Dinuclear [RNi(oxam)NiR] complexes (oxam = N1,N2-bis(2-pyridylmethyl)-N3,N4-bis (2,4,6-trimethylphenyl)-oxalamidinate; R = Me, Ph, C≡CH, C≡CPh): Reactions of the methyl complex and formation of [Li(THF)]2Li2Ni2Me8 and [Li(THF)]4Ni2Me8

Organometallics

Volumn 20, Issue 20, 2001, Pages 4221-4229

  Walther, Dirk ^a   Stollenz, Michael ^a   Görls, Helmar ^a  

^a FRIEDRICH SCHILLER UNIVERSITY JENA   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ELEMENTAL ANALYSIS; OXALAMIDINATO BRIDGE; SODIUM ACETYLIDE;

CATALYSIS; CHEMICAL ANALYSIS; CHEMICAL BONDS; COMPLEXATION; CRYSTALLIZATION; MASS SPECTROMETRY; METHANE; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SOLUTIONS; X RAY CRYSTALLOGRAPHY;

ORGANOMETALLICS;

EID: 0035497139     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om000960u     Document Type: Article

References (63)

1. Döhler, T.; Görls, H.; Walther, D. J. Chem. Soc., Chem. Commun. 2000, 945.
2. (a) Negishi, E.; Liu, F. Metal-catalyzed Cross-coupling Reactions; Diederich, F., Stang, P. J., Eds.; Wiley-VCH: Weinheim, 1998; Vol. 34, and references therein.
3. (b) Cárdenas, D. J. Angew. Chem. 1999, 111, 3201.
4. Cárdenas, D. J. Angew. Chem. Int. Ed. 1999, 38, 3018, and references therein.
5. (c) Negishi, E.; Takahashi, T.; Baba, S.; van Horn, D. E.; Okukado, N. J. Am. Chem. Soc. 1987, 109, 2393.
6. (d) Negishi, E.; Takahashi, T.; Akiyoshi, K. J. Organomet. Chem. 1987, 334, 181.
7. (e) Amatore, C.; Azzabi, M.; Jutand, A. J. Am. Chem. Soc. 1991, 113, 8375.
8. (f) Hartwig, J. F.; Paul, F. J. Am. Chem. Soc. 1995, 117, 5373.
9. Pasquali, M.; Floriani, C.; Chiesi-Villa, A.; Guastini, C. J. Am. Chem. Soc. 1979, 101, 4740.
10. Feeling, P.; Döring, M.; Knoch, F.; Beckert, R.; Görls, H. Chem. Ber. 1995, 128, 405.
11. Döring, M.; Görls, H.; Beckert, R. Z. Anorg. Allg. Chem. 1994, 620, 551.
12. Beckert, B.; Vorwerk, S.; Lindauer, D.; Döring, M. Z. Naturforsch. 1993, 48b, 1186.
13. Döring, M., Fehling, P.; Görls, H.; Imhof, W.; Beckert, R., Lindauer, D. J. Prakt. Chem. 1999, 341, 748.
14. Ruben, M.; Rau, S.; Skirl, A.; Krause, K.; Görls, H.; Walther, D.; Vos, J. G. Inorg. Chim. Acta 2000, 303, 206.
15. (a) Hofman, W. E. Proc. Indiana Acad. Sci. 1969, 79, 129.
16. Hofman, W. E. Chem. Abstr. 1970, 73, 126513r.
17. (b) Papavil, E. Anal. Stiint. Univ. Jasi, Sect. 110 1964, 115
18. Papavil, E. Chem. Abstr. 1965, 63, 14351h.
19. Allen, F. H.; Kennard, O.; Taylor, R. Acc. Chem. Res. 1983, 16, 146.
20. Klein, H.-F.; Wiemer, T.; Menu, M.-J.; Dartiguenave, M.; Dartiguenave, Y. Inorg. Chim. Acta 1988, 154, 21.
21. Klein, H.-F.; Wiemer, T.; Menu, M.-J.; Dartiguenave, M.; Dartiguenave, Y. Inorg. Chim. Acta 1991, 189, 45.
22. Klein, H.-F.; Wiemer, T.; Menu, M.-J.; Dartiguenave, M.; Dartiguenave, Y. Inorg. Chim. Acta 1991, 189, 35.
23. (a) Kaiser, S. W.; Saillant, R. B.; Butler, W. M.; Rasmussen, P. G. Inorg. Chem. 1976, 15, 2681.
24. (b) Haddad, M. S.; Duesler, E. N.; Hendrickson, D. N. Inorg. Chem. 1979, 18, 141.
25. (c) Garcia, M. P.; Lopez, A. M.; Esteruealas, M. A.; Lahoz, F. J.; Oro, L. A. Chem. Commun. 1988, 793.
26. (d) Garcia, M. P.; Lopez, A. M.; Esteruealas, M. A.; Lahoz, F. J.; Oro, L. A. J. Chem. Soc., Dalton Trans. 1990, 3465.
27. (e) Esteruealas, M. A.; Lahoz, F. J.; Lopez, A. M.; Onate, E.; Oro, L. A.; Ruiz, N.; Sola, E.; Tolosa, J. I. Inorg. Chem. 1996, 35, 7811.
28. (f) de Souza Lemos, S.; Bessler, K. E.; Schulz Lang, E. Z. Anorg. Allg. Chem. 1998, 624, 30.
29. (g) de Souza Lemos, S.; Bessler, K. E.; Schulz Lang, E. Z. Anorg. Allg. Chem. 1998, 624, 701.
30. (h) Rau, S.; Ruben, M.; Büttner, T.; Temme, C.; Dautz, S.; Görls, H.; Rudolph, M.; Walther, D.; Brotkorb, A.; Duati, M.; O'Connor, C.; Vos, J. G. J. Chem. Soc., Dalton Trans. 2000, 3649.
31. (i) Rau, S.; Büttner, T.; Temme, C.; Ruben, M.; Görls, H.; Walther, D.; Duati, M.; Fanni, S.; Vos, J. G. Inorg. Chem. 2000, 39, 1621.
32. (a) Brewe, G.; Sinn, E. Inorg. Chem. 1985, 24, 4580.
33. (b) Real, A.; Zarembowitch, J.; Kahn, O.; Solans, X. Inorg. Chem. 1987, 26, 2939.
34. (c) Sletten, J. Daraghmeh, H.; Lioret, F.; Julve, M. Inorg. Chim. Acta 1998, 279, 127.
35. (d) Mikuriya, M. Fukumoto, H.; Kako, T. Inorg. Chem. Commun. 1998, 1, 225.
36. (e) Baumann, F. Stange, A., Kaim, W. Inorg. Chem. Commun. 1998, 1, 305.
37. (f) De Munno, G.; Julve, M.; Lioret, F.; Faus, J.; Caneschi, A. J. Chem. Soc., Dalton Trans. 1994, 1175.
38. (g) Castro, I.; Sletten, J.; Glaerum, L. K.; Lioret, F.; Faus, J.; Julve, M. J. Chem. Soc., Dalton Trans. 1994, 2777.
39. (h) De Munno, G.; Viau, G.; Lioret, F.; Faus, J. Inorg. Chim. Acta 1997. 257, 121.
40. (i) Klein, A.; Kaim, W.; Hornung, F. M.; Fiedler, J. Zalis, S. Inorg. Chim. Acta 1997, 264, 269.
41. (k) Vogler, C.; Hausen, H.-D.; Kaim, W.; Kohlmann, S.; Kramer, H. E. A.; Rieker, J. Angew. Chem., Int. Ed. Engl. 1989, 28, 1659.
42. (l) Schwach, M.; Hausen, H.-D.; Kaim, W. Chem. Eur. J. 1996, 2, 446.
43. Tadokoro, M.; Sato, K.; Shiomi, D.; Takui, T.; Itoh, K. Mol. Cryst. Liq. Cryst. Sci. Technol., Sect. A 1997, 306, 49.
44. de Munno, G.; Julve, M.; Lioret, F.; Derory, A. J. Chem. Soc., Dalton Trans. 1993, 1179.
45. Taube, R.; Honymus, G. Angew. Chem. 1975, 87, 291.
46. Kurras, E.; Otto, J. J. Organom. Chem. 1965, 4, 114.
47. Krause, J.; Marx, G.; Schödl, G. J. Organomet. Chem. 1970, 21, 159.
48. Hao, S.; Gambarotta, S.; Bensimon, C. J. Am. Chem. Soc. 1992, 114, 3556.
49. Hao, S.; Song, J.-I.; Berno, P.; Gambarotta, S. Organometallics 1994, 13, 1326.
50. Cotton, F. A.; Troup, J. M.; Webb, D. H.; Williamson, G.; Wilkinson, J J. Am. Chem. Soc. 1974, 96, 3824.
51. Cotton, F. A.; Gage, L. D.; Mertis, L. W.; Shive, G.; Wilkinson, J. J. Am. Chem. Soc. 1976, 98, 6922.
52. Wyrwa, R.; Görls, H. Z. Anorg. Allg. Chem. 1999, 625, 1904.
53. Bauer, R. Ber. Dtsch. Chem. Ges. 1907, 40, 2650.
54. (a) Lindauer, D.; Beckert, R.; Döring, M.; Fehling, P.; Görls, H. J. Prakt. Chem. 1995, 337, 143.
55. (b) Langer, P.; Döring, M.; Wuckelt, J.; Görls, H. Eur. J. Inorg. Chem. 2001, 805.
56. Walther, D.; Stollenz, M.; Böttcher, L.; Görls, H. Z. Anorg. Allg. Chem., in press.
57. MOLEN, An Interactive Structure Solution Procedure; Enraf-Nonius: Delft, The Netherlands, 1990.
58. COLLECT, Data Collection Software; Nonius B.V., Netherlands, 1998.
59. Otwinowski, Z.; Minor, W. Processing of X-ray Diffraction Data Collected in Oscillation Mode. In Methods in Enzymology, Vol. 276, Macromolecular Crystallography, Part A; Carter, C. W., Sweet, R. M., Eds.; Academic Press: San Diego, 1997; pp 307-326.
60. Sheldrick, G. M. Acta Crystallogr. Sect. A 1990, 46, 467-473.
61. Sheldrick, G. M. SHELXL-97; University of Göttingen: Germany, 1993.
62. Further details of the crystal structure investigations are available on request from the director of the Cambridge Crystallographic Data Centre, 12 Union Road, GB-Cambridge CB2 1 EZ, on quoting the depository number CCSD-150911 (1), CCSD-164309 (3b), CCSD-150913 (5), and CCSD-150914 (6), the names of the authors, and the journal citation.
63. CCSD-150912 (3a) (private communication).