The related compounds MThTe3 (M = Mn, Mg) and ACuThSe3 (A = K, Cs): Syntheses and characterization

Inorganic Chemistry

Volumn 39, Issue 4, 2000, Pages 688-691

  Narducci, Amy A ^a   Ibers, James A ^a  

^a NORTHWESTERN UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CATION; CESIUM; CHALCOGEN; COPPER DERIVATIVE; FERROMAGNETIC MATERIAL; MAGNESIUM DERIVATIVE; MANGANESE DERIVATIVE; POTASSIUM DERIVATIVE; SELENIUM DERIVATIVE; TELLURIUM DERIVATIVE; THORIUM DERIVATIVE; URANIUM DERIVATIVE;

ARTICLE; CRYSTAL STRUCTURE; CRYSTALLIZATION; MAGNETISM; OXIDATION; STOICHIOMETRY; SYNTHESIS; TEMPERATURE; X RAY DIFFRACTION;

EID: 0034695871     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic991039b     Document Type: Article

References (33)

1. Daoudi, A.; Potel, M.; Noël, H. J. Alloys Compd. 1996, 232, 180-185.
2. Cody, J. A.; Ibers, J. A. Inorg. Chem. 1996, 35, 3836-3838.
3. Wu, E. J.; Pell, M. A.; Ibers, J. A. J. Alloys Compd. 1997, 255, 106-109.
4. Narducci, A. A.; Ibers, J. A. Inorg. Chem. 1998, 37, 3798-3801.
5. Choi, K.-S.; Patschke, R.; Billinge, S. J. L.; Waner, M. J.; Dantus, M.; Kanatzidis, M. G. J. Am. Chem. Soc. 1998, 120, 10706-10714.
6. Narducci, A. A.; Ibers, J. A. Chem. Mater. 1998, 10, 2811-2823.
7. Zachariasen, W. H. Acta Crystallogr. 1949, 2, 291-296.
8. D'Eye, R. W. M.; Sellman, P. G.; Murray, J. R. J. Chem. Soc. 1952, 2555-2562.
9. Brochu, R.; Padiou, J.; Grandjean, D. C. R. Seances Acad. Sci., Ser. C 1970, 271, 642-643.
10. Cody, J. A.; Ibers, J. A. Inorg. Chem. 1995, 34, 3165-3172.
11. Huffman, J. C. Ph.D. Dissertation, Indiana University, 1974.
12. SMART and SAINT-Plus Data Collection and Processing Software for the SMART System, Versions 5.054 and 6.0, respectively; Bruker Analytical X-ray Instruments, Inc.: Madison, WI, 1997.
13. Sheldrick, G. M. SHELXTL DOS/Windows/NT, Version 5.10; Bruker Analytical X-ray Instruments, Inc.: Madison, WI, 1997.
14. Sheldrick, G. M. Acta Cryslallogr., Sect. A: Cryst. Phys., Diffr., Theor. Gen. Crystallogr. 1990, 46, 467-473.
15. Julien, R.; Rodier, N.; Tien, V. Acta Crystallogr., Sect. B: Struct. Crystallogr. Cryst. Chem. 1978, 34, 2612-2614.
16. Noël, H. C. R. Seances Acad. Sci., Ser. C 1974, 279, 513-515.
17. Noël, H.; Padiou, J. Acta Crystallogr., Sect. B: Struct. Crystallogr. Cryst. Chem. 1976, 32, 1593-1595.
18. Noël, H. Rev. Chim. Miner. 1977, 14, 295-299.
19. Panzer, B.; Range, K.-J. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1985, 41, 1007-1009.
20. Wu, E. J.; Ibers, J. A. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1997, C53, 993-994.
21. Yanagisawa, S.; Tashiro, M.; Anzai, S. J. Inorg. Nucl. Chem. 1969, 31, 943-946.
22. Zachariasen, W. Z. Phys. Chem. 1927, 128, 417-420.
23. Kittel, C. Introduction to Solid State Physics, 6th ed.; Wiley: New York, 1986.
24. Christuk, A. E.; Wu, P.; Ibers. J. A. J. Solid State Chem. 1994, 110, 330-336.
25. Wu, P.; Christuk, A. E.; Ibers, J. A. J. Solid State Chem. 1994, 110, 337-344.
26. Yang, Y.; Ibers, J. A. J Solid State Chem.. 1999, 147, 366-371.
27. Mansuetto, M. F.; Keane, P. M.; Ibers, J. A. J. Solid State Chem. 1992, 101, 257-264.
28. Mansuetto, M. F.; Keane, P. M.; Ibers, J. A. J. Solid State Chem. 1993, 105, 580-587.
29. Ferro, R. Z. Anorg. Allg. Chem. 1954, 275, 320-326.
30. D'Eye, R. W. M.; Sellman, P. G. J. Chem. Soc. 1954, 3760-3766.
31. Graham, J.; McTaggart, F. K. Aust. J. Chem. 1960, 13, 67-73.
32. Palewski, T. Phys. Status Solidi A 1984, 84, K47-K50.
33. 3, Ag, Th, and Te (molar ratio = 1:1:2:3) at 700°C. See Supporting Information for crystallographic details. Se and Te atoms are disordered over the two crystallographically independent sites. The value of x = 0.73(1) is close to the EDS results on the crystal used for the structure determination. Additional EDS analyses of other crystals from the same reaction mixture yielded a range for x of 0.50-1.0.