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33749102180
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2 when connected to four N-atoms resulted in seven compounds, but all of them form discrete species with chelated lingands. A network structure with a -Cl analogue: Yaghi, O. M.; Li, G. Angew. Chem., Int. Ed. Engl. 1995, 34, 207.
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Yaghi, O.M.1
Li, G.2
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20
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0343983891
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note
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2 = 0.090.
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21
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0343111973
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note
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For easy understanding of the whole structure, some stereoview presentations are given in Supporting Information.
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23
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0343983889
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note
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2 = 0.0669. This structure was also solved and refined in the C2/c space group. However, it resulted in the disordered guest molecule but same R-value. All of the data were measured on a Siemens SMART/CCD diffractometer at 193 K. Non-hydrogen atoms were refined anisotropically, and hydrogen atoms were fixed at calculated positions and refined using a riding model.
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