Polynuclear chromium(III) carboxylates. 1. Synthesis, structure, and magnetic properties of an octanuclear complex with a ring structure

Inorganic Chemistry

Volumn 39, Issue 7, 2000, Pages 1376-1380

  Eshel, Michal ^a   Bino, Avi ^a   Felner, Israel ^a   Johnston, David C ^b   Luban, Marshall ^b   Miller, Lance L ^b  

^a HEBREW UNIVERSITY OF JERUSALEM   (Israel)

^b IOWA STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CARBOXYLIC ACID DERIVATIVE; CHROMIUM DERIVATIVE;

AQUEOUS SOLUTION; ARTICLE; CHEMICAL BOND; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; CRYSTALLIZATION; MAGNETISM; MOLECULAR MODEL; STRUCTURE ANALYSIS; SYNTHESIS; TEMPERATURE; THEORY; X RAY CRYSTALLOGRAPHY;

EID: 0034599287     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic9907009     Document Type: Article

References (43)

1. (a) Department of Inorganic and Analytical Chemistry, The Hebrew University of Jerusalem.
2. (b) Racah Institute of Physics, The Hebrew University of Jerusalem.
3. (c) Ames Laboratory and Department of Physics and Astronomy, Iowa State University.
4. (a) You, J. F.; Snyder, B. S.; Papaefthymiou, G. C.; Holm, R. H. J. Am. Chem. Soc. 1990, 112, 1067.
5. (b) Wieghardt, K.; Quilitzsch, U.; Weiss, J.; Nuber, B. Inorg. Chem. 1980, 19, 2514.
6. (c) Gaete, W.; Ros, J.; Solans, X.; Font-Altaba, M.; Briansó, I. L. Inorg. Chem. 1984, 23, 39.
7. (d) Launay, J. P.; Jeannin, Y.; Nel, A. Inorg. Chem. 1983, 22, 277.
8. (e) Hartl, H.; Mahdjour-Hassan-Abadi, F. Angew. Chem., Int. Ed. Engl. 1984, 23, 378.
9. (f) Peters, K.; Ott, W.; von Schnering, H. G. Angew. Chem., Int. Ed. Engl. 1982, 21, 697.
10. (g) Woodward, P.; Dahl, L. F.; Abel, E. W.; Crosse, B. C. J. Am. Chem. Soc. 1965, 87, 5251.
11. (h) Gould, R. O.; Harding, M. M. J. Chem. Soc. A 1970, 875.
12. (i) Carruthers, J. R.; Prout, K.; Rossotti, F. J. C. Acta Crystallogr. 1975, B31, 2044.
13. (j) Evans, H. T., Jr. Acta Crystallogr. 1974, B30, 2095.
14. (k) Müller, U. Angew. Chem., Int. Ed. Engl. 1981, 20, 692.
15. (l) Chen, Q.; Liu, S.; Zubieta, J. Inorg. Chem. 1989, 28, 4433.
16. (m) Dance, I. G.; Scudder, M. L.; Secomb, R. Inorg. Chem. 1985, 24, 1201.
17. (n) Galy, J.; Mosset, A.; Grenthe, I.; Puigdomènch, I.; Sjöberg, B.; Hultén, F. J. Am. Chem. Soc. 1987, 109, 380.
18. (o) Ardizzoia, G. A.; Angaroni, M. A.; La Monica, G.; Cariati, F.; Moret, M.; Masciocchi, N. J. Chem. Soc., Chem. Commun. 1990, 1021.
19. (p) Chen, Q.; Liu, S.; Zubieta, J. Angew. Chem., Int. Ed. Engl. 1988, 27, 1724.
20. (q) Grossmann, B.; Heinze, J.; Herdtweck, E.; Köhler, F.; Nöth, H.; Schwenk, H.; Spiegler, M.; Wachter, W.; Weber, B. Angew. Chem., Int. Ed. Engl. 1997, 36, 387.
21. (r) Kumagai, H.; Kitagawa, S. Chem. Lett. 1996, 471.
22. (s) Taft, K. L.; Delfs, C. D.; Papaefthymiou, G. C.; Foner, S.; Gatteschi, D.; Lippard, S. J. J. Am. Chem. Soc. 1994, 116, 823.
23. (t) Watton, S. P., Fuhrmann, P.; Pence, L. E.; Caneschi, A.; Cornia, A.; Abbati, G. L.; Lippard, S. J. Angew. Chem., Int. Ed. Engl. 1997, 36, 2774 [XDK = dianion of m-xylylenediaminebis(Kemp's triacid imide)].
24. Chang, S. C.; Jeffrey, G. A. Acta Crystallogr. 1970, B26, 673.
25. Harton, A.; Terrell, K.; Huffman, J. C.; MacDonald, C.; Beatty, A.; Li, S.; O'Connor, C. J.; Vincent, J. B. Inorg. Chem. 1997, 36, 4875.
26. Bino, A.; Johnston, D. C.; Goshorn, D. P.; Halbert, T. R.; Stiefel, E. I. Science 1988, 241, 1479.
27. (a) Bino, A.; Chayat, R.; Pedersen, E.; Schneider, A. Inorg. Chem. 1991, 30, 856.
28. (b) Ellis, T.; Glass, M.; Harton, A.; Folting, K.; Huffman, J. C.; Vincent, J. B. Inorg. Chem. 1994, 33, 5522.
29. (c) Donald, S.; Terrell, K.; Vincent, J. B. Polyhedron 1995, 14, 971.
30. (a) Gérbéléu, N. V.; Struchkov, Y. T.; Timko, G. A.; Batsanov, A. S.; Indrichan, K. M.; Popovich, G. A. Dokl. Akad. Nauk SSSR 1990, 313, 1459.
31. (b) Atkinson, I. M.; Benelli, C.; Murrie, M.; Parsons, S.; Winpenny, R. E. P. Chem. Commun. 1999, 285.
32. Batsanov, A. S.; Timko, G. A.; Struchkov, Y. T.; Gérbéléu, N. V.; Indrichan, K. M. Koord. Khim. 1991, 17, 662.
33. Brauer, G. Handbook of Preparative Inorganic Chemistry; Academic Press: London, 1965; Vol. 2, pp 1371-2.
34. TEXSAN: Single Crystal Structure Analysis Software, Version 5.0; Molecular Structure Corp. The Woodlands, TX, 1989.
35. Sheldrick, G. M. In Cristallographic Computing 3; Sheldrick, G. M., Krüger, C., Goddard, R., Eds.; Oxford University Press: Oxford, U.K., 1985; p 175.
36. All crystallographic computing was done on a VAX 9000 computer at The Hebrew University of Jerusalem.
37. Turowski, P. N.; Bino, A.; Lippard, S. J. Angew. Chem., Int. Ed. Engl. 1990, 29, 811.
38. (a) Wieghardt, K.; Schmidt, W.; van Eldik, R.; Nuber, B.; Weiss, J. Inorg. Chem. 1980, 19, 2922 (TACN = 1,4,7-triazacyclononane).
39. (b) Toftlund, H.; Simonsen, O.; Pedersen, E. Acta Chem. Scand. 1990, 44, 676.
40. Kittel, C. Introduction to Solid State Physics, 4th ed.; John Wiley: New York, 1971.
41. Johnston, D. C. In Handbook of Magnetic Materials; Buschow, K. H. J., Ed.; Elsevier: Amsterdam, 1997; Vol. 10, pp 1-237.
42. Luscombe, J. H.; Luban, M.; Borsa, F. J. Chem. Phys. 1998, 108, 7266.
43. Joyce, G. S. Phys. Rev. 1967, 155, 478.