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Tetrahedron Asymmetry

Volumn 11, Issue 18, 2000, Pages 3665-3669

Efficient synthesis of (S)-(-)- and (R)-(+)-enantiomers of 15-deoxyspergualin (15-DSG)

(2) Wang, Xuebao a Thottathil, John a

a BRISTOL MYERS SQUIBB (United States)

Author keywords

[No Author keywords available]

Indexed keywords

15 DEOXYSPERGUALIN;

ARTICLE; CRYSTALLIZATION; DIASTEREOISOMER; DRUG SYNTHESIS; ENANTIOMER; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; RACEMIC MIXTURE; REACTION ANALYSIS;

EID: 0034703150 PISSN: 09574166 EISSN: None Source Type: Journal
DOI: 10.1016/S0957-4166(00)00350-5 Document Type: Article

Times cited : (7)

References (15)

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9
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- Recently, a similar approach was described by: Durand, P.; Richard, P.; Renaut, P. J. Org. Chem. 1998, 63, 9723, which prompted us to disclose our results. Our work was completed in 1993 and patented: Wang, X.; Thottathil, J. K. Eur. Pat. Appl. EP 765,866, Apr. 2, 1997.

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13
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- note

14
- 0007409875
- 2 per injection, flow rate: 350 mL/min, detection: 254 nm UV, fractions: 500 ml each, collected: 8-9 fractions for the first diastereoisomer 10a and 14-15 for the second diastereoisomer 10b. The contaminated fractions 10-11 for 10a and 12-13 for 10b (analyzed by TLC) were combined, evaporated and re-injected.

15
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- 3a

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