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0007234881
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note
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77], and recrystallization from MeCN.
-
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19
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0007173172
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note
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29Si NMR (CP/MAS 80 Hz, 25.0 °C): δ -81.5.
-
-
-
-
20
-
-
0007227396
-
-
note
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w = 0.078, and GOF = 1.50 (6192 total reflections, 6192 unique reflections of which 3959 with I > 2.00σ(I) were used in all calculations).
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21
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