Two new iodine-capped carbon rods [13]

Journal of the American Chemical Society

Volumn 122, Issue 38, 2000, Pages 9320-9321

  Gao, Kunxiu ^a,b   Goroff, Nancy S ^a  

^a STONY BROOK UNIVERSITY   (United States)

^b WAYNE STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ACID; ALKYNE DERIVATIVE; CARBON 13; IODINE DERIVATIVE; LEWIS ACID; TRIPHENYLPHOSPHINE; UNCLASSIFIED DRUG;

CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL REACTION; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; LETTER; MOLECULAR INTERACTION; REACTION ANALYSIS; STRUCTURE ANALYSIS; SYNTHESIS; X RAY DIFFRACTION;

EID: 0034721425     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja001722t     Document Type: Letter

References (29)

1. Baeyer, A. Chem. Ber. 1885, 18, 2269-2281.
2. (a) Heibronner, E.; Hornung, V.; Maier, J. P.; Kloster-Jensen, E. J. Am. Chem. Soc. 1974, 96, 4252-62.
3. (b) Klaboe, P.; Kloster-Jensen, E.; Bjarnov, E.; Christensen, D. H.; Nielsen, O. F. Spectrochim. Acta. Part A 1975, 31A, 931-43.
4. (a) Peregudova, S. M.; Denisovich, L. I.; Ustynyuk, N. A.; Leonteva, L. I.; Vinogradova, V. N.; Filatova, T. V. Russ. Chem. Bull. 1995, 44, 1973-1975.
5. (b) Hlavaty, J.; Kavan, L. Angew. Makromol. Chem. 1998, 254, 75-78.
6. (c) Hlavaty, J.; Kavan, L. Angew. Makromol. Chem. 1998, 259, 83-85.
7. (d) Kijima, M.; Sakai, Y.; Shirakawa, H. Synth. Met. 1995, 71, 1837-1840.
8. (a) Uji, S.; Terakura, C.; Terashima, T.; Aoki, H.; Yamamoto, H. M.; Yamaura, J.; Kato, R. Synth. Met. 1999, 103, 1978-1978.
9. (b) Yamamoto, H. M.; Yamaura, J. I.; Kato, R. Synth. Met. 1999, 102, 1448-1451.
10. (c) Yamamoto, H. M.; Yamaura, J.; Kato, R. Synth. Met. 1999, 102, 1515-1516.
11. (d) Yamamoto, H. M.; Yamaura, J. I.; Kato, R. J. Am. Chem. Soc. 1998, 120, 5905-5913.
12. (e) Yamamoto, H. M.; Yamaura, J. I.; Kato, R. J. Mater. Chem. 1998, 8, 15-16.
13. (a) Eastmond, R.; Walton, D. R. M. Tetrahedron 1972, 28, 4591-4599.
14. (b) Eastmond, R.; Johnson, T. R.; Walton, D. R. M. Tetrahedron 1972, 28, 4601-4616.
15. Cadiot, P.; Chodkiewicz, W. In Chemistry of Acetylenes; Viehe, H.-G., Ed.; Marcel Dekker: New York, 1969; Chapter 9.
16. Hay, A. S. J. Org. Chem. 1962, 27, 3320.
17. 2: (a) Grösser, T.; Hirsch, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1340-1342.
18. 2: (a) Grösser, T.; Hirsch, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1340-1342. (b) Schermann, G.; Grosser, T.; Hampel, F.; Hirsch, A. Chem. Eur. J. 1997, 3, 1105-1112. Schermann, G.; Vostrowsky, O.; Hirsch, A. Eur. J. Org. Chem. 1999, 2491-2500.
19. 2: (a) Grösser, T.; Hirsch, A. Angew. Chem., Int. Ed. Engl. 1993, 32, 1340-1342. (b) Schermann, G.; Grosser, T.; Hampel, F.; Hirsch, A. Chem. Eur. J. 1997, 3, 1105-1112. Schermann, G.; Vostrowsky, O.; Hirsch, A. Eur. J. Org. Chem. 1999, 2491-2500.
20. Nishikawa, T.; Shibuya, S.; Hosokawa, S.; Isobe, M. Synlett 1994, 485-486. For a recent review of halogenated alkynes, see: Hopf, H.; Witulski, B. In Modern Acetylene Chemistry; Stang, P. J., Diederich, F., Eds.; VCH: Weinheim, 1995; pp 33-66.
21. Nishikawa, T.; Shibuya, S.; Hosokawa, S.; Isobe, M. Synlett 1994, 485- 486. For a recent review of halogenated alkynes, see: Hopf, H.; Witulski, B. In Modern Acetylene Chemistry; Stang, P. J., Diederich, F., Eds.; VCH: Weinheim, 1995; pp 33-66.
22. Goroff, N. S. Acc. Chem. Res. 1996, 29, 77-83.
23. 13C NMR spectrum at 75 MHz in the presence of the relaxation agent chromium (III) acetylacetonate. Integration of the three peaks observed, at 88.0, 87.8, and 62.2 ppm, gave relative intensities of 1:1:2.
24. (a) Rubin, Y.; Lin, S. S.; Knobler, C. B.; Anthony, J.; Boldi, A. M.; Diederich, F. J. Am. Chem. Soc. 1991, 113, 6943-9.
25. (b) Walton, D. R. M.; Waugh, F. J. Organomet. Chem. 1972, 37, 45-56.
26. (c) Weng, W.; Bartik, T.; Brady, M.; Bartik, B.; Ramsden, J. A.; Arif, A. M.; Gladysz, J. A. J. Am. Chem. Soc. 1995, 117, 11922-11931.
27. Etter, M. C.; Baures, P. W. J. Am. Chem. Soc. 1988, 110, 639-640.
28. w = 5.3%, R = 5.7% for 253 variables and 1342 unique observations with (I > 3a).
29. Stang, P. J. In Modern Acetylene Chemistry; Stang, P. J., Diederich, F., Eds.; VCH: Weinheim, 1995; pp 67-98.