Optimization of the high-performance liquid chromatographic separation of a complex mixture containing urinary steroids, boldenone and bolasterone: Application to urine samples

Journal of Chromatography B: Biomedical Sciences and Applications

Volumn 742, Issue 1, 2000, Pages 47-57

  Gonzalo Lumbreras, R ^a   Izquierdo Hornillos, R ^a  

^a UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

Author keywords

Bolasterone; Boldenone; Urinary steroids

Indexed keywords

ANABOLIC AGENT; BOLASTERONE; BOLDENONE; CORTICOSTERONE; CORTISONE; DEOXYCORTICOSTERONE; EPITESTOSTERONE; HYDROCORTISONE; HYDROXYPROGESTERONE; KETOTESTOSTERONE; METHYLTESTOSTERONE; PRASTERONE; TESTOSTERONE; TESTOSTERONE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CALIBRATION; DRUG DETERMINATION; DRUG EXCRETION; EXTRACTION; HYDROLYSIS; PRIORITY JOURNAL; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; URINALYSIS;

ADRENAL CORTEX HORMONES; ANABOLIC AGENTS; CALIBRATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; HUMANS; REPRODUCIBILITY OF RESULTS; SALTS; SENSITIVITY AND SPECIFICITY; TEMPERATURE; TESTOSTERONE;

EID: 0034717096     PISSN: 13872273     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0378-4347(00)00084-0     Document Type: Article

References (26)

1. Kaplan L.A., Pesce A.J. Clinical Chemistry. 1989;C.V. Mosby, St Louis, MO.
2. List of Doping Classes and Methods. International Olympic Committee Medical Commission, Laussanne, 1995.
3. Prohibited Distribution of Anabolic Steroids, in: Pub. L. No 100-690, 102 Stat 4181, US Government, Prohibited Distribution USC section 323 a, Washington DC, 1988.
4. Venturelli E., Cavalleri A., Secreto G. J. Chromatogr. B. 671:1995;363.
5. Garle M., Ocka R., Palonek E., Björkhem I. J. Chromatogr. B. 687:1996;55.
6. Carlstom K., Palonek E., Garle M., Oftebro H., Stanghelle J., Björkhem I. Clin. Chem. 38:1992;1779.
7. Dehennin L., Matsumoto A.M. J. Steroid Biochem. 44:1993;179.
8. van Ginkel L.A., Jansen E.H.J.M., Stephany R.W., Zoontjes P.W., Schwillens P.L.W.J., van Rossum H.J., Visser T. J. Chromatogr. 624:1992;389.
9. Le Bizec B., Montrade M.P., Monteau F., Andre F. Anal. Chim. Acta. 275:1993;123.
10. Ayotte C., Groudreault D., Charlebois A. J. Chromatogr. B. 687:1996;3.
11. Masse R., Ayotte C., Dugal R. J. Chromatogr. 489:1989;24.
12. Schänzer W., Donike M. Anal. Chim. Acta. 275:1993;23.
13. Aguilera R., Becchi M., Casabianca H., Hatton C.K., Catlin D.H., Starcevic B., Pope H.G. Jr. J. Mass Spectrom. 31:1996;169.
14. Amin M., Harrinton K., von Wandruszka R. Anal. Chem. 65:1993;2346.
15. Walker V.R., Dombi G.W., Gutai J.P., Wade D.D., Swartz K.H., Liu H., Schroeder R.R. Ana. Anal. Biochem. 234:1996;194.
16. Komatsu F., Morioka M., Fujita Y., Sugahara K., Kodama H. J. Mass. Spectrom. 30:1995;698.
17. De Beer J.O. J. Chromatogr. 489:1989;139.
18. Santos-Montes A., Gasco-Lopez A.I., Izquierdo-Hornillos R. J. Chromatogr. B. 620:1993;15.
19. Snyder L.R., Glajch J.L., Kirkland J.L. Practical HPLC Method Development. 2nd Edition :1997;Wiley, New York.
20. Santos-Montes A., Gonzalo-Lumbreras R., Gasco-Lopez A.I., Izquierdo-Hornillos R. J. Chromatogr. B. 652:1994;83.
21. Santos-Montes A., Gonzalo-Lumbreras R., Gasco-Lopez A.I., Izquierdo-Hornillos R. J. Chromatogr. B. 657:1994;248.
22. Khaledi M.G., Strasters J.K., Rodgers A.H., Breyer E.D. Anal. Chem. 62:1990;130.
23. Sachs L. Applied Statistics. A Handbook of Technique. 1978;Springer Verlag, Berlin.
24. Skoog D.A., Leary J.J. Principles of Instrumental Analysis. 4th Edition :1993;Saunders College Publishing, Philadelphia. Chs. 1 and 4.
25. Logan B.K. Anal. Chim. Acta. 288:1994;111.
26. Santos-Montes A., Gonzalo-Lumbreras R., Izquierdo-Hornillos R. J. Chromatogr. B. 673:1995;27.