Characterization of silanol groups in protonated magadiite by 1H and 2H solid-state nuclear magnetic resonance

Clays and Clay Minerals

Volumn 48, Issue 6, 2000, Pages 632-637

  Komori, Yoshihiko ^a   Miyoshi, Masaki ^a   Hayashi, Shigenobu ^b   Sugahara, Yoshiyuki ^a   Kuroda, Kazuyuki ^a  

^a WASEDA UNIVERSITY   (Japan)

^b NATL INST OF MAT AND CHEM RES   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

CHARACTERIZATION; HYDROGEN BONDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SYNTHESIS (CHEMICAL);

MAGADIITE; SILANOL GROUP;

CLAY MINERALS;

CLAY MINERAL; MAGADIITE; NUCLEAR MAGNETIC RESONANCE;

EID: 0034352251     PISSN: 00098604     EISSN: None     Source Type: Journal    
DOI: 10.1346/CCMN.2000.0480604     Document Type: Article

References (45)

1. 29Si NMR spectroscopy. Journal of the Chemical Society, Chemical Communications, 851-852.
2. 23Na NMR study of hydrous layered silicates. Journal of Materials Chemistry, 6, 843-847.
3. Almond, G.G., Harris, R.K., and Franklin, K.R. (1997) A structural consideration of kanemite, octosilicate, magadiite and kenyaite. Journal of Materials Chemistry, 7, 681-687.
4. Barnes, R.G. (1974) Deuteron quadrupole coupling tensors in solids. In Advances in Nuclear Quadrupole Resonances, Volume I, J.A.S. Smith, ed., Heyden, London, 335-355.
5. Brandt, A., Schwieger, W., and Bergk, K.H. (1987) A new model structure of sheet sodium (Na) silicate hydrates (Na-SH)-theoretical view based on known X-ray and NMR-measurements. Revue de Chimie Minérale, 24, 564-571.
6. Brandt, A., Schwieger, W., and Bergk, K.H. (1988) Development of a model structure for the sheet silicate hydrates ilerite, magadiite, and kenyaite. Crystal Research and Technology, 23, 1201-1203.
7. Brindley, G.W. (1969) Unit cell of magadiite in air, in vacuo, and under other conditions. American Mineralogist, 54, 1583-1591.
8. Butler, L.G. and Brown, T.L. (1981) Nuclear quadrupole coupling constants and hydrogen bonding. A molecular orbital study of oxygen-17 and deuterium field gradients in formaldehyde-water hydrogen bonding. Journal of the American Chemical Society, 103, 6541-6549.
9. +-magadiite, a crystalline hydrated silica. Chemistry of Materials, 4, 855-863.
10. Eckert, H., Yesinowski, J.P. and Stolper, E.M. (1989) Quantitative NMR studies of water in silicate glasses. Solid State Ionics, 32/33, 298-313.
11. Garcés, J.M., Rocke, S.C., Crowder, C.E., and Hasha, D.L. (1988) Hypothetical structures of magadiite and sodium octosilicate and structural relationships between the layered alkali metal silicates and the mordenite- and pentasil-group zeolites. Clays and Clay Minerals, 36, 409-418.
12. Gluszak, T.J., Chen, D.T., Sharma, S.B., Dumesic, J.A., and Root, T.W. (1992) Observation of Brensted acid sites of D-Y zeolite with deuterium NMR. Chemical Physics Letters, 190, 36-41.
13. Hadjar, H., Balard, H., and Papirer, E. (1995) Comparison of crystalline (H-magadiite) and amorphous silicas using inverse gas chromatography at finite concentration conditions. Colloids and Surfaces A, 103, 111-117.
14. Hayashi, S. (1994) Effects of magic-angle spinning on spinlattice relaxations in talc. Solid State Nuclear Magnetic Resonance, 3, 323-330.
15. 1H spectra. Journal of Physical Chemistry, 96, 10922-10928.
16. 2H NMR study of hydrogen bonding in deuterated kaolinite. Clays and Clay Minerals, 42, 561-566.
17. 2H-NMR spectroscopy of solids and liquid crystals. In NMR Basic Principles and Progress: Solid State NMR III: Organic Matter, Volume 32, P. Diehl, E. Fluck, H. Günther, R. Kosfeld, and J. Seelig, eds., Spriger-Verlag, Berlin, 1-67.
18. Huang, Y., Jiang, Z., and Schwieger, W. (1999) Vibrational spectroscopic studies of layered silicates. Chemistry of Materials, 11, 1210-1217.
19. Kobe, J.M., Gluszak, T.J., Dumestic, J.A., and Root, T.W. (1995) Deuterium NMR characterization of Brønsted acid sites and silanol species in zeolites. Journal of Physical Chemistry, 99, 5485-5491.
20. Kosuge, K., Yamazaki, A., Tsunashima, A., and Otsuka, R. (1992) Hydrothermal synthesis of magadiite and kenyaite. Journal of the Ceramic Society of Japan, 100, 326-331.
21. Lagaly, G., Beneke, K., and Weiss, A. (1975a) Magadiite and H-magadiite: I. Sodium magadiite and some of its derivatives. American Mineralogist, 60, 642-649.
22. Lagaly, G., Beneke, K., and Weiss, A. (1975b) Magadiite and H-magadiite: II. H-magadiite and its intercalation compounds. American Mineralogist, 60, 650-658.
23. Landis, M.E., Aufdembrink, B.A., Chu, P., Johnson, I.D., Kirker, G.W., and Rubin, M.K. (1991) Preparation of molecular sieves from dense, layered metal oxides. Journal of the American Chemical Society, 113, 3189-3190.
24. Mercier, L., Facey, G.A., and Detellier, C. (1994) Organolayered silicates. Interlamellar intercalation and grafting of ethylene glycol in magadiite. Journal of the Chemical Society, Chemical Communications, 2111-2112.
25. Ogawa, M., Miyoshi, M., and Kuroda, K. (1998a) Perfluoroalkylsilylation of the interlayer silanol groups of a layered silicate, magadiite. Chemistry of Materials, 10, 3787-3789.
26. Ogawa, M., Okutomo, S., and Kuroda, K. (1998b) Control of interlayer microstructures of a layered silicate by surface modification with organochlorosilanes. Journal of the American Chemical Society, 120, 7361-7362.
27. Okutomo, S., Kuroda, K., and Ogawa, M. (1999) Preparation and characterization of silylated-magadiite. Applied Clay Science, 15, 253-264.
28. Pfeifer, H. (1994) NMR of Solid Surfaces. In NMR Basic Principles and Progress: Solid State NMR II: Inorganic Matter, Volume 31, P. Diehl, E. Fluck, H. Günther, R. Kosfeld, and J. Seelig, eds., Spriger-Verlag, Berlin, 31-90.
29. 2O). Journal of Solid State Chemistry, 63, 118-121.
30. Rojo, J.M., Ruiz-Hitzky, E., Sanz, J., and Serratosa, J.M. (1983) Characterization of surface Si-OH groups in layer silicic acids by IR and NMR spectroscopies. Revue de Chimie Minérale, 20, 807-816.
31. Rojo, J.M., Ruiz-Hitzky, E., and Sanz, J. (1988) Proton-sodium exchange in magadiite. Spectroscopic study (NMR, IR) of the evolution of interlayer OH groups. Inorganic Chemistry, 27, 2785-2790.
32. Ruiz-Hitzky, E. and Rojo, J.M. (1980) Intracrystalline grafting on layer silicic acids. Nature, 287, 28-30.
33. Ruiz-Hitzky, E., Rojo, J.M., and Lagaly, G. (1985) Mechanism of the grafting of organosilanes on mineral surfaces III. Interlamellar grafting of layer silicic acids. Colloid and Polymer Science, 263, 1025-1030.
34. 1H MAS NMR study of benzene and p-xylene in zeolites and a mesoporous material FSM-16. Bulletin of the Chemical Society of Japan, 70, 97-105.
35. Scholzen, G., Beneke, K., and Lagaly, G. (1991) Diversity of magadiite. Zeitschrift für Anorganische und Allgemeine Chemie, 597, 183-196.
36. Schwieger, W., Heidemann, D., and Bergk, K. (1985) High-resolution solid-state silicon-29 nuclear magnetic resonance spectroscopic studies of synthetic sodium silicate hydrates. Revue de Chimie Minérale, 22, 639-650.
37. Sprung, R., Davis, M.E., Kauffman, J.S., and Dybowski, C. (1990) Pillaring of magadiite with silicate species. Industrial & Engineering Chemistry Research, 29, 213-220.
38. Wong, S. and Cheng, S. (1993) Preparation and characterization of pillared magadiite. Chemistry of Materials, 5, 770-777.
39. Xie, X. and Hayashi, S. (1999a) NMR study of kaolinite intercalation compounds with formamide and its derivatives. 1. Structure and orientation of guest molecules. Journal of Physical Chemistry B, 103, 5949-5955.
40. Xie, X. and Hayashi, S. (1999b) NMR study of kaolinite intercalation compounds with formamide and its derivatives. 2. Dynamics of guest molecules. Journal of Physical Chemistry B, 103, 5956-5962.
41. Yanagisawa, T., Kuroda, K., and Kato, C. (1988a) Organic derivatives of layered polysilicates I. Trimethylsilylation of magadiite and kenyaite. Reactivity of Solids, 5, 167-175.
42. Yanagisawa, T., Kuroda, K., and Kato, C. (1988b) Organic derivatives of layered polysilicates II. Reaction of magadiite and kenyaite with diphenylmethylchlorosilane. Bulletin of the Chemical Society of Japan, 61, 3743-3745.
43. Yanagisawa, T., Harayama, M., Kuroda, K., and Kato, C. (1990) Organic derivatives of layered polysilicates III. Reaction of magadiite and kenyaite with alkyldimethylchlorosilane. Solid State Ionics, 42, 15-19.
44. Yanagisawa, T., Kuroda, K., Doi, A., and Kato, C. (1991) Heat-treatment of trimethylsilylated layered polysilicates and the variation in their specific surface areas. Clay Science, 8, 107-116.
45. 1H MAS NMR at high spinning speeds. Journal of the American Chemical Society, 109, 6274-6282.