메뉴 건너뛰기




Volumn 144, Issue 2, 2000, Pages 207-216

Deuterium Nuclear Spin-Lattice Relaxation Times and Quadrupolar Coupling Constants in Isotopically Labeled Saccharides

Author keywords

13C T1; 2H quadrupolar coupfing constants; 2H T1; Isotopically labeled saccharides

Indexed keywords

DEUTERIUM; ISOTOPE; MONOSACCHARIDE;

EID: 0034203198     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2000.2045     Document Type: Article
Times cited : (13)

References (38)
  • 1
    • 0040240399 scopus 로고
    • Deuterium magnetic resonance, applications in chemistry, physics and biology
    • H. H. Mantsch, H. Saito, and I. C. P. Smith, Deuterium magnetic resonance, applications in chemistry, physics and biology, Prog. NMR Spectrosc. 11, 211-271 (1977).
    • (1977) Prog. NMR Spectrosc. , vol.11 , pp. 211-271
    • Mantsch, H.H.1    Saito, H.2    Smith, I.C.P.3
  • 3
    • 0032513009 scopus 로고    scopus 로고
    • 13C cross- Correlation NMR experiments: Application to the N-terminal SH3 domain from drk
    • 13C cross- correlation NMR experiments: Application to the N-terminal SH3 domain from drk, J. Mol. Biol. 276, 939-954 (1998).
    • (1998) J. Mol. Biol. , vol.276 , pp. 939-954
    • Yang, D.1    Mittermaier, A.2    Mok, Y.K.3    Kay, L.E.4
  • 5
    • 0000350649 scopus 로고
    • Deuteron magnetic resonance study of some crystals containing an O-D⋯O bond
    • T. Chiba, Deuteron magnetic resonance study of some crystals containing an O-D⋯O bond, J. Chem. Phys. 41, 1352-1358 (1964).
    • (1964) J. Chem. Phys. , vol.41 , pp. 1352-1358
    • Chiba, T.1
  • 6
    • 0009655232 scopus 로고
    • Field gradients at the deuteron in molecules
    • R. Bersohm, Field gradients at the deuteron in molecules, J. Chem. Phys. 32, 85-88 (1960).
    • (1960) J. Chem. Phys. , vol.32 , pp. 85-88
    • Bersohm, R.1
  • 7
    • 0348059565 scopus 로고
    • The dependence of the deuteron quadrupolar coupling constant, diamagnetic shielding, and diamagnetic susceptibility of methane on internuclear dis-tance
    • M. Dixon, T. A. Claxton, and R. E. Overill, The dependence of the deuteron quadrupolar coupling constant, diamagnetic shielding, and diamagnetic susceptibility of methane on internuclear dis-tance, J. Magn. Reson. 12, 193-198 (1973).
    • (1973) J. Magn. Reson. , vol.12 , pp. 193-198
    • Dixon, M.1    Claxton, T.A.2    Overill, R.E.3
  • 8
    • 8244221922 scopus 로고
    • Carbon-13-enriched carbohydrates. Preparation of aldononitriles and their reduction with a palladium catalyst
    • A. S. Serianni, H. A. Nunez, and R. Barker, Carbon-13-enriched carbohydrates. Preparation of aldononitriles and their reduction with a palladium catalyst, Carbohydr. Res. 72, 71-78 (1979).
    • (1979) Carbohydr. Res. , vol.72 , pp. 71-78
    • Serianni, A.S.1    Nunez, H.A.2    Barker, R.3
  • 9
    • 0025109615 scopus 로고
    • Stable isotopically-enriched D-glucose: Strategies to introduce carbon, hydrogen and oxygen isotopes at various carbons
    • A. S. Serianni, T. Vuorinen, and P. B. Bondo, Stable isotopically-enriched D-glucose: Strategies to introduce carbon, hydrogen and oxygen isotopes at various carbons, J. Carbohydr. Chem. 90, 513-541 (1990).
    • (1990) J. Carbohydr. Chem. , vol.90 , pp. 513-541
    • Serianni, A.S.1    Vuorinen, T.2    Bondo, P.B.3
  • 10
    • 0028179487 scopus 로고
    • 13C-labeled D-ribose: Chemienzymic synthesis of various isotopomers
    • 13C-labeled D-ribose: Chemienzymic synthesis of various isotopomers, J. Biomol. Struct. Dynam. 11, 1133-1148 (1994).
    • (1994) J. Biomol. Struct. Dynam. , vol.11 , pp. 1133-1148
    • Serianni, A.S.1    Bondo, P.B.2
  • 14
    • 0003616787 scopus 로고
    • Chemical synthesis of aldoses enriched with isotopes of hydrogen and oxygen
    • A. S. Serianni, E. L. Clark, and R. Barker, Chemical synthesis of aldoses enriched with isotopes of hydrogen and oxygen, Methods Enzymol. 89, Part D, 79-83 (1982).
    • (1982) Methods Enzymol. , vol.89 , Issue.PART D , pp. 79-83
    • Serianni, A.S.1    Clark, E.L.2    Barker, R.3
  • 15
    • 36849104960 scopus 로고
    • Measurement of spin relaxation in complex systems
    • R. L Void, J. S. Waugh, M. P. Klein, and D. E. Phelps, Measurement of spin relaxation in complex systems, J. Chem. Phys. 48, 3831-3832 (1968).
    • (1968) J. Chem. Phys. , vol.48 , pp. 3831-3832
    • Void, R.L.1    Waugh, J.S.2    Klein, M.P.3    Phelps, D.E.4
  • 16
    • 0000165391 scopus 로고
    • Optimal design of relaxation time experiments
    • G. H. Weiss and J. A. Ferretti, Optimal design of relaxation time experiments, Prog. NMR Spectrosc. 4, 317-335 (1988).
    • (1988) Prog. NMR Spectrosc. , vol.4 , pp. 317-335
    • Weiss, G.H.1    Ferretti, J.A.2
  • 18
    • 0346798630 scopus 로고
    • Proton spin-lattice relaxation: A new, quantitative measure of aglycone-sugar interactions
    • Anomeric Effect: Origin and Consequences(W. A. Szarek and D. Horton, Eds.), American Chemical Society
    • J. M. Berry, L. D. Hall, D. G. Welder, and K. F. Wong, Proton spin-lattice relaxation: A new, quantitative measure of aglycone-sugar interactions, in "Anomeric Effect: Origin and Consequences" (W. A. Szarek and D. Horton, Eds.), ACS Symposium Series 87, pp. 30-49, American Chemical Society (1979).
    • (1979) ACS Symposium Series , vol.87 , pp. 30-49
    • Berry, J.M.1    Hall, L.D.2    Welder, D.G.3    Wong, K.F.4
  • 19
    • 0028824890 scopus 로고
    • Carbon-13 nuclear magnetic relaxation and motional behavior of carbohydrate molecules in solution
    • P. Dais, Carbon-13 nuclear magnetic relaxation and motional behavior of carbohydrate molecules in solution, Adv. Carbohydr. Chem. Biochem. 51, 63-131 (1995).
    • (1995) Adv. Carbohydr. Chem. Biochem. , vol.51 , pp. 63-131
    • Dais, P.1
  • 20
    • 0000438294 scopus 로고
    • Ab initio quadratic configuration interaction calculation of indirect NMR spin-spin coupling constants
    • I. Carmichael, Ab initio quadratic configuration interaction calculation of indirect NMR spin-spin coupling constants, J. Phys. Chem. 97, 1789-1792 (1993).
    • (1993) J. Phys. Chem. , vol.97 , pp. 1789-1792
    • Carmichael, I.1
  • 22
    • 0000189651 scopus 로고
    • Density-functional thermochemistry. III. the role of exact exchange
    • A. D. Becke, Density-functional thermochemistry. III. The role of exact exchange, J. Chem. Phys. 98, 5648-5652 (1993).
    • (1993) J. Chem. Phys. , vol.98 , pp. 5648-5652
    • Becke, A.D.1
  • 24
    • 0000721485 scopus 로고
    • Density functional theories in quantum chemistry-Beyond the local density approximation
    • American Chemical Society, Washington, DC
    • A. D. Becke, Density functional theories in quantum chemistry-Beyond the local density approximation, in "ACS Symposium Series 394," pp. 165-179, American Chemical Society, Washington, DC (1989).
    • (1989) ACS Symposium Series , vol.394 , pp. 165-179
    • Becke, A.D.1
  • 25
    • 0000216001 scopus 로고
    • Accurate spin-dependent electron liquid correlation energies for local spin density calculations: A critical analysis
    • S. H. Vosko, L. Wilk, and M. Nusair, Accurate spin-dependent electron liquid correlation energies for local spin density calculations: A critical analysis, Can. J. Phys. 58, 1200-1211 (1980).
    • (1980) Can. J. Phys. , vol.58 , pp. 1200-1211
    • Vosko, S.H.1    Wilk, L.2    Nusair, M.3
  • 26
    • 0345491105 scopus 로고
    • Development of the Colle-Salvetti correlation-energy formula into a functional of the electron density
    • C. Lee, W. Yang, and R. G. Parr, Development of the Colle-Salvetti correlation-energy formula into a functional of the electron density, Phys. Rev. B 37, 785-789 (1988).
    • (1988) Phys. Rev. B , vol.37 , pp. 785-789
    • Lee, C.1    Yang, W.2    Parr, R.G.3
  • 27
    • 0347170005 scopus 로고
    • Self-consistent molecular orbital methods. XII. Further extensions of gaussian-type basis sets for use in molecular orbital studies of organic molecules
    • W. J. Hehre, R. Ditchfield, and J. A. Pople, Self-consistent molecular orbital methods. XII. Further extensions of gaussian-type basis sets for use in molecular orbital studies of organic molecules, J. Chem. Phys. 56, 2257-2261 (1972).
    • (1972) J. Chem. Phys. , vol.56 , pp. 2257-2261
    • Hehre, W.J.1    Ditchfield, R.2    Pople, J.A.3
  • 29
    • 0000089343 scopus 로고    scopus 로고
    • 13C spin-coupling behavior in aldofuranosyl rings from density functional theory
    • 13C spin-coupling behavior in aldofuranosyl rings from density functional theory, J. Phys. Chem. A 103, 3783-3785 (1999).
    • (1999) J. Phys. Chem. A , vol.103 , pp. 3783-3785
    • Cloran, F.1    Carmichael, I.2    Serianni, A.S.3
  • 30
    • 0007445559 scopus 로고
    • Carbon-13 nuclear magnetic resonance of ganglioside sugars. Spin-lattice relaxation probes for structure and microdynamics of cell surface carbohydrates
    • M. F. Czarniecki and E. R. Thornton, Carbon-13 nuclear magnetic resonance of ganglioside sugars. Spin-lattice relaxation probes for structure and microdynamics of cell surface carbohydrates, J. Am. Chem. Soc. 99, 8279-8282 (1977).
    • (1977) J. Am. Chem. Soc. , vol.99 , pp. 8279-8282
    • Czarniecki, M.F.1    Thornton, E.R.2
  • 33
    • 85031538350 scopus 로고    scopus 로고
    • 2-deoxy-β-D-ribofuranosylamine: Quantum mechanical calculations of molecular structure and NM R spin-spin coupling constants in nitrogen-containing saccharides
    • in press
    • F. Cloran, Y. Zhu, J. Osborn, I. Carmichael, and A. S. Serianni, 2-deoxy-β-D-ribofuranosylamine: Quantum mechanical calculations of molecular structure and NM R spin-spin coupling constants in nitrogen-containing saccharides, J. Am. Chem. Soc., in press.
    • J. Am. Chem. Soc.
    • Cloran, F.1    Zhu, Y.2    Osborn, J.3    Carmichael, I.4    Serianni, A.S.5
  • 34
    • 0001233775 scopus 로고
    • Neutron diffraction refinement of the crystal structures of methyl α-D-galactopyranoside monohydrate and methyl β-D galactopyranoside
    • S. Takagi and G. A. Jeffrey, Neutron diffraction refinement of the crystal structures of methyl α-D-galactopyranoside monohydrate and methyl β-D galactopyranoside, Acta Crystallogr. Sect. B 35, 902-906 (1979).
    • (1979) Acta Crystallogr. Sect. B , vol.35 , pp. 902-906
    • Takagi, S.1    Jeffrey, G.A.2
  • 35
    • 0029354841 scopus 로고
    • 1H spin-coupling constants in aldofuranosyl rings: Effect of conformation on coupling magnitude
    • 1H spin-coupling constants in aldofuranosyl rings: Effect of conformation on coupling magnitude, J. Am. Chem. Soc. 117, 8645-8650 (1995).
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 8645-8650
    • Serianni, A.S.1    Wu, J.2    Carmichael, I.3
  • 36
    • 0030792778 scopus 로고    scopus 로고
    • Carbohydrate reaction intermediates: Effect of ring-oxygen protonation on the structure and conformation of aldofuranosyl rings
    • J. Kennedy, J. Wu, K. Drew, I. Carmichael, and A. S. Serianni, Carbohydrate reaction intermediates: Effect of ring-oxygen protonation on the structure and conformation of aldofuranosyl rings, J. Am. Chem. Soc. 119, 8933-8945 (1997).
    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 8933-8945
    • Kennedy, J.1    Wu, J.2    Drew, K.3    Carmichael, I.4    Serianni, A.S.5
  • 37
    • 0001229902 scopus 로고    scopus 로고
    • A new method for the determination of the dynamic isotope effect and the deuterium quadrupole coupling constant in liquids
    • E. H. Hardy, R. Witt, A. Dölle, and M. D. Zeidler, A new method for the determination of the dynamic isotope effect and the deuterium quadrupole coupling constant in liquids, J. Magn. Reson. 134, 300-307 (1998).
    • (1998) J. Magn. Reson. , vol.134 , pp. 300-307
    • Hardy, E.H.1    Witt, R.2    Dölle, A.3    Zeidler, M.D.4


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.