Solid-state NMR and small-angle X-ray scattering study of microphase structure of amorphous and semicrystalline poly(styrene-ethylene oxide) diblock copolymers

Macromolecules

Volumn 34, Issue 5, 2001, Pages 1258-1266

  Yu, Hongshi ^a   Natansohn, Almeria ^a   Singh, Marsha A ^a   Torriani, Iris ^b  

^a QUEEN S UNIVERSITY   (Canada)

^b LABORATÓRIO NACIONAL DE LUZ SÍNCROTRON   (Brazil)

Author keywords

[No Author keywords available]

Indexed keywords

AMORPHOUS MATERIALS; APPROXIMATION THEORY; COMPUTER SIMULATION; CRYSTAL STRUCTURE; CRYSTALLINE MATERIALS; DIFFERENTIAL SCANNING CALORIMETRY; DIFFUSION IN SOLIDS; MORPHOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYETHYLENE OXIDES; POLYSTYRENES; X RAY SCATTERING;

SEMICRYSTALLINE POLYMERS; SMALL ANGLE X RAY SCATTERING (SAXS);

BLOCK COPOLYMERS;

EID: 0035250050     PISSN: 00249297     EISSN: None     Source Type: Journal    
DOI: 10.1021/ma001127b     Document Type: Article

References (43)

1. Noshay, A.; McGrath, J. E. In Block Copolymers: Overview and Critical Survey; Academic Press: New York, 1977; Chapter 3.
2. Helfand, E.; Wasserman, Z. R. In Development in Block Copolymers; Goodman, J., Ed.; Applied Science: New York, 1982; Vol. 1.
3. Gallot, B. Adv. Polym. Sci. 1978, 29, 85.
4. Gervais, M.; Gallot, B. Polymer 1981, 22, 1124.
5. Gervais, M.; Gallot, B. Makromol. Chem. 1973, 171, 157; 1973, 174, 193; 1977, 178, 1577; 1977, 178, 2071; 1979, 180, 2041.
6. Gervais, M.; Gallot, B. Makromol. Chem. 1973, 171, 157; 1973, 174, 193; 1977, 178, 1577; 1977, 178, 2071; 1979, 180, 2041.
7. Gervais, M.; Gallot, B. Makromol. Chem. 1973, 171, 157; 1973, 174, 193; 1977, 178, 1577; 1977, 178, 2071; 1979, 180, 2041.
8. Gervais, M.; Gallot, B. Makromol. Chem. 1973, 171, 157; 1973, 174, 193; 1977, 178, 1577; 1977, 178, 2071; 1979, 180, 2041.
9. Gervais, M.; Gallot, B. Makromol. Chem. 1973, 171, 157; 1973, 174, 193; 1977, 178, 1577; 1977, 178, 2071; 1979, 180, 2041.
10. DiMarzio, E. A.; Guttman, C. M.; Hoffman, J. D. Macromolecules 1980, 13, 1194.
11. Floudas, G.; Tsitsilianis, C. Macromolecules 1997, 30, 4381.
12. VanderHart, D. L.; Manley, R. S. J.; Barnes, J. D. Macromolecules 1994, 27, 2826.
13. Jack, K. S.; Natansohn, A.; Wang, J.; Favis, B. D.; Cigana, P. Chem. Mater. 1998, 10, 1031.
14. White, J. L.; Brant, P. Macromolecules 1998, 31, 5424.
15. Schmidt-Rohr, K.; Clauss, J.; Blümich, B.; Spiess, H. W. Magn. Reson. Chem. 1990, 28, S3.
16. Cai, W. Z.; Schmidt-Rohr. K.; Egger, N.; Gerharz, B.; Spiess, H. W. Polymer 1993, 34, 267.
17. Cho, G.; Natansohn, A.; Ho, T.; Wynne, K. J. Macromolecules 1996, 29, 2563.
18. Schmidt-Rohr, K.; Spiess, H. W. In Multidimensional Solid State NMR and Polymers; Academic Press: London, 1994.
19. Jack, K. S.; Wang, J.; Natansohn, A.; Register, R. A. Macromolecules 1998, 31, 3282.
20. Havens, J. R.; VanderHart, D. L. Macromolecules 1985, 18, 1663.
21. Kimura, T.; Neki, K.; Tamura, N.; Horii, F.; Nakagawa, M.; Odani, H. Polymer 1992, 33, 493.
22. Eckman, R. R.; Henrichs, P. M.; Peacock, A. J. Macromolecules 1997, 30, 2474.
23. Clayden, N. J. Polym. Sci., Part B: Polym. Phys. 1994, 32, 2321.
24. Clauss, J.; Schmidt-Rohr, K.; Spiess, H. W. Acta Polym. 1993, 44, 1.
25. Wang, J.; Jack, K. S.; Natansohn, A. J. Chem. Phys. 1997, 107, 1016.
26. Wang, J. J. Chem. Phys. 1996, 104, 4850.
27. Yu, H.; Wang, J.; Natansohn, A.; Singh, M. A.Macromolecules 1999, 32, 4365.
28. Yu, H.; Natansohn, A.; Singh, M. A.; Plivelíc, T. Macromolecules 1999, 32, 7562.
29. Richardson, M. J.; Savill, N. G. Polymer 1977, 18, 3.
30. Miller, R. L.; Lee, W. A.; Rutherford, R. A. In Polymer Handbook, 2nd ed.; Brandrup, J., Immergut, E. H., Eds.; Wiley-Interscience: New York, 1975; Vol. III.
31. Egger, N.; Schmidt-Rohr, K.; Blümich, B.; Dmmke, W. D.; Stapp, B. J. Appl. Polym. Sci. 1992, 44, 289.
32. Kellermann, G.; Vicentin, F.; Tamura, E.; Rocha, M.; Tolentino, H.; Barbosa, A.; Craievich, A.; Torriani, I. J. Appl. Crystallogr. 1997, 30, 880.
33. Demco, D. E.; Johansson, A.; Tegenfeldt, J. Solid State Nucl. Magn. Reson. 1995, 4, 13.
34. Wilhelm, M.; Lehmann, S.; Jäger, C.; Spiess, H. W. Magn. Reson. Chem. 1994, 32, S3.
35. Spiegel, S.; Schmidt-Rohr, K.; Boeffel, C.; Spiess, H. W. Polymer 1993, 34, 4566.
36. Mellinger, F.; Wilhelm, M.; Spiess, H. W. Macromolecules 1999, 32, 4686.
37. Van Den Bossche, G.; Sobry, R.; Frédéric, F.; Clacens, J.-M.; Gabelica, Z. J. Appl. Crystallogr. 1997, 30, 1065
38. Sakurai, S.; Kawada, H.; Hashimoto, T. Macromolecules 1993, 26, 5796.
39. De Paul, S. M.; Zwanziger, J. W.; Ulrich, R.; Wiesner, U.; Spiess, H. W. J. Am. Chem. Soc. 1999, 121, 5727.
40. Feigin, L. A.; Svergun, D. I. In Structure Analysis by Small-Angle X-ray and Neutron Scattering; Plenum Press: New York, 1987.
41. Sauer, B. B.; Hsiao, B. S. Polymer 1995, 36, 2553.
42. Sakurai, S.; Okamoto, S.; Kawamura, T.; Hashimoto, T. J. Appl. Crystallogr. 1991, 24, 679.
43. Glatter, O.; Kratky, O. In Small-Angle X-ray Scattering; Academic Press: London, 1982.