Time-Shared X(ω 1 )-Half-Filter for Improved Sensitivity in Subspectral Editing

Journal of Magnetic Resonance

Volumn 144, Issue 1, 2000, Pages 168-170

  Andersson, Patrik ^a   Otting, Gottfried ^a  

^a KAROLINSKA INSTITUTE   (Sweden)

Author keywords

Protein DNA complex; Semi constant time; Subspectral editing; X( 1 ) half filter

Indexed keywords

BACTERIAL DNA; CARBON; DNA BINDING PROTEIN;

ARTICLE; CHEMISTRY; ESCHERICHIA COLI; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SENSITIVITY AND SPECIFICITY;

CARBON ISOTOPES; DNA, BACTERIAL; DNA-BINDING PROTEINS; ESCHERICHIA COLI; MAGNETIC RESONANCE SPECTROSCOPY; SENSITIVITY AND SPECIFICITY;

EID: 0034181859     PISSN: 10907807     EISSN: None     Source Type: Journal    
DOI: 10.1006/jmre.2000.2057     Document Type: Editorial

References (13)

1. 15 N labeling of proteins, J. Magn. Reson. 70, 500-505 (1986).
2. S. W. Fesik, R. T. Gampe Jr., and T. W. Rockway, Application of isotope-filtered 2D NOE experiments in the conformational analysis of atrial natriuretic factor (7-23), J. Magn. Reson. 74, 366-371 (1987).
3. 1 H]-NMR spectroscopy: Combined use with isotope labeling for studies of macromolecular conformation and intermolecular interactions, Q. Rev. Biophys. 23, 39-96 (1990).
4. 13 C-labeled Antennapedia homeodomain and structure determination of the DNA-bound homeodomain, J. Mol. Biol. 234, 1084-1097 (1993).
5. 1 H TOCSY experiment for assignment of aromatic ring resonances and selective identification of tyrosine ring resonances in proteins: Description and application to photoactive yellow protein, J. Biomol. NMR 9, 313-316 (1997).
6. M. Sattler, J. Schleucher, and C. Griesinger, Heteronuclear multidimensional NMR experiments for the structure determination of proteins in solution employing pulsed field gradients, Prog. NMR Spectrosc. 34, 93-158 (1999).
7. 13 C magnetization, J. Magn. Reson. B 101, 114-119 (1993).
8. T. M. Logan, E. T. Olejniczak, R. X. Xu, and S. W. Fesik, A general method for assigning NMR spectra of denatured proteins using 3D HC(CO)NH-TOCSY triple resonance experiments, J. Biomol. NMR 3, 225-231 (1993).
9. M. Sunnerhagen, M. Nilges, G. Otting, and J. Carey, Solution structure of the DNA-binding domain and model for the binding of multifunctional arginine repressor to DNA, Nat. Struct. Biol. 4, 819-826 (1997).
10. 13 C] double half-filter technique, J. Biomol. NMR 3, 709-714 (1993).
11. P. Plateau and M. Guéron, Exchangeable proton NMR without base-line distortion, using new strong-pulse sequences, J. Am. Chem. Soc. 104, 7310-7311 (1982).
12. A. J. Shaka, P. B. Barker, and R. Freeman, Computer-optimized decoupling scheme for wideband applications and low-level operation. J. Magn. Reson. 64, 547-552 (1985).
13. L. Emsley and G. Bodenhausen, Gaussian pulse cascades: New analytical functions for rectangular selective inversion and in-phase excitation in NMR, Chem. Phys. Lett. 165, 469-476 (1990).