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6
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0343656309
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1/n, R1 - 1.0596 for 3994 data with I > 2(σ)I; 2, a = 21.0073(12), b = 44.156(3), c = 8.1877(5) Å, Z = 8, space group Fdd2, R1 = 0.046 for 2402 data with I > 2σ(I). Crystallographic data (excluding structure factors) for the structures reported in this paper have been deposited with the Cambridge Cristallographic Data Centre as supplementary publication no. CCDC-143879 and CCDC-143880. Copies of the data can be obtained free of charge on application to CCDC, 12 Union Road, Cambridge CB2 1EZ, UK (fax: (+ 44) 1223-336-033; e-mail: deposit@ccdc.cam.ac.uk).
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0342786166
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Attempts to grow crystals suitable for neutron diffraction studies are in progress.
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13
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