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0001943237
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3 of methanol solution (0.15 M) of sodium hydroxide. To the resulting solution was added basic iron(III) acetate (23 mg, 0.07 mmol) to give a dark reddish brown solution. The solution was filtered and allowed to stand several days at room temperature. Black crystals deposited were collected by filtration (yield 12 mg).
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7
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0001963761
-
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note
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w = 0.099. Intensity data were collected on an Enraf-Nonius CAD4 diffractometer using graphite-monochromated Mo-Kα radiation. All the structures were solved by the direct method and refined by the full-matrix least-squares method using a MolEN program package.
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13
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0001930313
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note
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30)), where x = exp(-J/kT); the other symbols have their usual meanings.
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