SCOPUS 정보 검색 플랫폼

Volumn 11, Issue 19, 2000, Pages 3887-3900

Asymmetrization of all-cis-3,5-dihydroxy-1-(methoxycarbonyl)cyclohexane and of the 4-methyl and 4-ethyl substituted homologues

(6) Zhao, Yurui a Wu, Yusheng a De Clercq, Pierre a Vandewalle, Maurits a Maillos, Philippe b Pascal, Jean Claude b

a GHENT UNIVERSITY (Belgium)

b R and D Chemical Department (Monaco)

Author keywords

[No Author keywords available]

Indexed keywords

3,5 DIHYDROXY 1 CYCLOHEXANECARBOXYLIC ACID DERIVATIVE; CYCLOHEXANE DERIVATIVE; TRIACYLGLYCEROL LIPASE; UNCLASSIFIED DRUG;

ACYLATION; ARTICLE; CATALYSIS; DRUG PURITY; DRUG SYNTHESIS; ENANTIOMER; ENZYME ACTIVITY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HYDROGENATION; IN VITRO STUDY; INFRARED SPECTROPHOTOMETRY; MASS SPECTROMETRY; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL; REACTION ANALYSIS; TECHNIQUE; TEMPERATURE;

EID: 0034612957 PISSN: 09574166 EISSN: None Source Type: Journal
DOI: 10.1016/S0957-4166(00)00339-6 Document Type: Article

Times cited : (17)

References (12)

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2
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- (a) Carda, M.; Van der Eycken, J.; Vandewalle, M. Tetrahedron: Asymmetry 1990, 1, 17; (b) Suemene, H.; Takahashi, M.; Maeda, S.; Xie, Z. F.; Sakai, K. Tetrahedron: Asymmetry 1990, 1, 425; (c) Dumortier, L.; Carda, M.; Van der Eycken, J.; Snatske, G.; Vandewalle, M. Tetrahedron: Asymmetry 1991, 2, 789.

3
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4
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- 8 and 9 from the commercially available acids (Aldrich). To the best of our knowledge 10 has not been described before. It was prepared from p-ethylbenzoic acid as described for 9 by: Manchand, P. S.; Towsend, J. M.; Belica, P. S.; Wong, H. S. Synthesis 1980, 409.

5
- 0007429979
- CAL; lipase from Candida antartica (0.5 u/mg), Fluka. PSL; lipase from Pseudomas cepacia (40 u/mg), Fluka. SAM II; lipase from Pseudomonas fluorescens (42 u/mg), Fluka. CCL; lipase, type II, from Candida cyclindracea, Aldrich. PPL; lipase from Hog pancreas (21 u/mg), Fluka. PLE; esterase from pig liver (130 u/mg), Fluka. GCL; lipase from Geotrichum candidum, Biocatalyst Ltd.

6
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- 2 modified with MeOH (5%).

7
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- 2).

8
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- Smidt, H. Chem. Ber. 1953, 86, 1437.

9
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- Mori, K.; Igarashi, Y. Liebigs Ann. Chem. 1988, 93.

10
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- Kagan H.B. (Ed.), Stuttgart: George Thieme Verlag
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* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.