NMR quantification in hydrothermal in situ syntheses

Magnetic Resonance in Chemistry

Volumn 38, Issue 6, 2000, Pages 429-435

  Gerardin, Corine ^a,b   Haouas, Mohamed ^a   Lorentz, Chantal ^a   Taulelle, Francis ^a  

^a CNRS   (France)

^b Fluids Laboratory   (United States)

Author keywords

14N NMR; 27AL NMR; External calibration; Hydrothermal; NMR; NMR tubes; Quantification

Indexed keywords

HYDROFLUORIC ACID; HYDROLYSIS; HYDROTHERMAL SYNTHESIS; MICROPOROUS MATERIALS; Q FACTOR MEASUREMENT; TEMPERATURE;

14N NMR; 27AL NMR; EXTERNAL CALIBRATION; HYDROTHERMAL; IN-SITU OBSERVATIONS; IN-SITU SYNTHESIS; NMR TUBES; OUTER DIAMETERS; QUANTIFICATION; SIGNAL LOSS;

CALIBRATION;

EID: 0034196232     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/1097-458X(200006)38:6<429::AID-MRC671>3.0.CO;2-S     Document Type: Article

References (36)

1. 1. Tison K, Hunt ER. J. Chem. Phys. 1971; 54: 1526.
2. 2. VonJouanne J, Heidberg H. J. Magn. Reson. 1972; 7: 1.
3. 3. Yamada H. Rev. Sci. Instrum. 1974; 45: 640.
4. 4. Roe D. J. Magn. Reson. 1985; 63: 388.
5. 5. Kinrade SD, Swaddle TWJ. J. Magn. Reson. 1988; 77: 669.
6. 6. Horvath IT, Ponce EC. Rev. Sci. Instrum. 1991; 62: 1104.
7. 7. Bai S, Taylor CM, Mayene CL, Pugmire RJ, Grant DM. Rev. Sci. Instrum. 1996; 67: 240.
8. 8. Jonas J. Rev. Sci. Instrum. 1972; 43: 643.
9. 9. Earl WL, Vanni H, Merbach E. J. Magn. Reson. 1978; 30: 571.
10. 10. DeFries TH, Jonas J. J. Magn. Reson. 1979; 35: 111.
11. 11. Rathke JW. J. Magn. Reson. 1989; 85: 150.
12. 12. Prey U, Helm L, Merbach E. High Press. Res. 1990; 2: 237.
13. 13. Mao XA, Holz M. Appl. Magn. Reson. 1994; 6: 529.
14. 14. Gadan DG, Robinson FNH. J. Magn. Reson. 1979; 34: 449.
15. 15. Bahlmann EKF, Harris RK, Say BJ. Magn. Reson. Chem. 1993; 31: 266.
16. 16. Vogel AI. A Text Book of Quantitative Inorganic Analysis. Longman: London, 1961.
17. 17. VanGeet AL. Anal. Chem. 1968; 40: 2227.
18. 18. VonHippel A. Handbook of Physics. (2nd edn). McGraw-Hill: New York, 1967.
19. 19. Clark WG. Rev. Sci. Instrum. 1964; 35: 316.
20. 20. Kong JA. Theory of Electromagnetic Waves. Wiley: New York, 1975.
21. 21. Shaw D. Fourier Transform NMR Spectroscopy. Elsevier: Amsterdam, 1976.
22. 22. Bradley DJ, Pitzer KS. J. Phys. Chem. 1979; 83: 1599.
23. 23. Uematsu M, Franck EU. J. Phys. Chem. Ref. Data 1980; 9: 1291.
24. 24. Akitt JW, Elders JM. J. Chem. Soc. Farad. Trans. 1985; 81: 1923.
25. 25. Fu G, Nazar LF, Bain AD. Chem. Mater. 1991: 3: 602.
26. 26. Bertsch PM. Soil Sci. Soc. Am. J. 1987; 51: 825.
27. 27. Kloprogge JT, Seykens D, Geus JW, Jansen JBH. J. Non-Cryst. Solids 1992; 142: 94.
28. 28. Turner RC. Can. J. Chem. 1976; 54: 1528.
29. 29. Bottero JY, Cases JM, Flessinger F, Poirier JE. J. Phys. Chem. 1980; 84: 2933.
30. 30. Hsu PH. Clays Clay Miner. 1997; 45: 286.
31. 31. Akitt JW, Elders JM, Fontaine XLR, Kundu AK. J Chem. Soc. Dalton Trans. 1989; 1889.
32. 32. Wang WZH. Clays Clay Miner. 1994; 42: 356.
33. 33. Kloprogge JTS, Jansen JBH, Geus JW. J. Non-Cryst. Solids 1993; 152: 207.
34. 34. Gerardin C, In M, Allouche L, Haouas M, Taulelle F. Chem. Mater. 1999; 11: 1285.
35. 35. Gerardin C, Haouas M, Taulelle F, Estournes C, Loiseau T, Ferey G. In Materials Research Society Proceedings, 12th International Zeolite Conference, 1998 Baltimore, Maryland, USA. Treacy MMJ, Marcus BK, Bisher ME, Higgins JB (eds). Warrendale, USA, 1999.
36. 36. Haouas M, Gerardin C, Taulelle F, Estournes C, Loiseau T, Ferey G. J. Chim. Phys. 1998; 95: 302.