The development of reference materials for paralytic shellfish poisoning toxins in lyophilized mussel. II: Certification study

Food Additives and Contaminants

Volumn 18, Issue 9, 2001, Pages 810-824

  Van Den Top, H J ^a   Boenke, A ^b   Burdaspal, P A ^c   Bustos, J ^c   Van Egmond, H P ^a   Legarda, T ^c   Mesego, A ^d   Mourino A ^d   Paulsch, W E ^a   Salgado, C ^d  

^a NATIONAL INSTITUTE FOR PUBLIC HEALTH AND THE ENVIRONMENT   (Netherlands)

^b EUROPEAN COMMISSION   (Belgium)

^c INSTITUTO DE SALUD CARLOS III   (Spain)

^d UNIVERSITY OF SANTIAGO DE COMPOSTELA   (Spain)

Author keywords

Certification; Dc saxitoxin; Interlaboratory; Material; Paralytic shellfish poison; Phycotoxin; PSP; Reference; Regulatory level; Saxitoxin; Shellfish; Standardization

Indexed keywords

HYDROCHLORIC ACID; MARINE TOXIN; POISON; SAXITOXIN;

ACCURACY; ANALYTIC METHOD; ANIMAL EXPERIMENT; ANIMAL TISSUE; ARTICLE; CERTIFICATION; CHEMICAL ANALYSIS; CHEMICAL COMPOSITION; CHEMICAL STRUCTURE; CONTROLLED STUDY; FRACTIONATION; FREEZE DRYING; INTOXICATION; LABORATORY TEST; MASS; MATERIALS TESTING; METHODOLOGY; MUSSEL; NONHUMAN; PARALYSIS; PRIORITY JOURNAL; QUALITY CONTROL; REFERENCE VALUE; REHYDRATION; SHELLFISH; TOXICITY TESTING; TOXIN ANALYSIS;

ANIMALIA;

EID: 0034845313     PISSN: 0265203X     EISSN: 14645122     Source Type: Journal    
DOI: 10.1080/02652030120735     Document Type: Article

References (20)

1. Association Of Official Analytical Chemists, 1990, Fish and Other Marine Products, AOAC Official Method 959.08.
2. Paralytic Shellhsh Poison, Biological Method, Final Action. Official Methods of Analysis of the Association of Official Analytical Chemists, 15th edn, edited by K. Helrich (Arlington, Virginia, USA: AOAC) pp. 881-882.
3. Councel Of The European Communities, 1986, Council Directive of 24 November 1986 on the approximation of laws, regulations and administrative provisions of the Member States regarding the protection of animals used for experimental and other scien-tihc purposes (86/609/EEC). Official Journal of the European Communities, L 358, 1-28.
4. Councel Of The European Communities, 1991, Council Directive of 15 July 1991 laying down the health conditions for the production and the placing on the market of live bivalve molluscs (91/ 492/EEC). Official Journal of the European Communities, L 268, 1-14.
5. European Commission, Standards, Measurements And Testing Programme, 1994, Guidelines for the Production and Certihcation of BCR Reference Materials (RMs). Document Doc. BCR/48/93, version 15th December 1994.
6. Franco, J. M., and Fernandez, P., 1993, Separation of paralytic shellhsh toxins by reversed phase high performance liquid chromatography, with postcolumn reaction and fluorimetric detection. Chromatographia, 35, 613-620.
7. Hall, S., 1982, Toxins and toxicity of Protogonyaulax (Alexandrium) from the Northeast Pacihc, PhD Thesis, University of Alaska, Fairbanks, Alaska, pp.1-196.
8. Krogh, P., 1988, Report of the Scientific Veterinary Committee (Section Public Health) on Paralytic Shellfish Poison. Document VII6492l88-EN-Rev.1 (Brussels: Commission of the European Communities DG VI/8/II.B).
9. Lawrence, J. F., And Menard, C., 1991, Liquid chromatographic determination of paralytic shellhsh poisons in shellhsh after prechromatographic oxidation. Journal of the Association of Official Analytical Chemists, 74, 1006-1012.
10. Lawrence, J.F., Menard, C., and Cleroux, C., 1995, Evaluation of prechromatographic oxidation for liquid chromatographic detection of Paralytic Shellhsh Poisons in shellhsh. Journal of the Association of Official Analytical Chemists International, 78, 514-520.
11. Luckas, B., Tfflelert, G., and Peters, K., 1990, The problem of the selective determination of PSP toxins in mussels. Zeitschrift fur Lebensmitteluntersuchung und Forschung, 190, 491-495.
12. Mesego, A., Sanvicente, F., Salgado, C., and Mourino, A., 1996, PSP-Biotoxins: purihcation of saxitoxin and procurement of the interconversion index of saxitoxin. Poster Presentation (PO-42) at the 1st International Symposium on New Horizons of Organic Chemistry in Biomedicine, September 1996, Santiago de Compostela, Spain.
13. Oshima, Y., Sugino, K., and Yasumoto, T., 1989, Latest advances in HPLC analysis of Paralytic Shellhsh Toxins. Mycotoxins and Phycotoxins. A collection of invited papers at the Seventh International IUPAC Symposium on Mycotoxins and Phycotoxins, Tokyo, Japan, 16-19 August 1988, edited by S. Natori, K. Hashimoto and Y. Ueno (Amsterdam: Elsevier Science Publishers BV), pp. 319-326.
14. Thielert, G., Kaiser, L., and Luckas, B., 1991, HPLC determination of PSP toxins. Proceedings of Symposium on Marine Biotoxins, Paris, France, 30-31 January 1991, edited by J.M. Fremy (Maisons-Alfort: Centre National d’Etudes Veterinaires), pp. 121-125.
15. Van Den Top, H. J., Boenke, A., Burdaspal, P. A., Bustos, J., Van Egmond, H. P., Legarda, T., Mesego, A., Moureno, A., Paulsch, W. E., And Salgado, C., 2000, The development of reference materials for paralytic shellhsh poisoning toxins in lyophilized mussel. I: Interlaboratory studies of methods of analysis. Food Additives and Contaminant s, 17, 419-433.
16. Van Egmond, H.P., Speijers, G.J.A., and Van Den Top, H.J., 1992, Current situation on worldwide regulations for marine phyco-toxins. Journal of Natural Toxins, 1, 47-85.
17. Van Egmond, H.P., Aune, T., Lassus, P., Speijers, G.J.A., and Waldock, M., 1993, Paralytic and diarrhoeic shellfish poisons: occurrence in Europe, toxicity, analysis and regulation. Journal of Natural Toxins, 2, 41-83.
18. Van Egmond, H. P., Van Den Top, H. J., Paulsch, W. E., Goenaga, X., and Vieytes, R., 1994, Paralytic Shellfish Poison reference materials: an intercomparison of methods for the determination of saxitoxin. Food Additives and Contaminants, 11, 39-56.
19. Van Egmond, H. P., Mourino, A., Burdaspal, P. A., Bustos, J., Legarda, T., Mesego, A., Paulsch, W. E., Salgado, C., Van Den Top, H. J., and Boenke, A., 1998, The certification of the mass fractions of saxitoxin and dc-saxitoxin in two mussel reference materials (CRMs 542 & 543) including the identification of other PSP-toxins, and a spiking procedure based on an enrichment solution (RM 663) with a certified mass concentration of saxitoxin. Report EUR 18318 EN, Luxembourg, Commission of the European Communities, Directorate-General Science, Research and Development.
20. Vantrijp, J. M. P., and Roos, A. H., 1991, Model for the calculation of calibration curves. RIKILT-Report 91.02, January 1991 (Wageningen, The Netherlands).