyclophanes," ed. by P. M. Keehn and S. M. Rosenfeld, Academic Press, New York (1983) Vol. I and II; V. Boekelheide, "Topics in Current Chemistry," ed. by F. L. Boschke, Springger-Verlag, Berlin (1987); F. Diederich, "Cyclophanes," The Royal Society of Chemistry, Cambridge (1989); "Monographs in Supramolecular Chemistry," ed. by J. F. Stoddart; The Royal Society of Chemistry, Cambridge (1989), Vol I; J. M. Lehn, "Supramolecular Chemistry," VCH, Weinheim (1995); "Suplamolecular Control of Structure and Reactivity," ed. by A. D. Hamilton, Weiley, Chichester (1996).
7. T. Otsubo, M. Kitagawa, and S. Misumi, Bull. Chem. Soc. Jpn., 52, 1515 (1979); M. F. Semmelhack, Y. Thebtaranonth, and L. Keller, J. Am. Chem. Soc., 99, 959 (1977).
8. T. Otsubo, M. Kitagawa, and S. Misumi, Bull. Chem. Soc. Jpn., 52, 1515 (1979); M. F. Semmelhack, Y. Thebtaranonth, and L. Keller, J. Am. Chem. Soc., 99, 959 (1977).
9. K. Böckmann and F. Vögtle, Chem. Ber., 114, 1965 (1981); A. Tsuge, H. Takeo, H. Kabashima, T. Moriguchi, S. Mataka, and M. Tashiro, Chem.Lett., 1996, 425.
10. K. Böckmann and F. Vögtle, Chem. Ber., 114, 1965 (1981); A. Tsuge, H. Takeo, H. Kabashima, T. Moriguchi, S. Mataka, and M. Tashiro, Chem.Lett., 1996, 425.
11. R. H. Mitchell and V. Boekelheide, J. Am. Chem. Soc., 96, 1547 (1973).
12. w = 0.069; 6686 unique reflections with 2θ ≤ 55.6°. Of these, 6076 I > 2.00 σ(I).
13. w = 0.114; 4620 unique reflections with 2θ ≤ 60.1°. Of these, 3433 I > 3.00 σ(I).
14. w = 0.236; 6093 unique reflections with 2θ ≤ 55.6°. Of these, 1914 I > 2.00 σ(I). Intensity data for MCP 3 and 6 were collected on a Rigaku RAXIS-4 imaging plate with graphite-monochromatized Mo Kα radiation. Intensity data for MCP 4 were collected on a Rigaku AFC-7R diffractmeter with graphite-mono-chromatized Mo Kα radiation. All structures were solved with teXsan crystallographic software package of Molecular Structure Corporation.