9-(1-Acetoxyethylidene)fluorene (′diacetylfluorene′), a by-product from the acetylation of 9-fluorenyllithium

Acta Crystallographica Section C: Crystal Structure Communications

Volumn 57, Issue 4, 2001, Pages 428-430

  Robinson, Paul D ^a   Lutfi, Hisham G ^a   Hou, Yuqing ^a   Meyers, Cal Y ^a  

^a SOUTHERN ILLINOIS UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ACETYLATION; ALKYLATION; CHEMICAL BONDS; CHROMATOGRAPHY; CRYSTALLINE MATERIALS; NUCLEAR MAGNETIC RESONANCE; X RAY ANALYSIS;

STRUCTUTAL DISTORTIONS;

ORGANIC COMPOUNDS;

EID: 0035298624     PISSN: 01082701     EISSN: None     Source Type: Journal    
DOI: 10.1107/S0108270100020539     Document Type: Article

References (21)

1. Caine, D. (1979). Carbon-Carbon Bond Formation, Vol. 1, edited by R. L. Augustine, pp. 85-352. New York: Marcel Dekker.
2. Eliel, E. L. & Wilen, S. H. (1994). Stereochemistry of Organic Compounds, pp. 738 ff. New York: Wiley-Interscience, John Wiley and Sons.
3. Greenhow, E. J., White, E. N. & McNeil, D. (1953). J. Chem. Soc. pp. 3099-3105.
4. Johnson, C. K. (1965). ORTEP. Report ORNL-3794. Oak Ridge National Laboratory, Tennessee, USA.
5. Johnson, F. (1968). Chem. Rev. 68, 375-413.
6. Lambert, J. B. (1989). Conformational Analysis of Cyclohexenes, Cyclohexadienes and Related Hydroaromatic Compounds, edited by P. W. Rabideau, pp. 47-63. New York: VCH.
7. Malhotra, S. K. & Johnson, F. (1968). Chem. Commun, pp. 1149-1150.
8. Meyers, C. Y., Lutfi, H. G. & Robinson, P. D. (2000). Acta Cryst. C56, IUC0000220.
9. Meyers, C. Y., Wahner, A. P., Manohar, S. K., Carr, S. E., Chan-Yu-King, R. & Robinson, P. D. (1991). Acta Cryst. C47, 1236-1239.
10. Miller, H. F. & Bachman, B. (1935). J. Am. Chem. Soc. 57, 766-771.
11. Molecular Structure Corporation (1996). MSC/AFC Diffractometer Control Software. MSC, 9009 New Trails Drive, The Woodlands, TX 77381, USA.
12. Molecular Structure Corporation (1997). TEXSAN. MSC, 9009 New Trails Drive, The Woodlands, TX 77381, USA.
13. Naik, S. N., Pandey, B. & Ayyangar, N. R. (1988). Synth. Commun. 18, 625-632.
14. Ohwada, T. & Shudo, K. (1988). J. Am. Chem. Soc. 110, 1862-1870.
15. Robinson, P. D., Lutfi, H. G., Hou, Y. & Meyers, C. Y. (2000). Acta Cryst. C56, 1380-1382.
16. Rouzaud, J., Cauquil, G. & Boyer, J. (1965). Bull. Soc. Chim. Fr. pp. 2345-2353.
17. Scherf, G. W. H. & Brown, R. K. (1961). Can. J. Chem. 39, 1613-1618.
18. Sheldrick, G. M. (1990). Acta Cryst. A46, 467-473.
19. Sheldrick, G. M. (1997). SHELXL97. University of Göttingen, Germany.
20. Spek, A. L. (2000) PLATON. Utrecht University, The Netherlands.
21. Von, I. & Wagner, E. C. (1944). J. Org. Chem. 9, 155-169.