Analysis of 1H and 13C NMR spectra of cis- and trans-10-substituted decal-2-ones by 2D NMR techniques

Magnetic Resonance in Chemistry

Volumn 38, Issue 2, 2000, Pages 108-114

  Di Maio, G ^a   Migneco, L M ^a   Vecchi, E ^a   Iavarone, C ^b  

^a SAPIENZA UNIVERSITY OF ROME   (Italy)

^b CNR   (Italy)

Author keywords

2D NMR; Cis and trans 10 substituted decal 2 ones; Conformational analysis; COSY; HETCOR; NMR

Indexed keywords

CHEMICAL SHIFT; CONFORMATIONS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

2-D NMR; CHEMICAL SHIFT ASSIGNMENT; CIS- AND TRANS-10-SUBSTITUTED DECAL-2-ONE; CONFORMATIONAL ANALYSIS; COSY; DECOUPLINGS; HETCOR; NMR CHEMICAL SHIFTS; NMR SPECTRUM; NMR TECHNIQUES;

DIHEDRAL ANGLE;

EID: 0034134499     PISSN: 07491581     EISSN: None     Source Type: Journal    
DOI: 10.1002/(sici)1097-458x(200002)38:2<108::aid-mrc607>3.0.co;2-a     Document Type: Article

References (18)

1. 1. Di Maio G, Iavarone C, Migneco LM, Vecchi E. Magn. Reson. Chem. 1996; 34: 18.
2. 2. Browne LM, Klinck RE, Stothers JB. Org. Magn. Reson. 1979; 12: 561.
3. 3. Desmaele D. D'Angelo J. Tetrahedron Lett. 1989; 30: 345.
4. 4. Grover SH, Marr DH, Stothers JB, Tun CT. Can. J. Chem. 1975; 53: 1351.
5. 5. Gramain JC, Quirion JC. Magn. Reson. Chem. 1986; 24: 938.
6. 6. Monson R. Advanced Organic Synthesis. Academic Press: New York 1971; 27-28, 81-82.
7. 7. Dreiding AS, Tomasewski AJ. J. Am. Chem. Soc. 1955; 77: 411.
8. 8. Brown HC, Geoghegan PJ Jr. J. Org. Chem. 1970; 35: 1844.
9. 9. Sanders JKM, Hunter BK. Modern NMR Spectroscope. Oxford University Press: Oxford, 1988.
10. 10. Program PC Model Version MMX. Serena Software: Bloomington. IN, 1993.
11. 11. Allinger NL. J. Am. Chem. Soc. 1977; 99: 8127.
12. 12. Allinger NL, Sprague JT. J. Am. Chem. Soc. 1973; 95: 3593.
13. 13. Chemwin 3.0. Softshell International: Grand Junction, CO, 1993.
14. 14. Juckman LM, Sternhell S. Applications of NMR Spectroscopy in Organic Chemistry. Pergamon Press: Oxford, 1969; 281.
15. 15. Jackman LM, Sternhell S. Applications of NMR Spectroscopy in Organic Chemistry. Pergamon Press: Oxford, 1969; 238.
16. 16. Bhacca NS, Williams DH. Applications of NMR Spectroscopy in Organic Chemistry. Holden Day: San Francisco, 1964.
17. 17. Wehrli FW, Wirthlin T. Interpretation of Carbon-13 NMR Spectroscopy. Heyden: London, 1978; 36.
18. 18. Klyne W. Experientia 1956; 12: 119.