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18
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84991430063
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2O. A satisfactory spectroscopic characterisation was achieved
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2O. A satisfactory spectroscopic characterisation was achieved.
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20
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0029975056
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22
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84991422822
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Although the stereochemistry at the anomeric centre is not fixed, the adducts 10, 11, 12 and 14 are present in aqueous solution as a single anomer, most likely the α-anomer, as reported in Scheme 2
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Although the stereochemistry at the anomeric centre is not fixed, the adducts 10, 11, 12 and 14 are present in aqueous solution as a single anomer, most likely the α-anomer, as reported in Scheme 2
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23
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0001676496
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Bednarski, M. D.; Simon, E. S.; Bischofberger, N.; Fessner, W. D.; Kim, M. J.; Lees, W.; Saito, T.; Waldmann, H.; Whitesides, G. M. J. Am. Chem. Soc. 1989, 111, 627-635.
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Bednarski, M.D.1
Simon, E.S.2
Bischofberger, N.3
Fessner, W.D.4
Kim, M.J.5
Lees, W.6
Saito, T.7
Waldmann, H.8
Whitesides, G.M.9
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24
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84991420387
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Approximately the same results (yield and diastereomeric ratio) were obtained by using acid or alkaline phosphatase
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Approximately the same results (yield and diastereomeric ratio) were obtained by using acid or alkaline phosphatase.
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25
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84991428674
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note
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24 As we did not isolate the intermediate monophosphate, it is not possible to decide definitively in which step such hydrolysis takes place.
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