In situ monitoring of solid-state polymerization reactions in sodium chloroacetate and sodium bromoacetate by 23Na and 13C solid-state NMR spectroscopy

Chemistry - A European Journal

Volumn 6, Issue 7, 2000, Pages 1120-1126

  Aliev, Abil E ^a   Elizabé, Laurent ^b   Kariuki, Benson M ^b   Kirschnick, Holger ^c   Thomas, John Meurig ^d   Epple, Matthias ^c   Harris, Kenneth D M ^b  

^a UNIVERSITY COLLEGE LONDON   (United Kingdom)

^b UNIVERSITY OF BIRMINGHAM   (United Kingdom)

^c UNIVERSITY OF HAMBURG   (Germany)

^d DAVY FARADAY RESEARCH LABORATORY   (United Kingdom)

Author keywords

NMR spectroscopy; Polymerizations; Solid state chemistry; Solid state reactions

Indexed keywords

BROMOACETIC ACID; CHLOROACETIC ACID;

ARTICLE; CHEMICAL ANALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYMERIZATION;

EID: 0034599373     PISSN: 09476539     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3765(20000403)6:7<1120::AID-CHEM1120>3.3.CO;2-1     Document Type: Article

References (46)

1. R. Hoffmann, Liebigs Ann. Chem. 1857, 102, 1-20.
2. R. Anschütz, Chem. Ber. 1892, 25, 3506-3512.
3. M. Epple, O. Herzberg, J. Mater. Chem. 1997, 7, 1037-1042.
4. L. B. McCusker, Acta Crystallogr. Sect. A 1991, 47, 297-313.
5. A. K. Cheetham, A. P. Wilkinson, Angew. Chem. 1992, 104, 1594-1608; Angew. Chem. Int. Ed. Engl. 1992, 31, 1557-1570.
6. A. K. Cheetham, A. P. Wilkinson, Angew. Chem. 1992, 104, 1594-1608; Angew. Chem. Int. Ed. Engl. 1992, 31, 1557-1570.
7. K. D. M. Harris, M. Tremayne, Chem. Mater. 1996, 8, 2554-2570.
8. D. M. Poojary, A. Clearfield, Acc. Chem. Res. 1997, 30, 414-422.
9. K. D. M. Harris, J. Chin. Chem. Soc. 1999, 46, 23-34.
10. M. Epple, H. Kirschnick, Chem. Ber. 1997, 130, 291-294.
11. L. Elizabé, B. M. Kariuki, K. D. M. Harris, M. Tremayne, M. Epple, J. M. Thomas, J. Phys. Chem. B 1997, 101, 8827-8831.
12. H. Ehrenberg, B. Hasse, K. Schwarz, M. Epple, Acta Crystallogr. Sect. B 1999, 55, 517-524.
13. M. Epple, U Sazama, A. Reller, N. Hilbrandt, M. Martin, L. Tröger, J. Chem. Soc. Chem. Commun. 1996, 1755-1756.
14. M. Epple, H. Kirschnick, Chem. Ber. 1996, 129, 1123-1129.
15. M. Epple, H. Kirschnick, J. M. Thomas, J. Therm. Anal. 1996, 47, 331-338.
16. O. Herzberg, R. Gehrke, M. Epple, Polymer 1999, 40, 507-511.
17. H. Schmalzried, Chemical Kinetics of Solids, VCH, Weinheim, 1995.
18. J. M. Thomas, Chem. Eur. J. 1997, 3, 1557-1562.
19. C. A. Fyfe, Solid State NMR for Chemists, CRC Press, 1984.
20. G. Engelhardt, D. Michel, High-resolution solid-state NMR of silicates and zeolites, Wiley, Chichester, 1987.
21. B. Blümich, Adv. Mater. 1991, 3, 237-245.
22. L. v. Wüllen, B. Gee, L. Züchner, M. Bertmer, H. Eckert, Ber. Bunsenges. Phys. Chem. 1996, 100, 1539-1549.
23. R. K. Harris, M. M. Sünnetcioglu, R. D. Fischer, Spectrochim. Acta 1994, 50A, 2069-2078.
24. A. E. Aliev, S. P. Smart, I. J. Shannon, K. D. M. Harris, J. Chem. Soc. Faraday Trans. 1996, 92, 2179-2185.
25. T. Xu, J. F. Haw, J. Am. Chem. Soc. 1994, 116, 7753-7759.
26. A. R. Brough, C. M. Dobson, I. G. Richardson, G. W. Groves, J. Mat. Sci. 1994, 29, 3926-3940.
27. D. B. Ferguson, J. F. Haw, Anal. Chem. 1995, 67, 3342-3348.
28. K. D. M. Harris, M. Tremayne, P. Lightfoot, P. G. Bruce, J. Am. Chem. Soc. 1994, 116, 3543-3547.
29. K. D. M. Harris, B. M. Kariuki, M. Tremayne, Mater. Sci. Forum 1998, 278-281, 32-37.
30. M. Epple, G. Sankar, J. M. Thomas. Chem. Mater. 1997, 9, 3127-3131.
31. M. Epple, L. Tröger, J. Chem. Soc. Dalton Trans. 1996, 11-16.
32. K. Schwarz, M. Epple, Macromol. Chem. Phys. 1999, 200, 2221-2229.
33. B. Nagasaka, S. Takeda, N. Nakamura, Chem. Phys. Lett. 1994, 222, 486.
34. S. H. Alarcon, A. C. Olivieri, S. A. Carss, R. K. Harris, Angew. Chem. 1994, 106, 1708-1709; Angew. Chem. Int. Ed. Engl. 1994, 33, 1624-1625.
35. S. H. Alarcon, A. C. Olivieri, S. A. Carss, R. K. Harris, Angew. Chem. 1994, 106, 1708-1709; Angew. Chem. Int. Ed. Engl. 1994, 33, 1624-1625.
36. A. E. Aliev, K. D. M. Harris, P. J. Barrie, S. Camus, J. Chem. Soc. Faraday Trans. 1994, 90, 3729-3730.
37. A. E. Aliev, K. D. M. Harris, R. K. Harris, S. A. Carss, A. C. Olivieri, J. Chem. Soc. Faraday Trans. 1995, 91, 3167-3176.
38. G. Kister, G. Cassanas, M. Vert, Polymer 1998, 39, 3335-3340.
39. H. W. Kohlschütter, L. Sprenger, Z. Phys. Chem. 1932, B16, 284-302.
40. G. M. J. Schmidt, Pure Appl. Chem. 1971, 27, 647-678.
41. J. M. Thomas, Phil. Trans. Roy. Soc. 1974, A277, 251.
42. G. Wegner, Pure Appl. Chem. 1977, 49, 443-454.
43. J. M. Thomas, Pure Appl. Chem. 1979, 51, 1065-1082.
44. J. W. Visser, J. Appl. Crystallogr. 1969, 2, 89.
45. Program OCTOPUS96 (Monte Carlo Technique for Powder Structure Solution), M. Tremayne, B. M. Kariuki, K. D. M. Harris, 1996.
46. Program GSAS, Los Alamos Lab. Report No. LA-UR-86-748, Los Alamos National Laboratory: Los Alamos, NM, A. C. Larson, R. B. von Dreele, 1987.