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1H NMR (300 MHz) δ 7.02 (1H, s), 5.35 (1H, br s), 2.98 (1H, d, J = 16.5), 2.91 (1H, d, J = 16.5), 1.90 (3H, d, J = 1.5), 1.66 (3H, br s), 1.29 (3H, s).
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note
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1H NMR (300 MHz) δ 5.39 (1H, br s), 4.95 (1H, br dd, J = 5.4, 6.5), 2.92 (1H, dd, J = 3.9, 13.8), 2.70-2.60 (1H, m), 2.49 (1H, dd, J = 8.4, 15.6), 2.42 (1H, dd, J = 6.5, 15.2), 2.30-2.22 (2H, m), 2.07 (1H, dd, J = 7.2, 13.8), 2.00 (1H, br dd, J = 5.4, 15.2), 1.83 (3H, d, J = 2.1), 1.74 (3H, d, J = 1.8), 1.27 (3H, s).
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56
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For a general description of the experimental procedures employed in this research, see ref 10
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For a general description of the experimental procedures employed in this research, see ref 10.
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W-2 Raney Ni was deactivated by heating the ethanolic suspension at 60°C for 3-4 days
-
(b) W-2 Raney Ni was deactivated by heating the ethanolic suspension at 60°C for 3-4 days.
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