Combined variable-temperature and variable-field 15N cross-polarization magic angle spinning NMR study of 15N,14N residual dipolar coupling in pyrazole derivatives

Magnetic Resonance in Chemistry

Volumn 38, Issue 4, 2000, Pages 305-310

  Alarcón, Sergio H ^a   Jiménez, José A ^b   Claramunt, Rosa M ^b   Limbach, Hans Heinrich ^c   Elguero, José ^d  

^a UNIVERSIDAD NACIONAL DE ROSARIO   (Argentina)

^b UNIVERSIDAD NACIONAL DE EDUCACIÓN A DISTANCIA   (Spain)

^c FREIE UNIVERSITÄT BERLIN   (Germany)

^d INSTITUTO DE QUÍMICA MÉDICA   (Spain)

Author keywords

15N, 14N residual dipolar coupling; NMR; Pyrazoles; Solid state 15N NMR

Indexed keywords

MAGIC ANGLE SPINNING; POLARIZATION; X RAY DIFFRACTION;

15N, 14N RESIDUAL DIPOLAR COUPLING; CROSS POLARIZATION MAGIC-ANGLE SPINNINGS; CROSS-POLARIZATION/MAGIC ANGLE SPINNINGS; MAGIC-ANGLE-SPINNING NMR; NMR STUDIES; PYRAZOLE DERIVATIVES; PYRAZOLES; RESIDUAL DIPOLAR COUPLINGS; SOLID-STATE 15N NMR; VARIABLE TEMPERATURE;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 0034164241     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(sici)1097-458x(200004)38:4<305::aid-mrc633>3.0.co;2-e     Document Type: Article

References (32)

1. 1. Harris RK, Olivieri AC. Prog. Nucl. Magn. Reson. Spectrosc. 1992; 24: 435.
2. 2. Eichele K, Wasylishen RE, Corrigan JF, Doherty S, Sun Y, Carty AJ. Inorg. Chem. 1993; 32: 121; Eichele K, Wasylishen RE. Angew. Chem., Int. Ed. Engl. 1992; 31: 1222.
3. 2. Eichele K, Wasylishen RE, Corrigan JF, Doherty S, Sun Y, Carty AJ. Inorg. Chem. 1993; 32: 121; Eichele K, Wasylishen RE. Angew. Chem., Int. Ed. Engl. 1992; 31: 1222.
4. 3. Alarcon SH, Olivieri AC, Carss SA, Harris RK, Zuriaga M, Monti GA. J. Magn. Reson. 1995; 116: 244; Alarcón SH, Olivieri AC, Carss SA, Harris RK. Angew. Chem. 1994; 106: 1624; Olivieri AC, Elguero J, Sobrados I, Cabildo P, Claramunt R. J. Phys. Chem. 1994; 98: 5207; Alarcón SH, Olivieri AC, Harris RK. Solid State NMR 1993; 2: 325.
5. 3. Alarcon SH, Olivieri AC, Carss SA, Harris RK, Zuriaga M, Monti GA. J. Magn. Reson. 1995; 116: 244; Alarcón SH, Olivieri AC, Carss SA, Harris RK. Angew. Chem. 1994; 106: 1624; Olivieri AC, Elguero J, Sobrados I, Cabildo P, Claramunt R. J. Phys. Chem. 1994; 98: 5207; Alarcón SH, Olivieri AC, Harris RK. Solid State NMR 1993; 2: 325.
6. 3. Alarcon SH, Olivieri AC, Carss SA, Harris RK, Zuriaga M, Monti GA. J. Magn. Reson. 1995; 116: 244; Alarcón SH, Olivieri AC, Carss SA, Harris RK. Angew. Chem. 1994; 106: 1624; Olivieri AC, Elguero J, Sobrados I, Cabildo P, Claramunt R. J. Phys. Chem. 1994; 98: 5207; Alarcón SH, Olivieri AC, Harris RK. Solid State NMR 1993; 2: 325.
7. 3. Alarcon SH, Olivieri AC, Carss SA, Harris RK, Zuriaga M, Monti GA. J. Magn. Reson. 1995; 116: 244; Alarcón SH, Olivieri AC, Carss SA, Harris RK. Angew. Chem. 1994; 106: 1624; Olivieri AC, Elguero J, Sobrados I, Cabildo P, Claramunt R. J. Phys. Chem. 1994; 98: 5207; Alarcón SH, Olivieri AC, Harris RK. Solid State NMR 1993; 2: 325.
8. 4. Alarcón SH, Olivieri AC, Carss SA, Harris RK. Magn. Reson. Chem. 1995; 33: 603.
9. 5. Hoelger CG, Rössler E, Wherle B, Aguilar-Parrilla F, Limbach H. J. Phys. Chem. 1995; 99: 14271.
10. 6. Alarcón SH, Olivieri AC. Recent Advances in Analytical Techniques. Gordon and Breach Science: Amsterdam, 1998; 263; Grondona P, Olivieri AC. Concepts Magn. Reson. 1993; 5: 319.
11. 6. Alarcón SH, Olivieri AC. Recent Advances in Analytical Techniques. Gordon and Breach Science: Amsterdam, 1998; 263; Grondona P, Olivieri AC. Concepts Magn. Reson. 1993; 5: 319.
12. 7. Olivieri AC. J. Magn. Reson. 1989; 81: 201.
13. 8. Vega S. J. Chem. Phys. 1974; 81: 201.
14. 9. Harris RK, Jonsen P, Packer KJ. J. Magn. Reson. 1985; 23: 565.
15. 10. Neunhoeffer H, Clausen M, Vötter HD, Ohl H, Krüger C, Argermund K. Liebigs Ann. Chem. 1985; 1732.
16. 11. Fruchier A, Pellegrin V, Claramunt RM, Elguero J. Org. Magn. Reson. 1984; 22: 473.
17. 12. Jiménez JA, Claramunt RM, Mó O, Wehrmann F, Buntkowsky G, Limbach H-H, Goddard R, Elguero J. Phys. Chem. Chem. Phys. 1999; 1: 5113.
18. 13. Klebe KJ, Habraken CL. Synthesis 1973; 294.
19. 14. Crivello JV. J. Org. Chem. 1981; 46: 3056.
20. 15. Palmer M, Scott FE, Smith JAS. Chem. Phys. 1983; 74: 9.
21. 16. Palmer M, Stephenson D, Smith JAS. Chem. Phys. 1985; 97: 103.
22. 17. Lucken EAC. Nuclear Quadrupole Coupling Constants. Academic Press: London, 1969.
23. 18. Schempp E, Bray PJ. Phys. Lett. A 1967; 25: 414.
24. 19. Guibé L, Lucken EAC. Mol. Phys. 1968; 14: 73.
25. 20. Garcia MLS, Smith JAS, Bavin PMG, Ganellin CR. J. Chem. Soc., Perkin Trans 2 1983; 1391.
26. 21. Olivieri AC, Frydman L, Grasselli M, Diaz E. Magn. Reson. Chem. 1988; 26: 281.
27. 22. Alarcón SH, Jonsen P, Olivieri AC. J. Chem. Soc., Perkin Trans 2 1993; 1783.
28. 23. Taramichi C, Schempp E. Acta Crystallogr., Sect. B 1977; 33: 240.
29. 24. Olivieri AC, Frydman L, Diaz LE. J. Magn. Reson. 1987; 75: 50.
30. 25. Allen FH, Davies JE, Galloy JJ, Johnson O, Kennard O, Macrae CF, Mitchell EM, Mitchell GF, Smith JM, Watson DG. J. Chem. Inf. Comput. Sci. 1991; 31: 187.
31. 26. Blanco S, Löpez JC, Alonso JL, Mó O, Yáñez M, Jagerovic N, Elguero J. J. Mol. Struct. 1995; 344: 241.
32. 27. Olivieri AC. J. Magn. Reson. 1989; 82: 342.