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D. J. Cram, J. Day, D. R. Rayner, D. M. von Schrilts, D. J. Duchamp, D. C. Garwood, J. Am. Chem. Soc. 1970, 92, 7369; B. H. Nicolet, J. Willard, Science 1921, 53, 217; F. G. Mann, W. J. Pope, J. Chem. Soc. 1922, 1052; I. Kapovits, F. Ruff, A. Kucsmann, Tetrahedron 1972, 28, 4405; I. Kapovits, F. Ruff, A. Kucsmann, Tetrahedron. 1972, 28, 4413; N. Kunieda, S. Oae, Bull. Chem. Soc. Jpn. 1973, 46, 1745.
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Kapovits, I.1
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40
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0001131169
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D. J. Cram, J. Day, D. R. Rayner, D. M. von Schrilts, D. J. Duchamp, D. C. Garwood, J. Am. Chem. Soc. 1970, 92, 7369; B. H. Nicolet, J. Willard, Science 1921, 53, 217; F. G. Mann, W. J. Pope, J. Chem. Soc. 1922, 1052; I. Kapovits, F. Ruff, A. Kucsmann, Tetrahedron 1972, 28, 4405; I. Kapovits, F. Ruff, A. Kucsmann, Tetrahedron. 1972, 28, 4413; N. Kunieda, S. Oae, Bull. Chem. Soc. Jpn. 1973, 46, 1745.
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0003077051
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B. C. Menon, D. Darwish, Tetrahedron Lett. 1973, 4119; N. Furukawa, K. Harada, K. Tsujihara, S. Oae, Tetrahedron Lett. 1972, 1377; D. Darwish, S. K. Datta, Tetrahedron 1974, 30, 1155; M. Moriyama, N. Furukawa, T. Numata, S. Oae, J. Chem. Soc. Perkin Trans. 2 1977, 1783.
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0002944692
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B. C. Menon, D. Darwish, Tetrahedron Lett. 1973, 4119; N. Furukawa, K. Harada, K. Tsujihara, S. Oae, Tetrahedron Lett. 1972, 1377; D. Darwish, S. K. Datta, Tetrahedron 1974, 30, 1155; M. Moriyama, N. Furukawa, T. Numata, S. Oae, J. Chem. Soc. Perkin Trans. 2 1977, 1783.
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B. C. Menon, D. Darwish, Tetrahedron Lett. 1973, 4119; N. Furukawa, K. Harada, K. Tsujihara, S. Oae, Tetrahedron Lett. 1972, 1377; D. Darwish, S. K. Datta, Tetrahedron 1974, 30, 1155; M. Moriyama, N. Furukawa, T. Numata, S. Oae, J. Chem. Soc. Perkin Trans. 2 1977, 1783.
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37049107633
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B. C. Menon, D. Darwish, Tetrahedron Lett. 1973, 4119; N. Furukawa, K. Harada, K. Tsujihara, S. Oae, Tetrahedron Lett. 1972, 1377; D. Darwish, S. K. Datta, Tetrahedron 1974, 30, 1155; M. Moriyama, N. Furukawa, T. Numata, S. Oae, J. Chem. Soc. Perkin Trans. 2 1977, 1783.
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45
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33947326756
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D. R. Rayner, A. J. Gorden, K. Mislow, J. Am. Chem. Soc. 1968, 90, 4854; E. G. Miller, D. R. Rayner, K. Mislow, J. Am. Chem. Soc. 1968, 90, 4861; P. Bickart, F. W. Carson, J. Jacobus, E. G. Miller. K. Mislow, J. Am. Chem. Soc. 1968, 90, 4869; R. Tang, K. Mislow, J. Am. Chem. Soc. 1970, 92, 2100; R. W. Hoffman, Angew. Chem. 1979, 91, 625; Angew. Chem. Int. Ed. Engl. 1979, 18, 563.
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D. R. Rayner, A. J. Gorden, K. Mislow, J. Am. Chem. Soc. 1968, 90, 4854; E. G. Miller, D. R. Rayner, K. Mislow, J. Am. Chem. Soc. 1968, 90, 4861; P. Bickart, F. W. Carson, J. Jacobus, E. G. Miller. K. Mislow, J. Am. Chem. Soc. 1968, 90, 4869; R. Tang, K. Mislow, J. Am. Chem. Soc. 1970, 92, 2100; R. W. Hoffman, Angew. Chem. 1979, 91, 625; Angew. Chem. Int. Ed. Engl. 1979, 18, 563.
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D. R. Rayner, A. J. Gorden, K. Mislow, J. Am. Chem. Soc. 1968, 90, 4854; E. G. Miller, D. R. Rayner, K. Mislow, J. Am. Chem. Soc. 1968, 90, 4861; P. Bickart, F. W. Carson, J. Jacobus, E. G. Miller. K. Mislow, J. Am. Chem. Soc. 1968, 90, 4869; R. Tang, K. Mislow, J. Am. Chem. Soc. 1970, 92, 2100; R. W. Hoffman, Angew. Chem. 1979, 91, 625; Angew. Chem. Int. Ed. Engl. 1979, 18, 563.
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b) K. Tsujihara, N. Furukawa, K. Oae, S. Oae, Bull. Chem. Soc. Jpn. 1969, 42, 2631;
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c) J. B. Lamber, C. E. Mxan, D. S. Bailey, J. Am. Chem. Soc. 1972, 94, 208.
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54
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85037482814
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-
note
-
The rather wide range of melting points is due to partial thermal pyramidal inversion. In fact, the sample after the m.p. measurement showed the existence of the cis isomer by TLC.
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55
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0007162045
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J. Boeseken, A. T. H. van der Meulen, Recl. Trav. Chim. Pays-Bas 1936, 55, 925; H. Gilman, D. R. Swayampati, J. Am. Chem. Soc. 1955, 77, 5944; A. Fava, P. B. Sogo, M. Calvin, J. Am. Chem. Soc. 1957, 79, 1078; C. Friedel, J. M. Crafts, Ann. Chim. (Paris) 1888, 14, 433.
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J. Boeseken, A. T. H. van der Meulen, Recl. Trav. Chim. Pays-Bas 1936, 55, 925; H. Gilman, D. R. Swayampati, J. Am. Chem. Soc. 1955, 77, 5944; A. Fava, P. B. Sogo, M. Calvin, J. Am. Chem. Soc. 1957, 79, 1078; C. Friedel, J. M. Crafts, Ann. Chim. (Paris) 1888, 14, 433.
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J. Boeseken, A. T. H. van der Meulen, Recl. Trav. Chim. Pays-Bas 1936, 55, 925; H. Gilman, D. R. Swayampati, J. Am. Chem. Soc. 1955, 77, 5944; A. Fava, P. B. Sogo, M. Calvin, J. Am. Chem. Soc. 1957, 79, 1078; C. Friedel, J. M. Crafts, Ann. Chim. (Paris) 1888, 14, 433.
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K. Fries, W. Vogt, Ber. Dtsh. Chem. Ges. 1911, 44, 756; E. Bergmann, M. Tschudnowsky, Ber. Dtsh. Chem. Ges. B 1932, 65, 457; H. Baw, M. G. Bennett, P. Dearns, J. Chem. Soc. 1934, 680; W. T. J. Taylor, J. Chem. Soc. 1935, 625; D. A. Shirley, P. A. Roussel, Science 1951, 113, 208; S. Hosoya, R. G. Wood, Chem. Ind. (London) 1957, 1043; S. Hosoya, Chem. Ind. (London) 1958, 159; S. Hosoya, Acta Crystallogr. 1963, 16, 310.
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K. Fries, W. Vogt, Ber. Dtsh. Chem. Ges. 1911, 44, 756; E. Bergmann, M. Tschudnowsky, Ber. Dtsh. Chem. Ges. B 1932, 65, 457; H. Baw, M. G. Bennett, P. Dearns, J. Chem. Soc. 1934, 680; W. T. J. Taylor, J. Chem. Soc. 1935, 625; D. A. Shirley, P. A. Roussel, Science 1951, 113, 208; S. Hosoya, R. G. Wood, Chem. Ind. (London) 1957, 1043; S. Hosoya, Chem. Ind. (London) 1958, 159; S. Hosoya, Acta Crystallogr. 1963, 16, 310.
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K. Fries, W. Vogt, Ber. Dtsh. Chem. Ges. 1911, 44, 756; E. Bergmann, M. Tschudnowsky, Ber. Dtsh. Chem. Ges. B 1932, 65, 457; H. Baw, M. G. Bennett, P. Dearns, J. Chem. Soc. 1934, 680; W. T. J. Taylor, J. Chem. Soc. 1935, 625; D. A. Shirley, P. A. Roussel, Science 1951, 113, 208; S. Hosoya, R. G. Wood, Chem. Ind. (London) 1957, 1043; S. Hosoya, Chem. Ind. (London) 1958, 159; S. Hosoya, Acta Crystallogr. 1963, 16, 310.
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K. Fries, W. Vogt, Ber. Dtsh. Chem. Ges. 1911, 44, 756; E. Bergmann, M. Tschudnowsky, Ber. Dtsh. Chem. Ges. B 1932, 65, 457; H. Baw, M. G. Bennett, P. Dearns, J. Chem. Soc. 1934, 680; W. T. J. Taylor, J. Chem. Soc. 1935, 625; D. A. Shirley, P. A. Roussel, Science 1951, 113, 208; S. Hosoya, R. G. Wood, Chem. Ind. (London) 1957, 1043; S. Hosoya, Chem. Ind. (London) 1958, 159; S. Hosoya, Acta Crystallogr. 1963, 16, 310.
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K. Fries, W. Vogt, Ber. Dtsh. Chem. Ges. 1911, 44, 756; E. Bergmann, M. Tschudnowsky, Ber. Dtsh. Chem. Ges. B 1932, 65, 457; H. Baw, M. G. Bennett, P. Dearns, J. Chem. Soc. 1934, 680; W. T. J. Taylor, J. Chem. Soc. 1935, 625; D. A. Shirley, P. A. Roussel, Science 1951, 113, 208; S. Hosoya, R. G. Wood, Chem. Ind. (London) 1957, 1043; S. Hosoya, Chem. Ind. (London) 1958, 159; S. Hosoya, Acta Crystallogr. 1963, 16, 310.
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