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85153001740
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note
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6a: Anal. found C 42.58, H 4.84, N 4.63, Cl 26.12, V 8.60, S 2.30. Based on nitrogen analysis 4.63 ≈ 2 N: MW = 605; stoichiometry: 21.4 C; 29.0 H; 4.5 Cl; 1.0 V; 0.4 S. Based on residual mass: 4.1 O. 6c: Anal. found C 46.05, H 5.81, N 3.80; Cl, 26.97. Based on nitrogen analysis 3.80 ≈ 2 N: MW = 737; stoichiometry: 28.3 C; 42.5 H; 5.6 Cl. 6d. Anal. found C 38.03, H 3.86, N 4.43, Cl 34.29. Based on nitrogen analysis 4.43 ≈ 2 N: MW = 632; stoichiometry: 20.0 C; 24.2 H; 6.1 Cl. 6e: Anal, found C 56.34, H 4.83, N 12.33; Cl, 13.51. Based on nitrogen analysis 12.33 ≈ 6 N: MW = 682; stoichiometry: 32.0 C; 32.6 H; 2.6 Cl. 6f: Anal. found C 43.98, H 5.02, N 4.17; Cl, 23.49; V, 8.43, S 3.51. Based on nitrogen analysis 4.17 ≈ 2 N: MW = 672; stoichiometry: 24.6 C; 33.7 H; 4.5 Cl; 1.1 V; 0.7 S. Based on residual mass: 4.8 O.
-
-
-
-
14
-
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85152983467
-
-
note
-
The residue in the case of 7a contained three equivalents of chlorine. Anal. found C 47.44, H 5.38, N 5.90, Cl 22.35. Based on nitrogen analysis 5.90 ≈ 2 N: MW = 475; stoichiometry: 18.8 C; 25.3 H; 3.0 Cl.
-
-
-
-
15
-
-
85153009239
-
-
note
-
7c: Anal. found C 53.85, H 7.01, N 4.67; Cl, 20.59. Based on nitrogen analysis 4.67 ≈ 2 N: MW = 600; stoichiometry: 26.9 C; 41.7 H; 3.5 Cl.
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22
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