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note
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Typical Reaction Procedure. To a solution of the aldehyde 5 in EtOH was added the amine 3a and 2-furylboronic acid (4a) successively. The reaction mixture was sealed and stirred at room temperature for 24 h. After concentration under vacuum, the residue was purified by chromatography with hexanes/ethyl acetate (9:1) to yield 6a as colorless oil (560 mg, 85% yield, >99% de).
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