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Catalyst separation was accomplished by column chromatography. Filtration of the reaction mixture through a short dry Florisil column (eluent: hexane) and subsequent removal of the solvent at room temperature under vacuum (0.2 torr) furnished pure polymers in high yields. In some cases this process was repeated 2-3 times in order to remove the remaining traces of the catalyst
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Catalyst separation was accomplished by column chromatography. Filtration of the reaction mixture through a short dry Florisil column (eluent: hexane) and subsequent removal of the solvent at room temperature under vacuum (0.2 torr) furnished pure polymers in high yields. In some cases this process was repeated 2-3 times in order to remove the remaining traces of the catalyst.
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