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1H NMR to possess three THF molecules of crystallization. The product of the subsequent step was shown by 'H NMR to be H(OEt2)(THF)TFPB rather than the expected H(OEt2)2TFPB
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1H NMR to possess three THF molecules of crystallization. The product of the subsequent step was shown by 'H NMR to be H(OEt2)(THF)TFPB rather than the expected H(OEt2)2TFPB.
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0342857631
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See Supporting Information for details
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See Supporting Information for details.
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27
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33847551206
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In this case, we were unable to obtain a 29Si NMR signal at low temperature due to the long relaxation time of the Si center and difficulty using a DEPT sequence (lack of α-protons)
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In this case, we were unable to obtain a 29Si NMR signal at low temperature due to the long relaxation time of the Si center and difficulty using a DEPT sequence (lack of α-protons).
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28
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84985631338
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Klebe, G.4
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