Direct evidence for O - H···NC hydrogen bonding in a cyanide-bridged lanthanide - transition-metal complex (H2O)6(DMF)6Ho2[Ni(CN)4]3: An eight-coordinated holmium center with a bicapped (square face) trigonal prismatic geometry

Inorganic Chemistry

Volumn 39, Issue 20, 2000, Pages 4639-4645

  Du, Bin ^a   Meyers, Edward A ^a   Shore, Sheldon G ^a  

^a OHIO STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CYANIDE; HOLMIUM; LANTHANIDE; METAL COMPLEX; NICKEL; WATER;

ARTICLE; CATALYST; CHEMICAL REACTION; COMPLEX FORMATION; CRYSTAL STRUCTURE; DATA ANALYSIS; ENERGY TRANSFER; GEOMETRY; HYDROGEN BOND; INFRARED SPECTROMETRY; X RAY CRYSTALLOGRAPHY;

EID: 0034596927     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic000207t     Document Type: Article

References (92)

1. (a) Gallagher, P. K. Mater. Res. Bull. 1968, 3, 225.
2. (b) Nakayama, S.; Sakamoto, M.; Matsuki, K.; Okimura, Y.; Ohsumi, R.; Nakayama, Y.; Sadaoka, Y. Chem. Lett. 1992, 2145.
3. (c)Traversa, E.; Nunziante, P.; Sakamoto, M.; Watanabe, K.; Sadaoka, Y.; Sakai, Y. Chem. Lett. 1995, 189.
4. Minh, N. Q. J. Am. Ceram. Soc. 1993, 76, 563.
5. Dunbar, K. R.; Heintz, R. A. In Progress in Inorganic Chemistry; Karlin, K. D., Ed.; John Wiley & Sons: New York, 1997; Vol. 45, p 283.
6. (a) Shuk, P.; Vecher, A.; Kharton, V.; Tichonova, L.; Wiemhöfer, H. D.; Guth, U.; Göpel, W. Sens. Actuators. B 1993, 16, 401.
7. (b) Sadaoka, Y.; Traversa, E.; Sakamoto, M. J. Mater. Chem. 1996, 6(8), 1355.
8. (a) Arakawa, T.; Takada, K. I.; Tsunemine, Y.; Shiokawa, J. Sens. Actuators 1988, 14, 215.
9. (b) Matuura, Y.; Matsushima, S.; Sakamoto, M.; Sadaoka, Y. J. Mater. Chem. 1993, 3(7), 767.
10. (c) Traversa, E.; Matsushima, S.; Okada, G.; Sadaoka, Y.; Sakai, Y.; Watanabe, K. Sens. Actuators, B 1995, 25, 661.
11. Sakamoto, M.; Matsuki, K.; Ohsumi, R.; Nakayama, Y.; Matsumoto, A.; Okawa, Y. Bull. Chem. Soc. Jpn. 1992, 65, 2278.
12. (a) Mullica, D. F.; Milligan, W. O.; Kouba, W. T. J. Inorg. Nucl. Chem. 1979, 41, 967.
13. (b) Mullica, D. F.; Milligan, W. O.; Garner, R. L. Acta Crystallogr., Sect. B 1980, 36, 2561.
14. (c) Mullica, D. F.; Perkins, H. O.; Sappenfield, E. L.; Grossic, D. A. J. Solid State Chem. 1988, 74, 9.
15. (d) Mullica, D. F.; Perkins, H. O.; Sappenfield, E. L. J. Solid Slate Chem. 1988, 74, 419.
16. (e) Mullica, D. F.; Perkins, H. O.; Sappenfield, E. L.; Leschnitzer, D. Acta Crystallogr., Sect. C 1989, 45, 330.
17. (f) Mullica, D. F.; Sappenfield, E. L. J. Solid State Chem. 1989, 82, 168.
18. (g) Mullica, D. F.; Sappenfield, E. L. Acta Crystallogr., Sect. C 1991, 47, 2433.
19. (h) Mullica, D. F.; Sappenfield, E. L. J. Crystallogr. Spectrosc. Res. 1991, 21, 529.
20. (i) Mullica, D. F.; Alvarez, F. H.; Sappenfield, E. L. J. Solid State Chem. 1997, 129, 12.
21. (a) Extended Linear Chain Compounds; Miller, J. S., Ed.; Plenum Press: New York, 1982/1983; Vols. I-III.
22. (b) Gliemann, G.; Yersin, H. Struct. Bonding 1985, 62, 87.
23. (c) Synthesis and Properties of Low-Dimensional Materials; Miller, J. S., Epstein, A. J., Eds.; The New York Academy of Sciences: New York, 1978; p 539.
24. (d) Yersin, H. J. Phys. Chem. 1978, 68, 4707.
25. (e) Yersiri, H.; Ammon, W. v.; Stock. M.; Gliemann, G. J. Lumin. 1979, 18/19, 774.
26. (a) Inorganic Semipermeable Membranes: Research and Development Progress Report No. 723; Milligan, W. O., Ed.; U.S. Department of the Interior, Office of Saline Water: Washington, DC, Oct 1971.
27. (b) The structure and Morphology of Inorganic Membranes; Research and Development Progress Report No. 594: Milligan, W. O., Ed.; U.S. Department of the Interior, Office of Saline Water: Washington, DC, Dec 1970.
28. (a) Amer, I.; Alper, H. J. Am. Chem. Soc. 1989, 111, 927.
29. (b) Matsubara, S.; Kodama, T.; Utimoto, K. Tetrahedron Lett. 1990, 31, 6379.
30. Jain, A. K.; Singh, R. P.; Bala, C. Analyst 1982, 107, 770.
31. (a) Knoeppel, D. W.; Shore, S. G. Inorg. Chem. 1996, 35, 1747.
32. (b) Knoeppel, D. W.; Shore, S. G. Inorg. Chem. 1996, 35, 5328.
33. (c) Shore, S. G.; Knoeppel, D. W.; Deng, H. B.; Liu, I. P.; White, J. P., III; Chun, S. H. J. Alloys Compd. 1997, 249, 25.
34. (d) Knoeppel, D. W.; Liu, J. P.; Meyers, E. A.; Shore, S. G. Inorg. Chem. 1998, 37, 4828.
35. (e) Liu, J. P.; Meyers, E. A.; Shore, S. G. Inorg. Chem. 1998, 37, 5410.
36. (a) Du, B. Ph.D. Dissertation, The Ohio State University, Columbus, OH, 2000.
37. (b) Du, B.; Ebels, U. S.; Wigen, P. E.; Shore, S. G. Abstracts of the ACS 31st Central Regional Meeting; American Chemical Society: Washington, DC, 1999: No. 283.
38. (c) Du, B.; Shore, S. G.; Ebels, U. S.; Wigen, P. E. Abstracts of the 216th ACS National Meeting; American Chemical Society: Washington, DC, 1998; INOR-596.
39. (d) Du, B.; Knoeppel, D. W.; Meyers, E. A.; Shore, S. G. Abstracts of the 214th ACS National Meeting: American Chemical Society: Washington, DC, 1997; INOR-198.
40. (a) Hulliger, F.; Landolt, M.; Vetsch, H. In Proceedings of the Tenth Rare Earth Research Conference, Carefree, AZ, 1973; p 80.
41. (b) Hulliger, F.; Landolt, M.; Vetsch, H. J. Solid State Chem. 1976, 18, 283, 307.
42. (c) Petter, W.; Gramlich, V.; Hulliger, F. J. Solid State Chem. 1989, 82, 161.
43. (d) Gramlich, V.; Petter, W.; Hulliger, F. Acta Crystallogr., Sect. C 1990, 46, 724.
44. (e) Dommann, A.; Vetsch, H.; Hulliger, F. Acta Crystallogr., Sect. C 1990, 46, 1992, 1994.
45. (f) Xu, X. L.; Emmenegger, R.; Hulliger, F. Eur. J. Solid State Inorg. Chem. 1990, 27, 537.
46. (g) Hulliger, F.; Vetsch, H.; Xu, X. L. Eur. J. Solid State Inorg. Chem. 1995, 32, 907.
47. Bailey, W. E.; Williams, R. J.; Milligan, W. O. Acta Crystallogr., Sect. B 1973, 29, 1365.
48. von Kietaibl, H.; Petter, W. Helv. Phys. Acta 1974, 47, 425.
49. Klement, U. Z. Kristallogr. 1993, 208, 285, 288.
50. Shi, J. M.; Liao, D. Z.; Cheng, P.; Jiang, Z. H.; Wang, G. L.; Yao, X. K.; Wang, H. G. Acta Chim. Sinica 1997, 55, 467.
51. Du, B.; Meyers, E. A.; Shore, S. G. Manuscripts in preparation.
52. Kou, H. Z.; Yang, G. M.; Liao, D. Z.; Cheng, P.; Jiang, Z. H.; Yan, S. P.; Huang, X. Y.; Wang, G. L. J. Chem. Crystallogr. 1998, 28 (4), 303.
53. Mullica, D. F.; Farmer, J. M.; Cunningham, B. P. J. Coord. Chem. 1999, 48, 449.
54. (a) van Vleck, J. H. Rev. Mod. Phys. 1953, 25, 220.
55. (b) Mattis, D. C. The Theory of Magnetism I; Springer: Berlin, 1981.
56. Cotton, F. A.; Wilkenson, G. Advanced Inorganic Chemistry, 5th ed.; Wiley and Sons: New York, 1988.
57. (a) Moreau-Colin, M. L. Struct. Bonding 1972, 10, 167.
58. (b) Gliemann, G.; Yersin, H. Struct. Bonding 1985, 62, 87.
59. (c) Cernak, J.; Dunaj-Jurco, M.; Melnik, M.; Chomic, J.; Skorsepa, J. Rev. Inorg. Chem. 1988, 9, 259.
60. (a) Lippard, S. J. In Progress in Inorganic Chemistry; Cotton, F. A., Ed; John Wiley & Sons: New York, 1967; Vol. 8, p 109.
61. (b) Muetterties, E. L.; Wright, C. M. Q. Rev., Chem. Soc. 1967, 21, 109.
62. (c) Sinha, S. P. Struct. Bonding 1976, 25, 69.
63. (d) Kepert, D. L. In Progress in Inorganic Chemistry; Lippard, S. J., Ed.; John Wiley & Sons: New York, 1978; Vol. 24, p 179.
64. (e) King, R. B. Polyhedron 1994, 13, 2005.
65. Porai-Koshits, M. A.; Aslanov, L. A. Zh. Strukt. Khim. 1972, 13, 266.
66. (a) Hoard, J. L.; Silverton, J. V. Inorg. Chem. 1963, 2, 235.
67. (b) Kepert, D. L. J. Chem. Soc. 1965, 4736.
68. (c) Lippard, S. J.; Russ, B. J. Inorg. Chem. 1968, 7, 1686.
69. (d) Muetterties, E. L. Inorg. Chem. 1973, 12, 1963.
70. King, R. B. Polyhedron 1994, 13, 2005.
71. Aslanov, L. A.; Korytnyi, E. F.; Porai-Koshits, M. A. Zh. Strukt. Khim. 1971, 12, 661.
72. Templeton, L. K.; Templeton, D. H.; Zalkin, A. Acta Crystallogr., Sect. C 1985, 41, 355.
73. Shannon, R. D. Acta Crystallogr., Sect. A 1976, 32, 751.
74. (a) Hamilton, W. C.; Ibers, J. A. Hydrogen Bonding in Solids; Benjamin, Inc.: New York, 1968.
75. (b) Jeffrey, G. A. An introduction to Hydrogen Bonding; Oxford University Press: New York, 1997.
76. (c) Steiner, T.; Saenger, W. Carbohydr. Res. 1994, 259, 1.
77. The data in Table 5 were generated by the PLATON package. Spek, A. L. PLATON; Utrecht University: Utrecht, The Netherlands, 1980-1999.
78. (a) Taylor, R.; Kennard, O. Acta Crystallogr., Sect. B 1983, 39, 133.
79. (b) Jeffrey, G. A.; Lewis, L. Carbohydr. Res. 1978, 60, 179.
80. (c) Jeffrey, G. A.; Takagi, S. Acc. Chem. Res. 1978, 11, 264.
81. The difference maps were generated using the SHELXTL-97 program; see ref 44.
82. Sorrell, T. N. Interpreting Spectra of Organic Molecules; University Science Books: Mill Valley, CA, 1988; pp 16, 33.
83. Nakamoto, K.; Margoshes, M.; Rundle, R. E. J. Am. Chem. Soc. 1955, 77, 6480.
84. (a) Nakamoto, K. Infrared and Roman Spectra of Inorganic and Coordination Compounds, 4th ed.; John Wiley & Sons: New York, 1986; p 278.
85. (b) Adams, D. M. Metal-Ligand and Related Vibrations; Edward Arnold: London, 1967.
86. Kubas, G. J.; Jones, L. H. Inorg. Chem. 1974, 13, 2816.
87. Swanson, B. I.; Rafalko, J. J. Inorg. Chem. 1976, 15, 249.
88. Otwinowski, Z.; Minor, W. In Methods in Enzymology; Carter, C. W., Jr., Sweet, R. M., Eds.; Academic Press: New York, 1997; Vol. 276(A), p 307.
89. (a) Blessing, R. H. Acta Crystallogr., Sect. A 1995, 51, 33.
90. (b) Blessing, R. H. J. Appl. Crystallogr. 1997, 30, 421.
91. Mackay, S.; Gilmore, C. J.; Edwards, C.; Tremayne, M.; Stuart, N.; Shankland, K. MaXus: a computer program for the solution and refinement of crystal structures from diffraction data; University of Glasgow: Scotland, Nonius BV; Delft, The Netherlands, and MacScience Co. Ltd.: Yokohama, Japan, 1998.
92. Sheldrick, G. M. SHELXTL-97: A Structure Solution and Refinement Program, University of Göttingen: Germany, 1998.