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2OTi: C, 35.05; H, 7.07; N, 8.18%. Found: C, 34.85; H, 7.07; N, 8.09%.
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0002112522
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note
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-1, 3936 reflections, 2θmax = 55.0°, 2θ-ω scan, 25 °C), R1 = 0.124 (all data) and wR2 = 0.205 (all data) for 154 variables.
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28
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0001428641
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0001993070
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note
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4. The organic layer was separated and the products were extracted with ether. The crude products obtained were subjected to column chromatography (ethyl acetate-hexane, 1 : 3) to give 1,2-diphenyl-1,2-ethanediol (0.10 g, 92% yield, dl / mesu = >99 / <1).
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34
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0033214637
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