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2O, TSP): δ0.93(d, J =6.6 Hz, 12H), 1.36 (m, 2H), 1.55(m, 2H), 1.73 (m, 2H), 2.42 (s, 6H), 2.62-2.95 (m, 8H), 3.21 (s, 2H), 3.25 (dd, J = 4.0 Hz, 10.3 Hz, 2H).
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2O: C, 38.04; H, 7.13; N, 6.65%. Found: C, 38.06; H, 7.16; N, 6.68%, indicating a position of one crystal water was not determined by X-ray analysis.
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