Precipitation of solvent-free C60(CO2)0.95 from Conventional solvents: A new antisolvent approach to controlled crystal growth using supercritical carbon dioxide

Journal of the American Chemical Society

Volumn 122, Issue 11, 2000, Pages 2480-2488

  Field, Christian N ^a   Hamley, Paul A ^a   Webster, Jeremy M ^a   Gregory, Duncan H ^a   Titman, Jeremy J ^a   Poliakoff, Martyn ^a  

^a UNIVERSITY OF NOTTINGHAM   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

CARBON DIOXIDE; ORGANIC SOLVENT;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; PARTICLE SIZE; PRECIPITATION; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; X RAY DIFFRACTION;

EID: 0034701220     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja9919478     Document Type: Article

References (58)

1. Holleman, I.; von Heldern, G.; van Bentum, P. J. M.; Engeln, R.; Nachtegaal, G. H.; Kentgens, A. P. M.; Meier, B. H.; van der Avoird, A.; Meijer, G. Phys. Rev. Lett. 1997, 79, 1138-1141.
2. Holleman, I.; von Heldern, G.; van der Avoird, A.; Meijer, G. Phys. Rev. Lett. 1998, 80, 4899-4902.
3. van Smaalen, S.; Dinnebier, R. E.; Schnelle, W.; Holleman, I.; von Helden, G.; Meijer, G. Europhys. Lett. 1998, 43, 302-307.
4. van Smaalen, S.; Dinnibier, R.; Holleman, I.; von Helden, G.; Meijer, G. Phys. Rev. B 1998, 57, 6321-6324.
5. Holleman, I.; Robyr, P.; Kentgens, A. P. M.; Meier, B. H.; Meijer, G. J. Am. Chem. Soc. 1999, 121, 199-207.
6. Gadd, G. E.; James, M.; Moricca, S.; Cassidy, D.; Evans, P. J.; Collins, B.; Armstrong, R. S. J. Phys. Chem. Solids 1998, 59, 1383-1391.
7. James, M.; Kennedy, S. J.; Elcombe, M. M.; Gadd, G. E. Phys. Rev. B 1998, 58, 14780-14785.
8. Nagano, Y.; Kiyobayashi, T.; Nitta, T. Chem. Phys. Lett. 1994, 217, 186-190.
9. Gadd, G. E.; Moricca, S.; Kennedy, S. J.; Elcombe, M. M.; Evans, P. J.; Blackford, M.; Cassidy, D.; Howard, C. J.; Prasad, P.; Hanna, J. V.; Burchwood, A.; Levy, D. J. Phys. Chem. Solids 1997, 58, 1823-1832.
10. Morosin, B.; Jorgensen, J. D.; Short, S.; Kwei, G. H.; Schirber, J. E. Phys. Rev. B 1996, 53, 1675-1678.
11. Morosin, B.; Assink, R. A.; Dunn, R. G.; Massis, T. M.; Schirber, J. E.; Kwei, G. H. Phys. Rev. B 1997, 56, 13611-13614.
12. 2 in their sample preparation (Johnson, R. D.; Yannoni, C. S.; Dorn, H. C.; Salem, J. R.; Bethune, D. S. Science 1992, 255, 1235-1238).
13. Kratchmer, W.; Lamb, L. D.; Fostiropoulos, K.; Huffman, D. R. Nature 1990, 347, 354-358.
14. Siam, S.; Kuo, K. C.; Stalling, D. L. Sep. Sci. Technol. 1993, 28, 1509-1525.
15. Dixon, D. J.; Johnston, K. P. J. Appl. Polym. Sci. 1993, 50, 1929.
16. Mawson, S.; Yates, M. Z.; O'Neill, M. L.; Johnston, K. P. Langmuir 1997, 13, 1519.
17. Mawson, S.; Johnston, K. P.; Betts, D. E.; McClain, J. B.; DeSimone, J. M. Macromolecules 1997, 30, 71.
18. Mawson, S.; Kanakia, S.; Johnston, K. P. Polymer 1997, 38, 2957.
19. Palakodaty, S.; York, P.; Hana, M.; Pritchard, J. Proc. 5th Meeting on Supercritical Fluids, Nice, France 1998, T1, 275.
20. Gallagher, P. M.; Coffey, M. P.; Krukonis, V. J.; Hillstrom, W. W. J. Supercrit. Fluids 1992, 5, 130.
21. Yeo, S.-D.; Lim, G.-B.; Debendetti, P. G.; Bernstein, H. Biotechnol. Bioeng. 1992, 41, 341.
22. Randolph, T. W.; Randolph, A. D.; Mebes, M.; Yeung, S. Biotechnol. Prog. 1993, 9, 429.
23. Reverchon, E.; Porta, G. D.; Trolio, A. D. Proc. 4th Conf. on Supercritical Fluids and Their Applications, Capri, Italy 1997, 335.
24. Reverchon, E.; Barba, A. A.; Porta, G. D.; Ciambelli, P.; Sannino, D. Proc. 4th Conf. on Supercritical Fluids and Their Applications, Capri, Italy 1997, 385.
25. Bleich, J.; Müller, B. W.; Wassmus, W. Int. J. Pharm. 1993, 97, 111.
26. Bleich, J.; Muller, B. W. Microencapsulation 1996, 13, 131.
27. Da Ros, T.; Prato, M. Chem. Commun. 1999, 663-669.
28. Mawson, S.; Kanakia, S.; Johnston, K. P. J. Appl. Polym. Sci. 1997, 64, 2105-2118.
29. c at a given mixture composition.
30. Peng, D. Y.; Robinson, D. B. Ind. Eng. Chem. Fundam. 1976, 15, 59.
31. Ng, H.-J.; Robinson, D. B. J. Chem. Eng. Data 1978, 23, 325.
32. Heidemann, R. A.; Khalil, A. M. AIChE J. 1980, 26, 769.
33. 2 phase more dense than that of the solvent and so "float" the solvent away.
34. Louer, D.; Louer, M. J. Appl. Crystallogr. 1972, 5, 271.
35. Boultif, A.; Louer, D. J. Appl. Crystallogr. 1991, 24, 987.
36. Reitveld, H. M. J. Appl. Crystallogr. 1969, 2, 65.
37. Wiles, D. B.; Young, R. A. J. Appl. Crystallogr. 1981, 14, 149.
38. Howard, C. J.; Hill, R. J. A. A. E. C. Rep. 1986, No. M112.
39. Darr, J. A.; Poliakoff, M. Chem. Rev. 1999, 99, 495-541.
40. 30 equation of state; mixture parameters were obtained by fitting experimental data from the literature. Calculations were carried out using software (SUPERTRAPP Version 2.01) supplied by NIST (National Institute of Standards and Technology, Gaithersburg, MD 20899).
41. Taylor, R.; Hare, J. P.; Abdul-Sada, A. K.; Kroto, H. W. J. Chem. Soc., Chem. Commun. 1990, 1423-1425.
42. Taylor, R. The Chemistry of Fullerenes; World Scientific: Singapore, 1995.
43. Olthof, E. H. T.; van der Avoird, A.; Wormer, P. E. S. J. Chem. Phys. 1996, 104, 832-847.
44. 2.
45. Tycko, R.; Haddon, R. C.; Dabbagh, G.; Glarum, S. H.; Douglass, D. C.; Mujsce, A. M. J. Phys. Chem. 1991, 95, 518-520.
46. Yannoni, C. S.; Johnston, R. D.; Meijer, G.; Bethune, D. S.; Salem, J. R. J. Phys. Chem. 1991, 95, 9-10.
47. Beeler, A. J.; Orendt, A. M.; Grant, D. M.; Cutts, P. W.; Michl, J.; Zilm, K. W.; Downing, J. W.; Facelli, J. C.; Schindler, M. S.; Kutzelnigg, W. J. Am. Chem. Soc. 1984, 106, 7672-7676.
48. Hwang, S.-J.; Petucci, C.; Raftery, D. J. Am. Chem. Soc. 1998, 120, 4388-4397.
49. Luzzi, D. E.; Fischer, J. E.; Wang, X. Q.; Ricketts-Foot, D. A.; McGhie, A. R.; Romanow, W. J. J. Mater. Res. 1992, 7, 335-340.
50. Werner, H.; Bublak, D.; Göbel, U.; Henschke, B.; Bensch, W.; Schlögl, R. Angew. Chem., Int. Ed. Engl. 1992, 31, 868-870.
51. Fleming, R. M.; Seigrist, T.; Marsh, P. M.; Hessen, B.; Kortan, A. R.; Murphy, D. W.; Haddon, R. C.; Tycko, R.; Dabbagh, G.; Mujsce, A. M.; Kaplan, M. L.; Zahurak, S. M. Mater. Res. Soc. Symp. Proc. 1991, 206, 691.
52. André, D.; Dworkin, A.; Szwarc, H.; Céolin, R.; Agafonov, V.; Fabre, C.; Rassat, A.; Straver, L.; Bernier, P.; Zahab, A. Mol. Phys. 1992, 76, 1311-1317.
53. Chow, P. C.; Jiang, X.; Reiter, G.; Wochner, P.; Moss, S. C.; Axe, J. D.; Hanson, J. C.; McMullen, R. K.; Meng, R. L.; Chu, C. W. Phys. Rev. Lett. 1992, 69, 2943.
54. Dorset, D. L.; McCourt, M. P. Acta Crystallogr. A 1994, 50, 344.
55. Gadd, G. E.; Elcombe, M. M.; Dennis, J.; Moricca, S.; Webb, N.; Cassidy, D.; Evans, P. J. J. Phys. Chem. Solids 1998, 59, 937-944.
56. Nolze, G.; Kraus, W. Powder Diffract. 1998, 13, 256.
57. Herzberg, G. Molecular Spectra and Molecular Structure, II Infrared and Raman Spectra of Polyatomic Molecules; Van Nostrand Reinhold: New York, 1945; Vol. II.
58. Heiney, P. A.; Fischer, J. E.; McGhie, A. R.; Romanow, W. J.; Denenstein, A. M.; J. P. McCauley, J.; A. B. Smith, I.; Cox, D. E. Phys. Rev. Lett. 1991, 66, 2911-2914.