Solid-state 19F MAS, 19F CRAMPS, and 19F → 13C CP/MAS NMR study of an amorphous perfluoropolymer

Macromolecules

Volumn 34, Issue 1, 2001, Pages 66-75

  Ando, Shinji ^a   Harris, Robin K ^b   Hirschinger, Jérôme ^c   Reinsberg, Stefan A ^b,e   Scheler, Ulrich ^d  

^a TOKYO INSTITUTE OF TECHNOLOGY   (Japan)

^b DURHAM UNIVERSITY   (United Kingdom)

^c UNIVERSITÉ DE STRASBOURG   (France)

^d LEIBNIZ INSTITUTE OF POLYMER RESEARCH DRESDEN   (Germany)

^e MAX PLANCK INSTITUTE FOR POLYMER RESEARCH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

HETERONUCLEAR POLARIZATION TRANSFER; HETERORING; MAGIC ANGLE SPINNING; MAGNETIC INEQUIVALENCE; PERFLUOROPOLYMER; QUANTUM MECHANICAL MASTER EQUATION; SPINNING SIDEBANDS;

AMORPHOUS MATERIALS; CONFORMATIONS; DIFFUSION; EQUATIONS OF MOTION; MOLECULAR STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLARIZATION; PROBABILITY DENSITY FUNCTION; QUANTUM THEORY; THERMAL EFFECTS;

FLUORINE CONTAINING POLYMERS;

EID: 0035130009     PISSN: 00249297     EISSN: None     Source Type: Journal    
DOI: 10.1021/ma000275z     Document Type: Article

References (38)

1. Nakamura, M. US Patent 4,897,457, 1990.
2. Nakamura, M.; Kawasaki, T.; Unoki, M.; Oharu, K.; Sugiyama, N.; Kojima, G. Progress in Pacific Polymer Science; Springer-Verlag: Berlin, 1991; p 369.
3. Resnick, P. R. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1990, 31, 312.
4. Buck W. H.; Resnick, P. R. Electrochemical Society, Spring Meeting, Honolulu; Ext. Abs. 1993, 93-1, 548.
5. Sugiyama, N. Polym. Prepr. (Am. Chem. Soc., Div. Polym. Chem.) 1998, 39, 1028.
6. Dec, S. F.; Wind, R. A.; Maciel, G. E.; Anthonio, F. E. J. Magn. Reson. 1986, 70, 355.
7. Dec, S. F.; Wind, R. A.; Maciel, G. E. Macromolecules 1987, 20, 2754.
8. Harris, R. K.; Jackson, P. Chem. Rev. 1991, 91, 1427.
9. Holstein, P.; Scheler, U.; Harris, R. K. Magn. Reson. Chem. 1997, 35, 647.
10. Holstein, P.; Scheler, U.; Harris, R. K. Polymer 1998, 39, 4937.
11. Holstein, P.; Harris, R. K.; Say, B. J. Solid State Nucl. Magn. Reson. 1997, 8, 201.
12. Scheler, U.; Harris, R. K. Chem. Phys. Lett. 1996, 262, 137.
13. Scheler, U.; Harris, R. K. Solid State Nucl. Magn. Reson. 1996, 7, 11.
14. Scheler, U. Solid State Nucl. Magn. Reson. 1998, 12, 9.
15. Isbester, P. K.; Kestner, T. A.; Munson, E. J. Macromolecules 1998, 31, 8192.
16. Ando, S.; Harris, R. K.; Reinsberg, S. A. J. Magn. Reson. 1999, 141, 91.
17. Ando, S.; Harris, R. K.; Monti, G. A.; Reinsberg, S. A. Magn. Reson. Chem. 1999, 37, 709.
18. Legeay, G.; Coudreuse, A.; Legeais, J.; Werner, L.; Bulou, A.; Buzare, J.; Emery, J.; Silly, G. Eur. Polym. J. 1998, 34 1457.
19. Katoh, E.; Sugimoto, H.; Kita, Y.; Ando, I. J. Mol. Struct. 1995, 355, 21.
20. Katoh, E.; Sugisawa, H.; Oshima, A.; Tabata, Y.; Seguchi, T.; Yamazazki, T. Radiat. Phys. Chem. 1998, 54, 165.
21. Aosaki, K. J. Soc. Hybrid Microelectron. (Jpn.) 1996, 12, 2.
22. Zhang, S.; Meier, B. H.; Ernst, R. R. Solid State Nucl. Magn. Reson. 1992, 1, 313.
23. Frisch, M. J.; Trucks, G. W.; Schlegel, H. B.; Gill, P. M. W.; Johnson, B. G.; Robb, M. A.; Cheeseman, J. R.; Keith, T.; Petersson, G. A.; Montgomery, J. A.; Raghavachari, K.; Al-Laham, M. A.; Zakrzewski, V. G.; Ortiz, J. V.; Foresman, J. B.; Cioslowski, J.; Stefanov, B. B.; Nanayakkara, A.; Challacombe, M.; Peng, C. Y.; Ayala, P. Y.; Chen, W.; Wong, M. W.; Andres, J. L.; Replogle, E. S.; Gomperts, R.; Martin, R. L.; Fox, D. J.; Binkley, J. S.; Defrees, D. J.; Baker, J.; Stewart, J. P.; Head-Gordon, M.; Gonzalez, C.; Pople, J. A. Gaussian 94, revision E.2; Gaussian, Inc.: Pittsburgh, PA, 1995.
24. Wolinski, K.; Hinton, J. F.; Pulay, P. J. Am. Chem. Soc. 1990, 112, 8251.
25. Cheeseman, J. R.; Trucks, G. W.; Keith, T. A.; Frisch, M. J. J. Chem. Phys. 1996, 104, 5797.
26. Harris, R. K.; Jackson, P.; Nesbett, G. J. J. Magn. Reson. 1989, 85, 294.
27. Grievson, B. Ph.D. Thesis, University of Durham, 1983.
28. Adcock, W.; Lünsmann, D.; Peralta, J. E.; Contreras, R. H. Magn. Reson. Chem. 1999, 37, 167.
29. The "d" in 6-31G(d,p) indicates that d-type polarization functions are located on atoms except for hydrogen, and the "p" indicates that p-type functions are on hydrogens. Hence, 6-31G(d,p) and 6-31G(d) are the same basis sets for perfluorinated organic molecules because of the absence of hydrogens.
30. Homer, J.; Thomas, L. F. Trans. Faraday Soc. 1963, 59, 2431; 1966, 62, 2980.
31. Homer, J.; Thomas, L. F. Trans. Faraday Soc. 1963, 59, 2431; 1966, 62, 2980.
32. Homer, J.; Thomas, L. F. Proc. Chem. Soc. 1961, 139.
33. Ando, S.; Harris, R. K.; Holstein, P.; Reinsberg, S. A., to be submitted.
34. Reinheimer, P.; Hirschinger, J.; Gilard, P.; Goetz, N. Magn. Reson. Chem. 1997, 35, 757.
35. Müller, L.; Kumar, A.; Baumann, T.; Ernst, R. R. Phys. Rev. Lett. 1974, 32, 1402.
36. Hirschinger, J.; Hervé, M. Solid State Nucl. Magn. Reson. 1994, 3, 121.
37. Reinsberg, S. A. M.Sc. Thesis, University of Durham, 1998.
38. Reinsberg, S. A.; Ando, S.; Harris, R. K. Polymer 2000, 41, 3729.