Sequential hydrolysis of swine carcass samples and determination of amino acid concentrations using pre-column derivatization with phenyl isothiocyanate

Journal of the Science of Food and Agriculture

Volumn 80, Issue 6, 2000, Pages 757-762

  Wubben, Jennifer E ^a   Albin, David M ^a   Gabert, Vince M ^a  

^a UNIVERSITY OF ILLINOIS AT URBANA CHAMPAIGN   (United States)

Author keywords

Amino acids; Carcass; Hydrolysis time; Pig

Indexed keywords

AMINO ACID ANALYSIS; AMINO ACID; CARCASS; HYDROLYSIS KINETICS; HYDROLYSIS; PHENYL ISOTHIOCYANATE; REACTION TIME; SWINE;

EID: 0034192696     PISSN: 00225142     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1097-0010(20000501)80:6<757::AID-JSFA621>3.0.CO;2-Z     Document Type: Article

References (24)

1. Bikker P, Karabinas V, Verstegen MWA and Campbell RG, Protein and lipid accretion in body components of growing gilts (20 to 45 kilograms) as affected by energy intake. J Anim Sci 73:2355-2363 (1995).
2. Bidlingmeyer BA, Cohen SA and Tarvin TL, Rapid analysis of amino acids using pre-column derivatization. J Chromatogr 336:93-104 (1984).
3. Elkin RG and Wasynczuk AM, Amino acid analysis of feedstuff hydrolysates by precolumn derivatization with phenylisothiocyanate and reversed-phase high-performance liquid chromatography. Cereal Chem 64:226-229 (1987).
4. Gehrke CW, Wall Sr LL, Absheer JS, Kaiser FE and Zumwalt RW, Sample preparation for chromatography of amino acids: acid hydrolysis of proteins. J Assoc Off Anal Chem 68:811-821 (1985).
5. Henrickson RL and Meredith SC, Amino acid analysis by reverse-phase high-performance liquid chromatography: precolumn derivatization with phenylisothiocyanate. Anal Biochem 136:65-74 (1984).
6. Rowan AM, Moughan PJ and Wilson MN, Effect of hydrolysis time on the determination of amino acid composition of diet, ileal digesta, and feces samples and on the determination of dietary amino acid digestibility coefficients. J Agric Food Chem 40:981-985 (1992).
7. Rayner L, Protein hydrolysis of animal feeds for amino acid content. J Agric Food Chem 33:722-725 (1985).
8. Ott L, Multiple comparisons, in An Introduction to Statistical Methods and Data Analysis: 4th edn, Ed by Lozyniak K and Krikorian S. Wadsworth, Inc, Belmont, CA, pp 807-841 (1993).
9. Milliken GA and Johnson DE, Simultaneous inference procedures and multiple comparisons, in Analysis of Messy Data Volume 1: Designed Experiments, Ed by Mason R and Scheier B. Van Nostrand Reinhold, New York, NY, pp 29-45 (1984).
10. SAS/STAT user's guide (release 6.08), SAS Institute, Inc, Cary, NC (1990).
11. Darragh AJ, Garrick DJ, Moughan PJ and Hendriks WH, Correction for amino acid loss during acid hydrolysis of a purified protein. Anal Biochem 236:199-207 (1996).
12. Rees MW, The estimation of threonine and serine in proteins. Biochem J 40:632-640 (1946).
13. Glazer AN, Delange RJ and Sigman DS, Chemical modification of proteins, in Laboratory Techniques in Biochemistry and Molecular Biology, Ed by Work TS and Work E. North-Holland Publishing, Amsterdam, pp 1-205 (1976).
14. Finley JW, Reducing variability in amino acid analysis, in Digestibility and Amino Acid Availability in Cereals and Oilseeds, Ed by Finley JW and Hopkins DT. American Association of Cereal Chemists, St. Paul, MN, pp 15-30 (1985).
15. Fountoulakis M and Lahn HW, Hydrolysis and amino acid composition analysis of proteins. J Chromatogr 826:109-134 (1998).
16. Samuels SE, Aarts HLM and Ball RO, Effect of dietary proline on proline metabolism in the neonatal pig. J Nutr 119:1900-1906 (1989).
17. Southern BG, Kelly JM and McBride BW, Phenyalanine flooding dose procedure is effective in measuring intestinal and liver protein synthesis in sheep. J Nutr 122:2398-2407 (1992).
18. de Jonge LH and Breuer M, Modification of the analysis of amino acids in pig plasma. J Chromatogr 652:90-96 (1994).
19. Garnett NK, The influence of amino acid hydrolysis times on the determination of amino acid requirements for poultry, in Proceedings of the Regional Seminar on Future Developments in the Poultry Industry, Ed by Ideris A and Hamid R. World Poultry Science Association, Malaysia, pp 14-17 (1985).
20. Kohler GO and Palter R, Studies on methods for amino acid analysis of wheat products. Cereal Chem 44:512-520 (1967).
21. Tkachuk R and Irvine GN, Amino acid compositions of cereals and oilseeds meals. Cereal Chem 46:206-218 (1969).
22. Slump P, in Symposium mi Protein Metabolism and Nutrition, Proceedings ofthe 3rd European Association for Animal Production. European Association for Animal Production, Wageningen, The Netherlands, p 14 (1980).
23. Lenis NP, Van Diepen JThM and Goedhart PW, Amino acid requirements of pigs. 1. requirements for methionine + cystine, threonine and tryptophan of fast-growing boars and gilts, fed ad libitum. Neth J Agric Sci 38:577-595 (1990).
24. Mroz Z, Jongbloed AW and Kemme PA, Apparent digestibility and retention of nutrients bound to phytate complexes as influenced by microbial phytase and feeding regimen in pigs. J Anim Set 72:126-132 (1994).