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3
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5544265373
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note
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2 unit at a time (homologation) as opposed to two carbons at a time for olefin polymerization. The two materials can be differentiated by mass spectrometry. Polymethylene spectra show peaks separated by 14 mass units, in polyethylene, the peaks are separated by 28 mass units.
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For previous work on the synthesis of terminally functionalized polyethylene oligomers, see: a) D. E. Bergbreiter, J. R. Blanton, R. Chandran, M. D. Hein, K. J. Huang, D. R. Treadwell, S. A. Walker, J. Polym. Sci. Part A 1989, 27, 4205; b) D. E. Bergbreiter, Prog. Polym. Sci. 1994, 19, 529.
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Bergbreiter, D.E.1
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Treadwell, D.R.6
Walker, S.A.7
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For previous work on the synthesis of terminally functionalized polyethylene oligomers, see: a) D. E. Bergbreiter, J. R. Blanton, R. Chandran, M. D. Hein, K. J. Huang, D. R. Treadwell, S. A. Walker, J. Polym. Sci. Part A 1989, 27, 4205; b) D. E. Bergbreiter, Prog. Polym. Sci. 1994, 19, 529.
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Bergbreiter, D.E.1
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For reviews of the earlier literature of polymethylene synthesis, see: a) M. Imoto, T. Nakaya, J. Macromol. Sci. Rev. Macromol. Chem. C 1972, 7, 1; b) M. Mucha, B. Wunderlich, J. Polym. Sci. Polym. Phys. 1974, 12, 1993.
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Imoto, M.1
Nakaya, T.2
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For reviews of the earlier literature of polymethylene synthesis, see: a) M. Imoto, T. Nakaya, J. Macromol. Sci. Rev. Macromol. Chem. C 1972, 7, 1; b) M. Mucha, B. Wunderlich, J. Polym. Sci. Polym. Phys. 1974, 12, 1993.
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For reviews of living polymerizations, see: a) O. W. Webster, Science 1991, 251, 887; b) T. Aida, Prog. Polym. Sci. 1994, 19, 469.
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Webster, O.W.1
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For reviews of living polymerizations, see: a) O. W. Webster, Science 1991, 251, 887; b) T. Aida, Prog. Polym. Sci. 1994, 19, 469.
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Aida, T.1
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unpublished results
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B. Busch, unpublished results.
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Busch, B.1
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0003726028
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Wiley, New York
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Brown, H.C.1
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21
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5544315923
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note
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Hydroboration can give rise to regioisomeric products. In the example cited, the ratio of regioisomers is 95:5 favoring the terminal-functionalized organoborane.
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